Micro Thin-Layer Chromatography Fingerprints of Selected Basil Species and Their Chemometric Analysis

The dried aerial parts of 12 plants of Ocimum spp. were extracted with the Soxhlet apparatus using dichloromethane and methanol as solvents. A micro-TLC system with silica and a normal-phase solvent system (propan-2-ol-n-heptane-formic acid) was used for the chemometric analysis of 12 selected basil...

Full description

Saved in:
Bibliographic Details
Published in:Journal of AOAC International 2017-07, Vol.100 (4), p.916-921
Main Authors: Hawrył, Mirosław A, Świeboda, Ryszard, Hawrył, Anna, Niemiec, Małgorzata, Waksmundzka-Hajnos, Monika
Format: Article
Language:English
Subjects:
Basils
Chemical properties
Chromatography, Thin Layer
Ocimum basilicum - chemistry
Phytochemicals - analysis
Plant Components, Aerial - chemistry
Plant products
Testing
Thin layer chromatography
Citations: Items that cite this one
Online Access:Get full text
Tags: Add Tag
No Tags, Be the first to tag this record!
cited_by cdi_FETCH-LOGICAL-c338t-3a686d9949e5d3af6852a9e774ce073c71aba50489c745b6e47fbf69189e01073
cites
container_end_page 921
container_issue 4
container_start_page 916
container_title Journal of AOAC International
container_volume 100
creator Hawrył, Mirosław A
Świeboda, Ryszard
Hawrył, Anna
Niemiec, Małgorzata
Waksmundzka-Hajnos, Monika
description The dried aerial parts of 12 plants of Ocimum spp. were extracted with the Soxhlet apparatus using dichloromethane and methanol as solvents. A micro-TLC system with silica and a normal-phase solvent system (propan-2-ol-n-heptane-formic acid) was used for the chemometric analysis of 12 selected basil methanolic extracts. Some indices of similarity (Pearson's correlation coefficient, determination coefficient, congruence coefficient, and Euclidean, Manhattan (city-block), Chebyshev, and Hausdorff distances) were calculated on the basis of thin-layer chromatograms using ImageJ software. Principal component analysis was also performed. The method allowed the comparison of the analyzed extracts and confirmed the identities of two selected unknown plants.
doi_str_mv 10.5740/jaoacint.17-0166
format article
fullrecord <record><control><sourceid>gale_proqu</sourceid><recordid>TN_cdi_proquest_miscellaneous_1910800927</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><galeid>A503272412</galeid><sourcerecordid>A503272412</sourcerecordid><originalsourceid>FETCH-LOGICAL-c338t-3a686d9949e5d3af6852a9e774ce073c71aba50489c745b6e47fbf69189e01073</originalsourceid><addsrcrecordid>eNo9kTFv2zAQhYkiQZOm3TsVHLPIOVIUKY6O0bQBXHRIMhNn6mQzkESHlAf_-9JwUnAgQbzv3eE9xr4LWDRGwd0rRvRhmhfCVCC0_sSuhVWqMlbKi_IGDVUtjbhiX3J-BVBCg_zMrmSrZa0bec3oT_Ap8uddmKo1Hinx1S7FEee4TbjfHflDmLaU9qlMyTz2_IkG8jN1_B5zGPjTnnygzHHqigmFE09jHGlOwfPlhMMxh_yVXfY4ZPr2ft-wl4efz6vf1frvr8fVcl35um7nqkbd6s5aZanpaux120i0ZIzyBKb2RuAGG1Ct9UY1G03K9JteW9FaAlEUN-z27LtP8e1AeXZjyJ6GASeKh-yEFdACWHmSLs7SLQ7kwtTHOaEvp6Mx-DhRH8r_soGSn1RCFgDOQMkr50S9K6GMmI5OgDu14T7acMK4UxsF-fG-zmEzUvcf-Ii__gf-7ods</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1910800927</pqid></control><display><type>article</type><title>Micro Thin-Layer Chromatography Fingerprints of Selected Basil Species and Their Chemometric Analysis</title><source>Oxford Journals Online</source><creator>Hawrył, Mirosław A ; Świeboda, Ryszard ; Hawrył, Anna ; Niemiec, Małgorzata ; Waksmundzka-Hajnos, Monika</creator><creatorcontrib>Hawrył, Mirosław A ; Świeboda, Ryszard ; Hawrył, Anna ; Niemiec, Małgorzata ; Waksmundzka-Hajnos, Monika</creatorcontrib><description>The dried aerial parts of 12 plants of Ocimum spp. were extracted with the Soxhlet apparatus using dichloromethane and methanol as solvents. A micro-TLC system with silica and a normal-phase solvent system (propan-2-ol-n-heptane-formic acid) was used for the chemometric analysis of 12 selected basil methanolic extracts. Some indices of similarity (Pearson's correlation coefficient, determination coefficient, congruence coefficient, and Euclidean, Manhattan (city-block), Chebyshev, and Hausdorff distances) were calculated on the basis of thin-layer chromatograms using ImageJ software. Principal component analysis was also performed. The method allowed the comparison of the analyzed extracts and confirmed the identities of two selected unknown plants.