Synthesis and characterization of Fe sub(3)O sub(4)l sub(2)O sub(3) nanoparticles and investigation its catalyst application

In the current study, Fe sub(3)O sub(4)l sub(2)O sub(3) nanoparticles were successfully synthesized through the simple and cost effective co-precipitation method and were characterized using XRD, SEM, and FT-IR analysis. Since, oxidation of alcohols is one of the most fundamental and challenging pro...

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Published in:Journal of materials science. Materials in electronics 2017-04, Vol.28 (7), p.5360-5365
Main Authors: Tekiye, Elahe-Sadat, Aghajani, Zahra, Sharif, Mahboubeh A
Format: Article
Language:English
Subjects:
Alcohols
Analysis of variance
Catalysts
Electronics
Nanoparticles
Nanostructure
Oxidation
Solvents
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Aghajani, Zahra
Sharif, Mahboubeh A
description In the current study, Fe sub(3)O sub(4)l sub(2)O sub(3) nanoparticles were successfully synthesized through the simple and cost effective co-precipitation method and were characterized using XRD, SEM, and FT-IR analysis. Since, oxidation of alcohols is one of the most fundamental and challenging processes in organic chemistry, therefore; Fe sub(3)O sub(4)l sub(2)O sub(3) nanoparticles were applied as the catalyst for oxidation of alcohol. Besides, the effects of several oxidation reactions parameters such as catalyst concentration, type of solvents, and reaction temperature were studied on the oxidation percentage through the analysis of variance (ANOVA). In addition, recyclability of as-synthesized Fe sub(3)O sub(4)l sub(2)O sub(3) catalyst was studied which demonstrated that Fe sub(3)O sub(4)l sub(2)O sub(3) nano catalyst could be reused up to five runs without any significant loss of activities. The oxidation results indicated that Fe sub(3)O sub(4)l sub(2)O sub(3) nano catalyst provides a high oxidation yield of 91%.
doi_str_mv 10.1007/s10854-016-6195-5
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subjects Alcohols
Analysis of variance
Catalysts
Electronics
Nanoparticles
Nanostructure
Oxidation
Solvents
title Synthesis and characterization of Fe sub(3)O sub(4)l sub(2)O sub(3) nanoparticles and investigation its catalyst application
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