Nanofibers of cellulose bagasse from Agave tequilana Weber var. azul by electrospinning: preparation and characterization

• Published in: Carbohydrate polymers 2018-07, Vol.192, p.69-74
• Main Authors: Robles-García, Miguel Ángel, Del-Toro-Sánchez, Carmen Lizette, Márquez-Ríos, Enrique, Barrera-Rodríguez, Arturo, Aguilar, Jacobo, Aguilar, José A., Reynoso-Marín, Francisco Javier, Ceja, I., Dórame-Miranda, R., Rodríguez-Félix, Francisco
• Format: Article
• Language: English
• Subjects: Agave bagasse; Cellulose; Electrospinning; Nanofibers
• ISSN: 0144-8617; 1879-1344
• DOI: 10.1016/j.carbpol.2018.03.058

•Cellulose is extracted from agave bagasse.•Agave-bagasse cellulose nanofibers obtained by the electrospinning technique.•Nanofibers with useful properties to use in delivery systems and also reinforcing material. In this study, cellulose of bagasse from Agave tequilana Weber var. azul was extracted to elaborate nanofibers by the electrospinning technique. Fiber characterization was performed using Transmission Electron Microscopy (TEM), x-ray, Fournier Transform-InfraRed (FT-IR) spectroscopy, and thermal analysis by Differential Scanning Calorimetry-Thermogravimetric Analysis (DSC-TGA). Different diameters (ranging from 54.57 ± 0.02 to 171 ± 0.01 nm) of nanofibers were obtained. Cellulose nanofibers were analyzed by means of x-ray diffraction, where we observed a total loss of crystallinity in comparison with the cellulose, while FT-IR spectroscopy revealed that the hemicellulose and lignin present in the agave bagasse were removed. Thermal analysis showed that nanofibers exhibit enhanced thermal properties, and the zeta potential value (−32.5 mV) demonstrated moderate stability in the sample. In conclusion, the nanofibers obtained provide other alternatives-of-use for this agro-industrial residue and could have potential in various industrial applications, among these encapsulation of bioactive compounds and reinforcing material, to mention a few.