A low-cost home-built NMR using Halbach magnet

• Published in: Journal of magnetic resonance (1997) 2018-09, Vol.294, p.162-168
• Main Authors: Yu, Peng, Xu, Yajie, Wu, Zhongyi, Chang, Yan, Chen, Qiaoyan, Yang, Xiaodong
• Format: Article
• Language: English
• Subjects: Desktop NMR; Digital spectrometer; Halbach magnet
• ISSN: 1090-7807; 1096-0856
• DOI: 10.1016/j.jmr.2018.07.014

[Display omitted] •A low-cost desktop NMR system with 3-layer Halbach magnet was developed.•A wedge-shaped mechanical structure was designed for magnet rapid assembling.•A shimming manner with two magnetic blocks and steel pieces was proposed to reduce the cost and effort.•Digital modulation and demodulation were utilized with a single FPGA for better SNR and compact size. The objective of this work is to develop a low-cost compact desktop NMR system based on Halbach magnets with the advantages of small size and ability to generate relatively high field strength. Considering the cost of manufacturing and assembling the magnetic blocks, the system utilized a 3-layer Halbach magnet and a wedge-shaped mechanical structure, which was designed for magnet rapid assembling. The comparison between simulation and calculation results of the initial magnetic field strength distribution showed that design theory and practice were in accordance. The initial homogeneity was 576 ppm in a square with a length of 5 mm. After passive shimming with two magnetic blocks and steel pieces, the uniformity reached 120 ppm in the same area. We developed and tested a compact single board spectrometer with digital modulation and demodulation in order to enhance the system mobility and improve the SNR. A self-made probe was used to carry out experiments with the spectrometer, and the spectral width at half-height reached 20 ppm in a cylinder with a diameter of 1.5 mm and a length of 1 mm. Compact structure and low cost of the system will facilitate and extend the application of desktop NMR system.