Exploiting 13C/14N solid-state NMR distance measurements to assign dihedral angles and locate neighboring molecules

The RESPDOR NMR method rapidly provides multiple 13C/14N distance measurements in natural abundance solids. In this study, 13C/14N RESPDOR information is shown, for the first time, to provide accurate molecular conformation and to locate non-bonded neighboring molecules.

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Bibliographic Details
Published in:Chemical communications (Cambridge, England) England), 2018-06, Vol.54 (49), p.6376-6379
Main Authors: Pope, Giovanna M, Hung, Ivan, Gan, Zhehong, Mobarak, Hani, Widmalm, Göran, Harper, James K
Format: Article
Language:English
Subjects:
Carbon 13
Chemical bonds
Distance measurement
Molecular chains
Molecular conformation
Nitrogen isotopes
NMR
Nuclear magnetic resonance
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Description
Summary:The RESPDOR NMR method rapidly provides multiple 13C/14N distance measurements in natural abundance solids. In this study, 13C/14N RESPDOR information is shown, for the first time, to provide accurate molecular conformation and to locate non-bonded neighboring molecules.
ISSN:1359-7345
1364-548X
DOI:10.1039/c8cc02597e