Fractographic principles applied to Y-TZP mechanical behavior analysis

• Published in: Journal of the mechanical behavior of biomedical materials 2016-04, Vol.57, p.215-223
• Main Authors: Ramos, Carla Müller, Cesar, Paulo Francisco, Bonfante, Estevam Augusto, Rubo, José Henrique, Wang, Linda, Borges, Ana Flávia Sanches
• Format: Article
• Language: English
• Subjects: Ceramic; Fractography; Fracture toughness; Materials Testing; Mechanical Phenomena; Mechanical properties; Scanning electron microscopy; Strength; Stress, Mechanical; Surface Properties; Tetragonal zirconia polycrystals; Yttria stabilized zirconia; Yttrium; Zirconium; Zirconium dioxide
• ISSN: 1751-6161; 1878-0180
• DOI: 10.1016/j.jmbbm.2015.12.006

The purpose of this study was to evaluate the use of fractography principles to determine the fracture toughness of Y-TZP dental ceramic in which KIc was measured fractographically using controlled-flaw beam bending techniques and to correlate the flaw distribution with the mechanical properties. The Y-TZP blocks studied were: Zirconia Zirklein (ZZ); Zirconcad (ZCA); IPS e.max ZirCad (ZMAX); and In Ceram YZ (ZYZ). Samples were prepared (16mm×4mm×2mm) according to ISO 6872 specifications and subjected to three-point bending at a crosshead speed of 0.5mm/min. Weibull probability curves (95% confidence bounds) were calculated and a contour plot with the Weibull modulus (m) versus characteristic strength (σ0) was used to examine the differences among groups. The fractured surface of each specimen was inspected in a scanning electron microscope (SEM) for qualitative and quantitative fractographic analysis. The critical defect size (c) and fracture toughness (KIc) were estimated. The fractured surfaces of the samples from all groups showed similar fractographic characteristics, except ZCA showed pores and defects. Fracture toughness and the flexural strength values were not different among the groups except for ZCA. The characteristic strength (p