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Recovery of Ductility in Ultrafine-Grained Low-Carbon Steel Processed Through Equal-Channel Angular Pressing Followed by Cold Rolling and Flash Annealing
The low-carbon steel workpieces are deformed by equal-channel angular pressing at 293 K (20 °C) up to an equivalent strain of ~12 using route B c , which results in the bulk ultrafine-grained (UFG) structure with high dislocation density and partial dissolution of cementite. The yield strength (YS)...
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Published in: | Metallurgical and materials transactions. A, Physical metallurgy and materials science Physical metallurgy and materials science, 2017-03, Vol.48 (3), p.1189-1203 |
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container_title | Metallurgical and materials transactions. A, Physical metallurgy and materials science |
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description | The low-carbon steel workpieces are deformed by equal-channel angular pressing at 293 K (20 °C) up to an equivalent strain of ~12 using route
B
c
, which results in the bulk ultrafine-grained (UFG) structure with high dislocation density and partial dissolution of cementite. The yield strength (YS) is enhanced from 208 (as-received) to 872 MPa and the tensile strength is increased from 362 to 996 MPa, but the material loses total elongation (TE) from 36.2 to 2.9 pct. Cold rolling of equal-channel angular pressed steel produces the refined structure of grain size 0.11
μ
m. The YS increases further to 924 MPa with a marginal gain in ductility due to the reappearance of the
γ
fiber component. Flash annealing the samples, which were equal-channel angular pressed followed by cold rolling, at 873 K (600 °C) results in 27 pct of micron-sized (9
µ
m) ferrite grains in submicron-sized ( |
doi_str_mv | 10.1007/s11661-016-3892-x |
format | article |
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B
c
, which results in the bulk ultrafine-grained (UFG) structure with high dislocation density and partial dissolution of cementite. The yield strength (YS) is enhanced from 208 (as-received) to 872 MPa and the tensile strength is increased from 362 to 996 MPa, but the material loses total elongation (TE) from 36.2 to 2.9 pct. Cold rolling of equal-channel angular pressed steel produces the refined structure of grain size 0.11
μ
m. The YS increases further to 924 MPa with a marginal gain in ductility due to the reappearance of the
γ
fiber component. Flash annealing the samples, which were equal-channel angular pressed followed by cold rolling, at 873 K (600 °C) results in 27 pct of micron-sized (9
µ
m) ferrite grains in submicron-sized (<1
µ
m) matrix with a reduced defect density and small amount of precipitation of cementite. TE increases from 2.9 to 23.3 pct. The material retains a YS of 484 MPa and tensile strength of 517 MPa, which are higher than those of the as-received material. The UFG grains are failed by cleavage, but the micron-sized grains display ductile fracture. The ductility of the flash-annealed material is recovered significantly due to bimodal grain size distribution in ferrite and the development of a good amount of
γ
fiber texture components. The major contribution toward recovery of ductility comes from the bimodal grain size distribution in ferrite rather the precipitation of cementite.</description><identifier>ISSN: 1073-5623</identifier><identifier>EISSN: 1543-1940</identifier><identifier>DOI: 10.1007/s11661-016-3892-x</identifier><identifier>CODEN: MMTAEB</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Annealing ; Cementite ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Cold rolling ; Ductility ; Equal channel angular pressing ; Ferrite ; Grains ; Low carbon steel ; Materials Science ; Metallic Materials ; Metallurgy ; Nanotechnology ; Steel alloys ; Structural Materials ; Surfaces and Interfaces ; Texture ; Thin Films ; Yield strength</subject><ispartof>Metallurgical and materials transactions. A, Physical metallurgy and materials science, 2017-03, Vol.48 (3), p.1189-1203</ispartof><rights>The Minerals, Metals & Materials Society and ASM International 2016</rights><rights>Metallurgical and Materials Transactions A is a copyright of Springer, 2017.