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Magnetization study in solid state formation of lithium-titanium ferrites synthesized by electron beam heating
The solid state formation of substituted lithium-titanium ferrites with chemical formula Li0.5(1+х)Fe2.5−1.5xTixO4 (х = 0.2; 0.4) prepared by two different methods were studied by X-ray diffraction and saturation magnetization analyzes. For the first method, lithium-titanium ferrites were prepared b...
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Published in: | Materials chemistry and physics 2016-06, Vol.176, p.110-114 |
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creator | Surzhikov, Anatoly P. Lysenko, Elena N. Vlasov, Vitaly A. Malyshev, Andrey V. Vasendina, Elena A. |
description | The solid state formation of substituted lithium-titanium ferrites with chemical formula Li0.5(1+х)Fe2.5−1.5xTixO4 (х = 0.2; 0.4) prepared by two different methods were studied by X-ray diffraction and saturation magnetization analyzes. For the first method, lithium-titanium ferrites were prepared by conventional solid state synthesis in laboratory furnace at temperatures of 600, 700 and 750 °C and times of 0, 10, 20, 30, 60, and 120 min. For the second method, the samples were obtained by heating of reaction mixtures in high-energy (2.4 MeV) electron beam using similar time-temperature mode. XRD analysis results for all samples showed a high degree formation of lithium-titanium ferrites, obtained by high-energy electron beam heating at lower temperatures and times of synthesis compared with standard thermal heating. Such samples are characterized by the high values of saturation magnetization due to lithium-titanium ferrites formation. The observed radiation effect consists in significant decrease of the temperature and time of ferrite synthesis compared to conventional thermal heating in high-temperature furnaces. |
doi_str_mv | 10.1016/j.matchemphys.2016.03.037 |
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For the first method, lithium-titanium ferrites were prepared by conventional solid state synthesis in laboratory furnace at temperatures of 600, 700 and 750 °C and times of 0, 10, 20, 30, 60, and 120 min. For the second method, the samples were obtained by heating of reaction mixtures in high-energy (2.4 MeV) electron beam using similar time-temperature mode. XRD analysis results for all samples showed a high degree formation of lithium-titanium ferrites, obtained by high-energy electron beam heating at lower temperatures and times of synthesis compared with standard thermal heating. Such samples are characterized by the high values of saturation magnetization due to lithium-titanium ferrites formation. The observed radiation effect consists in significant decrease of the temperature and time of ferrite synthesis compared to conventional thermal heating in high-temperature furnaces.</description><identifier>ISSN: 0254-0584</identifier><identifier>EISSN: 1879-3312</identifier><identifier>DOI: 10.1016/j.matchemphys.2016.03.037</identifier><language>eng</language><publisher>Elsevier B.V</publisher><subject>Compaction ; Electron beam heating ; Ferrites ; Formations ; Furnaces ; Heat treatment ; Heating ; Magnetic materials ; Magnetic properties ; Powder diffraction ; Saturation (magnetic) ; Solid state ; Synthesis</subject><ispartof>Materials chemistry and physics, 2016-06, Vol.176, p.110-114</ispartof><rights>2016 Elsevier B.V.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c354t-d8013efbf19fd7bf8f31be6933e5f3c3edd92364b2eb6e3f15b9187419e93b363</citedby><cites>FETCH-LOGICAL-c354t-d8013efbf19fd7bf8f31be6933e5f3c3edd92364b2eb6e3f15b9187419e93b363</cites><orcidid>0000-0002-5946-2117</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids></links><search><creatorcontrib>Surzhikov, Anatoly P.</creatorcontrib><creatorcontrib>Lysenko, Elena N.</creatorcontrib><creatorcontrib>Vlasov, Vitaly A.</creatorcontrib><creatorcontrib>Malyshev, Andrey V.</creatorcontrib><creatorcontrib>Vasendina, Elena A.</creatorcontrib><title>Magnetization study in solid state formation of lithium-titanium ferrites synthesized by electron beam heating</title><title>Materials chemistry and physics</title><description>The solid state formation of substituted lithium-titanium ferrites with chemical formula Li0.5(1+х)Fe2.5−1.5xTixO4 (х = 0.2; 0.4) prepared by two different methods were studied by X-ray diffraction and saturation magnetization analyzes. For the first method, lithium-titanium ferrites were prepared by conventional solid state synthesis in laboratory furnace at temperatures of 600, 700 and 750 °C and times of 0, 10, 20, 30, 60, and 120 min. For the second method, the samples were obtained by heating of reaction mixtures in high-energy (2.4 MeV) electron beam using similar time-temperature mode. XRD analysis results for all samples showed a high degree formation of lithium-titanium ferrites, obtained by high-energy electron beam heating at lower temperatures and times of synthesis compared with standard thermal heating. Such samples are characterized by the high values of saturation magnetization due to lithium-titanium ferrites formation. The observed radiation effect consists in significant decrease of the temperature and time of ferrite synthesis compared to conventional thermal heating in high-temperature furnaces.