Synthesis of 2‐d‐acrylamide

2‐d‐Acrylamide was synthesized via the 2‐step procedure starting from acrylonitrile and deuterium oxide. This procedure affords 2‐d‐acrylamide in 99.9% chemical purity and 98.4% isotopic enrichment. 2‐d‐Acrylamide was synthesized via the 2‐step procedure starting from acrylonitrile and deuterium oxi...

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Bibliographic Details
Published in:Journal of labelled compounds & radiopharmaceuticals 2018-06, Vol.61 (8), p.595-598
Main Authors: Salin, Alexey V., Musin, Rashid Z.
Format: Article
Language:English
Subjects:
Acrylamide
Acrylonitrile
Deuterium
deuterium‐labeled acrylamide
deuterium‐labeled acrylonitrile
electron‐deficient alkenes
Heavy water
hydration
Isotopes
Isotopic enrichment
Organic chemistry
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Summary:2‐d‐Acrylamide was synthesized via the 2‐step procedure starting from acrylonitrile and deuterium oxide. This procedure affords 2‐d‐acrylamide in 99.9% chemical purity and 98.4% isotopic enrichment. 2‐d‐Acrylamide was synthesized via the 2‐step procedure starting from acrylonitrile and deuterium oxide. This procedure affords 2‐d‐acrylamide in 99.9% chemical purity and 98.4% isotopic enrichment.
ISSN:0362-4803
1099-1344
DOI:10.1002/jlcr.3603