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c349t-b63c149617ec041a4637b99a995cf74b628bed2cbc455a486491162e27e93e9d3</citedby><cites>FETCH-LOGICAL-c349t-b63c149617ec041a4637b99a995cf74b628bed2cbc455a486491162e27e93e9d3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27923,27924</link.rule.ids></links><search><creatorcontrib>Singh, Raj Bahadur</creatorcontrib><creatorcontrib>Mukhopadhyay, N. K.</creatorcontrib><creatorcontrib>Sastry, G. V. S.</creatorcontrib><creatorcontrib>Manna, R.</creatorcontrib><title>Recovery of Ductility in Ultrafine-Grained Low-Carbon Steel Processed Through Equal-Channel Angular Pressing Followed by Cold Rolling and Flash Annealing</title><title>Metallurgical and materials transactions. A, Physical metallurgy and materials science</title><addtitle>Metall Mater Trans A</addtitle><description>The low-carbon steel workpieces are deformed by equal-channel angular pressing at 293 K (20 °C) up to an equivalent strain of ~12 using route
B
c
, which results in the bulk ultrafine-grained (UFG) structure with high dislocation density and partial dissolution of cementite. The yield strength (YS) is enhanced from 208 (as-received) to 872 MPa and the tensile strength is increased from 362 to 996 MPa, but the material loses total elongation (TE) from 36.2 to 2.9 pct. Cold rolling of equal-channel angular pressed steel produces the refined structure of grain size 0.11
μ
m. The YS increases further to 924 MPa with a marginal gain in ductility due to the reappearance of the
γ
fiber component. Flash annealing the samples, which were equal-channel angular pressed followed by cold rolling, at 873 K (600 °C) results in 27 pct of micron-sized (9
µ
m) ferrite grains in submicron-sized (<1
µ
m) matrix with a reduced defect density and small amount of precipitation of cementite. TE increases from 2.9 to 23.3 pct. The material retains a YS of 484 MPa and tensile strength of 517 MPa, which are higher than those of the as-received material. The UFG grains are failed by cleavage, but the micron-sized grains display ductile fracture. The ductility of the flash-annealed material is recovered significantly due to bimodal grain size distribution in ferrite and the development of a good amount of
γ
fiber texture components. The major contribution toward recovery of ductility comes from the bimodal grain size distribution in ferrite rather the precipitation of cementite.</description><subject>Annealing</subject><subject>Cementite</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Cold rolling</subject><subject>Ductility</subject><subject>Equal channel angular pressing</subject><subject>Ferrite</subject><subject>Grains</subject><subject>Low carbon steel</subject><subject>Materials Science</subject><subject>Metallic Materials</subject><subject>Metallurgy</subject><subject>Nanotechnology</subject><subject>Steel alloys</subject><subject>Structural Materials</subject><subject>Surfaces and Interfaces</subject><subject>Texture</subject><subject>Thin Films</subject><subject>Yield strength</subject><issn>1073-5623</issn><issn>1543-1940</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><recordid>eNp1kcFq3DAQhkVpoek2D5CboJde1EqWLFvH4GbTwkJLmpyFLI93HRQpkewk-yh928yyPZRCTjPM__3DMD8hZ4J_EZw3X4sQWgvGhWayNRV7fkNORK0kE0bxt9jzRrJaV_I9-VDKLedcGKlPyJ8r8OkR8p6mkX5b_DyFad7TKdKbMGc3ThHYZXZYBrpJT6xzuU-R_p4BAv2Vk4dSULre5bRsd_TiYXGBdTsXI-rncbsEl5FDaopbuk4hpCfk-z3tUhjoFQ4OgosDXQdXduiJ4A6zj-Td6EKB0791RW7WF9fdd7b5efmjO98wL5WZWa-lF8po0YDnSjilZdMb44yp_dioXldtD0Ple6_q2qlWK4OvqqBqwEgwg1yRz8e99zk9LFBmezcVDyG4CGkpVrStErJWnCP66T_0Ni054nVI6bqq2xZfviLiSPmcSskw2vs83bm8t4LbQ1j2GJbFsOwhLPuMnuroKcjGLeR_Nr9qegHu5JiL</recordid><startdate>20170301</startdate><enddate>20170301</enddate><creator>Singh, Raj Bahadur</creator><creator>Mukhopadhyay, N. K.</creator><creator>Sastry, G. V. S.</creator><creator>Manna, R.</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>4T-</scope><scope>4U-</scope><scope>7SR</scope><scope>7XB</scope><scope>88I</scope><scope>8AF</scope><scope>8AO</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>8FK</scope><scope>8G5</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>GNUQQ</scope><scope>GUQSH</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>L6V</scope><scope>M2O</scope><scope>M2P</scope><scope>M7S</scope><scope>MBDVC</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope><scope>Q9U</scope><scope>S0X</scope></search><sort><creationdate>20170301</creationdate><title>Recovery of Ductility in Ultrafine-Grained Low-Carbon Steel Processed Through Equal-Channel Angular Pressing Followed by Cold Rolling and Flash Annealing</title><author>Singh, Raj Bahadur ; Mukhopadhyay, N. K. ; Sastry, G. V. S. ; Manna, R.