The analysis of bainitic ferrite microstructure in microalloyed plate steels through quantitative characterization of intervariant boundaries

• Published in: Materials science & engineering. A, Structural materials : properties, microstructure and processing Structural materials : properties, microstructure and processing, 2016-07, Vol.669, p.459-468
• Main Authors: Kang, Singon, Speer, John G., Regier, Ryan W., Nako, Hidenori, Kennett, Shane C., Findley, Kip O.
• Format: Article
• Language: English
• Subjects: Bainitic steels; Boundaries; Crystallography; Electron back scatter diffraction; Electron backscatter diffraction; Ferrite; Heat treatment; Microalloying; Microstructure; Misorientation; Phase transformation; Structural steels; Variant selection
• ISSN: 0921-5093; 1873-4936
• DOI: 10.1016/j.msea.2016.05.111

Electron backscatter diffraction (EBSD) measurements were performed to investigate the bainitic ferrite microstructure in low-carbon, microalloyed steels with varying C and Mn contents. Fully austenitized samples were isothermally heat treated at temperatures ranging from 450 to 550°C to form bainitic ferrite. The bainitic ferrite microstructures and boundary characteristics obtained from the EBSD measurements were analyzed based on an inferred Kurdjumov-Sachs (K-S) orientation relationship. The heat treated samples exhibit a microstructure composed of laths and the lath aspect ratio tends to increase at lower isothermal heat treatment temperatures. High fractions of boundary misorientation angles below 5° are observed, which are due to lath boundaries in the microstructure. Additionally, misorientations of approximately 7°, 53° and 60° are observed, which are related to the sub-block, packet, and block boundaries, respectively. With decreasing isothermal heat treatment temperature, there is an increase of block boundaries; these boundaries are intervariant boundaries between different blocks within a packet, most of which have the misorientation angle of 60°. The specimens with a higher carbon level contained increased length of block boundaries, whereas the addition of Mn moderated the dependence of block boundary length on the heat treatment temperature within the experimental temperature range. Meanwhile, the length of intervariant boundaries of both packet and sub-block character did not vary much with heat treatment temperature and alloy composition.