</description><subject>Compaction</subject><subject>Electron beam heating</subject><subject>Ferrites</subject><subject>Formations</subject><subject>Furnaces</subject><subject>Heat treatment</subject><subject>Heating</subject><subject>Magnetic materials</subject><subject>Magnetic properties</subject><subject>Powder diffraction</subject><subject>Saturation (magnetic)</subject><subject>Solid state</subject><subject>Synthesis</subject><issn>0254-0584</issn><issn>1879-3312</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><recordid>eNqNUMtKAzEUDaJgrf5D3LmZMZk7z6UUX1Bxo-uQTG46KfOoSSpMv96UunApXLjnPs6Bcwi55SzljJf323SQoe1w2HWzT7O4ShnEqs7IgtdVkwDw7JwsWFbkCSvq_JJceb9ljFecw4KMb3IzYrAHGew0Uh_2eqY2gqm3Oo4yIDWTG07nydDehs7uhyTYIMcIqEHnbEBP_TyGDr09oKZqpthjG1wkKZQD7TAqjJtrcmFk7_Hmty_J59Pjx-olWb8_v64e1kkLRR4SXTMOaJThjdGVMrUBrrBsALAw0AJq3WRQ5ipDVSIYXqgmus15gw0oKGFJ7k66Ozd97dEHMVjfYt_LEae9F7yOeeQ5y3l8bU6vrZu8d2jEztlBullwJo4Zi634k7E4ZiwYxKoid3XiYvTybdEJ31ocW9TWRfdCT_YfKj-0ZI8D</recordid><startdate>20160615</startdate><enddate>20160615</enddate><creator>Surzhikov, Anatoly P.</creator><creator>Lysenko, Elena N.</creator><creator>Vlasov, Vitaly A.</creator><creator>Malyshev, Andrey V.</creator><creator>Vasendina, Elena A.</creator><general>Elsevier B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope><orcidid>https://orcid.org/0000-0002-5946-2117</orcidid></search><sort><creationdate>20160615</creationdate><title>Magnetization study in solid state formation of lithium-titanium ferrites synthesized by electron beam heating</title><author>Surzhikov, Anatoly P. ; Lysenko, Elena N. ; Vlasov, Vitaly A. ; Malyshev, Andrey V. ; Vasendina, Elena A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c354t-d8013efbf19fd7bf8f31be6933e5f3c3edd92364b2eb6e3f15b9187419e93b363</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2016</creationdate><topic>Compaction</topic><topic>Electron beam heating</topic><topic>Ferrites</topic><topic>Formations</topic><topic>Furnaces</topic><topic>Heat treatment</topic><topic>Heating</topic><topic>Magnetic materials</topic><topic>Magnetic properties</topic><topic>Powder diffraction</topic><topic>Saturation (magnetic)</topic><topic>Solid state</topic><topic>Synthesis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Surzhikov, Anatoly P.</creatorcontrib><creatorcontrib>Lysenko, Elena N.</creatorcontrib><creatorcontrib>Vlasov, Vitaly A.</creatorcontrib><creatorcontrib>Malyshev, Andrey V.</creatorcontrib><creatorcontrib>Vasendina, Elena A.</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Materials chemistry and physics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Surzhikov, Anatoly P.</au><au>Lysenko, Elena N.</au><au>Vlasov, Vitaly A.</au><au>Malyshev, Andrey V.</au><au>Vasendina, Elena A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Magnetization study in solid state formation of lithium-titanium ferrites synthesized by electron beam heating</atitle><jtitle>Materials chemistry and physics</jtitle><date>2016-06-15</date><risdate>2016</risdate><volume>176</volume><spage>110</spage><epage>114</epage><pages>110-114</pages><issn>0254-0584</issn><eissn>1879-3312</eissn><abstract>The solid state formation of substituted lithium-titanium ferrites with chemical formula Li0.5(1+х)Fe2.5−1.5xTixO4 (х = 0.2; 0.4) prepared by two different methods were studied by X-ray diffraction and saturation magnetization analyzes. For the first method, lithium-titanium ferrites were prepared by conventional solid state synthesis in laboratory furnace at temperatures of 600, 700 and 750 °C and times of 0, 10, 20, 30, 60, and 120 min. For the second method, the samples were obtained by heating of reaction mixtures in high-energy (2.4 MeV) electron beam using similar time-temperature mode. XRD analysis results for all samples showed a high degree formation of lithium-titanium ferrites, obtained by high-energy electron beam heating at lower temperatures and times of synthesis compared with standard thermal heating. Such samples are characterized by the high values of saturation magnetization due to lithium-titanium ferrites formation. The observed radiation effect consists in significant decrease of the temperature and time of ferrite synthesis compared to conventional thermal heating in high-temperature furnaces.</abstract><pub>Elsevier B.V</pub><doi>10.1016/j.matchemphys.2016.03.037</doi><tpages>5</tpages><orcidid>https://orcid.org/0000-0002-5946-2117</orcidid></addata></record> |
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subjects | Compaction Electron beam heating Ferrites Formations Furnaces Heat treatment Heating Magnetic materials Magnetic properties Powder diffraction Saturation (magnetic) Solid state Synthesis |
title | Magnetization study in solid state formation of lithium-titanium ferrites synthesized by electron beam heating |
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