Fabrication of high strength in-situ Al-Al3Ti nanocomposite by mechanical alloying and hot extrusion: Investigation of fracture toughness

• Published in: Materials science & engineering. A, Structural materials : properties, microstructure and processing Structural materials : properties, microstructure and processing, 2016-03, Vol.658, p.246-254
• Main Authors: Basiri Tochaee, E., Madaah Hosseini, H.R., Seyed Reihani, S.M.
• Format: Article
• Language: English
• Subjects: Aluminum base alloys; Fracture mechanics; Fracture surfaces; Fracture toughness; Hot extrusion; In-situ aluminum based nanocomposite; Intermetallic compounds; Intermetallics; Mechanical alloying; Microvoid coalescence; Nanocomposites; Scanning electron microscopy; Titanium aluminides
• ISSN: 0921-5093; 1873-4936
• DOI: 10.1016/j.msea.2016.02.010

High energy vibratiory mill was used to produce Nanocrystalline Al-20wt% Ti powders by mechanical alloying. The milled powders were then consolidated by hot extrusion at 530°C. Produced bulk nanocomposite samples were studied by XRD analysis, optical microscopy (OM), Field Emission Scanning Electron Microscopy (FESEM), EDS spectroscopy, densitometry and hardness tests. Three point bending on SENB specimens was applied under quasi static condition to determine the fracture toughness and also investigate the fracture surface using SEM. The results indicated that after extrusion a fully dense Al-Al3Ti nanocomposite with the crystallite size of 200−400nm is produced in which the Al3Ti particles with the size of 50−500nm were homogeneously distributed. The mechanical properties of samples such as modulus, flexural strength and hardness were significantly increased to 130GPa, 910MPa and 136HV, respectively. These results are the consequence of refinement of Al matrix grain size, distribution of Al3Ti nano-particles and the absence of voids. The high density of grain boundries and particle-matrix interfaces provide a lot of sites for nucleation of dimples which leads to the delay in crack initiation stage. Accordingly, the fracture toughness of the nanocomposite sample obtained KQ=27.4MPam which is a high value in comparison with the conventional Al composites. On a macroscopic scale, the fracture surface was brittle and flat, while SEM images showed dimpled fracture surfaces confirming microvoid coalescence as the main fracture mechanism.