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c349t-b63c149617ec041a4637b99a995cf74b628bed2cbc455a486491162e27e93e9d3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Annealing</topic><topic>Cementite</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Cold rolling</topic><topic>Ductility</topic><topic>Equal channel angular pressing</topic><topic>Ferrite</topic><topic>Grains</topic><topic>Low carbon steel</topic><topic>Materials Science</topic><topic>Metallic Materials</topic><topic>Metallurgy</topic><topic>Nanotechnology</topic><topic>Steel alloys</topic><topic>Structural Materials</topic><topic>Surfaces and Interfaces</topic><topic>Texture</topic><topic>Thin Films</topic><topic>Yield strength</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Singh, Raj Bahadur</creatorcontrib><creatorcontrib>Mukhopadhyay, N. 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A, Physical metallurgy and materials science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Singh, Raj Bahadur</au><au>Mukhopadhyay, N. K.</au><au>Sastry, G. V. S.</au><au>Manna, R.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Recovery of Ductility in Ultrafine-Grained Low-Carbon Steel Processed Through Equal-Channel Angular Pressing Followed by Cold Rolling and Flash Annealing</atitle><jtitle>Metallurgical and materials transactions. A, Physical metallurgy and materials science</jtitle><stitle>Metall Mater Trans A</stitle><date>2017-03-01</date><risdate>2017</risdate><volume>48</volume><issue>3</issue><spage>1189</spage><epage>1203</epage><pages>1189-1203</pages><issn>1073-5623</issn><eissn>1543-1940</eissn><coden>MMTAEB</coden><abstract>The low-carbon steel workpieces are deformed by equal-channel angular pressing at 293 K (20 °C) up to an equivalent strain of ~12 using route
B
c
, which results in the bulk ultrafine-grained (UFG) structure with high dislocation density and partial dissolution of cementite. The yield strength (YS) is enhanced from 208 (as-received) to 872 MPa and the tensile strength is increased from 362 to 996 MPa, but the material loses total elongation (TE) from 36.2 to 2.9 pct. Cold rolling of equal-channel angular pressed steel produces the refined structure of grain size 0.11
μ
m. The YS increases further to 924 MPa with a marginal gain in ductility due to the reappearance of the
γ
fiber component. Flash annealing the samples, which were equal-channel angular pressed followed by cold rolling, at 873 K (600 °C) results in 27 pct of micron-sized (9
µ
m) ferrite grains in submicron-sized (<1
µ
m) matrix with a reduced defect density and small amount of precipitation of cementite. TE increases from 2.9 to 23.3 pct. The material retains a YS of 484 MPa and tensile strength of 517 MPa, which are higher than those of the as-received material. The UFG grains are failed by cleavage, but the micron-sized grains display ductile fracture. The ductility of the flash-annealed material is recovered significantly due to bimodal grain size distribution in ferrite and the development of a good amount of
γ
fiber texture components. The major contribution toward recovery of ductility comes from the bimodal grain size distribution in ferrite rather the precipitation of cementite.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s11661-016-3892-x</doi><tpages>15</tpages></addata></record> |
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subjects | Annealing Cementite Characterization and Evaluation of Materials Chemistry and Materials Science Cold rolling Ductility Equal channel angular pressing Ferrite Grains Low carbon steel Materials Science Metallic Materials Metallurgy Nanotechnology Steel alloys Structural Materials Surfaces and Interfaces Texture Thin Films Yield strength |
title | Recovery of Ductility in Ultrafine-Grained Low-Carbon Steel Processed Through Equal-Channel Angular Pressing Followed by Cold Rolling and Flash Annealing |
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