</description><identifier>ISSN: 1060-3271</identifier><identifier>EISSN: 1944-7922</identifier><identifier>DOI: 10.5740/jaoacint.17-0166</identifier><identifier>PMID: 28623652</identifier><language>eng</language><publisher>England: Oxford University Press</publisher><subject>Basils ; Chemical properties ; Chromatography, Thin Layer ; Ocimum basilicum - chemistry ; Phytochemicals - analysis ; Plant Components, Aerial - chemistry ; Plant products ; Testing ; Thin layer chromatography</subject><ispartof>Journal of AOAC International, 2017-07, Vol.100 (4), p.916-921</ispartof><rights>COPYRIGHT 2017 Oxford University Press</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c338t-3a686d9949e5d3af6852a9e774ce073c71aba50489c745b6e47fbf69189e01073</citedby></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/28623652$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Hawrył, Mirosław A</creatorcontrib><creatorcontrib>Świeboda, Ryszard</creatorcontrib><creatorcontrib>Hawrył, Anna</creatorcontrib><creatorcontrib>Niemiec, Małgorzata</creatorcontrib><creatorcontrib>Waksmundzka-Hajnos, Monika</creatorcontrib><title>Micro Thin-Layer Chromatography Fingerprints of Selected Basil Species and Their Chemometric Analysis</title><title>Journal of AOAC International</title><addtitle>J AOAC Int</addtitle><description>The dried aerial parts of 12 plants of Ocimum spp. were extracted with the Soxhlet apparatus using dichloromethane and methanol as solvents. A micro-TLC system with silica and a normal-phase solvent system (propan-2-ol-n-heptane-formic acid) was used for the chemometric analysis of 12 selected basil methanolic extracts. Some indices of similarity (Pearson's correlation coefficient, determination coefficient, congruence coefficient, and Euclidean, Manhattan (city-block), Chebyshev, and Hausdorff distances) were calculated on the basis of thin-layer chromatograms using ImageJ software. Principal component analysis was also performed. The method allowed the comparison of the analyzed extracts and confirmed the identities of two selected unknown plants.</description><subject>Basils</subject><subject>Chemical properties</subject><subject>Chromatography, Thin Layer</subject><subject>Ocimum basilicum - chemistry</subject><subject>Phytochemicals - analysis</subject><subject>Plant Components, Aerial - chemistry</subject><subject>Plant products</subject><subject>Testing</subject><subject>Thin layer chromatography</subject><issn>1060-3271</issn><issn>1944-7922</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><recordid>eNo9kTFv2zAQhYkiQZOm3TsVHLPIOVIUKY6O0bQBXHRIMhNn6mQzkESHlAf_-9JwUnAgQbzv3eE9xr4LWDRGwd0rRvRhmhfCVCC0_sSuhVWqMlbKi_IGDVUtjbhiX3J-BVBCg_zMrmSrZa0bec3oT_Ap8uddmKo1Hinx1S7FEee4TbjfHflDmLaU9qlMyTz2_IkG8jN1_B5zGPjTnnygzHHqigmFE09jHGlOwfPlhMMxh_yVXfY4ZPr2ft-wl4efz6vf1frvr8fVcl35um7nqkbd6s5aZanpaux120i0ZIzyBKb2RuAGG1Ct9UY1G03K9JteW9FaAlEUN-z27LtP8e1AeXZjyJ6GASeKh-yEFdACWHmSLs7SLQ7kwtTHOaEvp6Mx-DhRH8r_soGSn1RCFgDOQMkr50S9K6GMmI5OgDu14T7acMK4UxsF-fG-zmEzUvcf-Ii__gf-7ods</recordid><startdate>20170701</startdate><enddate>20170701</enddate><creator>Hawrył, Mirosław A</creator><creator>Świeboda, Ryszard</creator><creator>Hawrył, Anna</creator><creator>Niemiec, Małgorzata</creator><creator>Waksmundzka-Hajnos, Monika</creator><general>Oxford University Press</general><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20170701</creationdate><title>Micro Thin-Layer Chromatography Fingerprints of Selected Basil Species and Their Chemometric Analysis</title><author>Hawrył, Mirosław A ; Świeboda, Ryszard ; Hawrył, Anna ; Niemiec, Małgorzata ; Waksmundzka-Hajnos, Monika</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c338t-3a686d9949e5d3af6852a9e774ce073c71aba50489c745b6e47fbf69189e01073</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Basils</topic><topic>Chemical properties</topic><topic>Chromatography, Thin Layer</topic><topic>Ocimum basilicum - chemistry</topic><topic>Phytochemicals - analysis</topic><topic>Plant Components, Aerial - chemistry</topic><topic>Plant products</topic><topic>Testing</topic><topic>Thin layer chromatography</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Hawrył, Mirosław A</creatorcontrib><creatorcontrib>Świeboda, Ryszard</creatorcontrib><creatorcontrib>Hawrył, Anna</creatorcontrib><creatorcontrib>Niemiec, Małgorzata</creatorcontrib><creatorcontrib>Waksmundzka-Hajnos, Monika</creatorcontrib><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of AOAC International</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Hawrył, Mirosław A</au><au>Świeboda, Ryszard</au><au>Hawrył, Anna</au><au>Niemiec, Małgorzata</au><au>Waksmundzka-Hajnos, Monika</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Micro Thin-Layer Chromatography Fingerprints of Selected Basil Species and Their Chemometric Analysis</atitle><jtitle>Journal of AOAC International</jtitle><addtitle>J AOAC Int</addtitle><date>2017-07-01</date><risdate>2017</risdate><volume>100</volume><issue>4</issue><spage>916</spage><epage>921</epage><pages>916-921</pages><issn>1060-3271</issn><eissn>1944-7922</eissn><abstract>The dried aerial parts of 12 plants of Ocimum spp. were extracted with the Soxhlet apparatus using dichloromethane and methanol as solvents. A micro-TLC system with silica and a normal-phase solvent system (propan-2-ol-n-heptane-formic acid) was used for the chemometric analysis of 12 selected basil methanolic extracts. Some indices of similarity (Pearson's correlation coefficient, determination coefficient, congruence coefficient, and Euclidean, Manhattan (city-block), Chebyshev, and Hausdorff distances) were calculated on the basis of thin-layer chromatograms using ImageJ software. Principal component analysis was also performed. The method allowed the comparison of the analyzed extracts and confirmed the identities of two selected unknown plants.</abstract><cop>England</cop><pub>Oxford University Press</pub><pmid>28623652</pmid><doi>10.5740/jaoacint.17-0166</doi><tpages>6</tpages></addata></record>
fulltext fulltext
identifier ISSN: 1060-3271
ispartof Journal of AOAC International, 2017-07, Vol.100 (4), p.916-921
issn 1060-3271
1944-7922
language eng
recordid cdi_proquest_miscellaneous_1910800927
source Oxford Journals Online
subjects Basils
Chemical properties
Chromatography, Thin Layer
Ocimum basilicum - chemistry
Phytochemicals - analysis
Plant Components, Aerial - chemistry
Plant products
Testing
Thin layer chromatography
title Micro Thin-Layer Chromatography Fingerprints of Selected Basil Species and Their Chemometric Analysis
url http://sfxeu10.hosted.exlibrisgroup.com/loughborough?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-12-25T06%3A35%3A35IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-gale_proqu&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Micro%20Thin-Layer%20Chromatography%20Fingerprints%20of%20Selected%20Basil%20Species%20and%20Their%20Chemometric%20Analysis&rft.jtitle=Journal%20of%20AOAC%20International&rft.au=Hawry%C5%82,%20Miros%C5%82aw%20A&rft.date=2017-07-01&rft.volume=100&rft.issue=4&rft.spage=916&rft.epage=921&rft.pages=916-921&rft.issn=1060-3271&rft.eissn=1944-7922&rft_id=info:doi/10.5740/jaoacint.17-0166&rft_dat=%3Cgale_proqu%3EA503272412%3C/gale_proqu%3E%3Cgrp_id%3Ecdi_FETCH-LOGICAL-c338t-3a686d9949e5d3af6852a9e774ce073c71aba50489c745b6e47fbf69189e01073%3C/grp_id%3E%3Coa%3E%3C/oa%3E%3Curl%3E%3C/url%3E&rft_id=info:oai/&rft_pqid=1910800927&rft_id=info:pmid/28623652&rft_galeid=A503272412&rfr_iscdi=true