BANGO SEA XLOC/HMBC-H2OBC: complete heteronuclear correlation within minutes from one NMR pulse sequence

Novel NMR experiments, BANGO SEA XLOC-H2OBC or BANGO HMBC-H2OBC, can deliver complete heteronuclear correlation maps on a time scale of minutes for small molecules. By way of example, it is demonstrated that all intra- and inter-residue 1 H and 13 C correlations and assignments of a trisaccharide ar...

Full description

Saved in:
Bibliographic Details
Published in:Chemical communications (Cambridge, England) England), 2019-10, Vol.55 (81), p.1228-12211
Main Authors: Nagy, Tamás Milán, Gyöngyösi, Tamás, Kövér, Katalin E, Sørensen, Ole W
Format: Article
Language:English
Subjects:
Correlation
NMR
Nuclear magnetic resonance
Oligosaccharides
Citations: Items that this one cites
Items that cite this one
Online Access:Get full text
Tags: Add Tag
No Tags, Be the first to tag this record!
Description
Summary:Novel NMR experiments, BANGO SEA XLOC-H2OBC or BANGO HMBC-H2OBC, can deliver complete heteronuclear correlation maps on a time scale of minutes for small molecules. By way of example, it is demonstrated that all intra- and inter-residue 1 H and 13 C correlations and assignments of a trisaccharide are obtained in 20 or 5 minutes of instrument time without or with 25% NUS, respectively. Novel NMR experiments, BANGO SEA XLOC-H2OBC or BANGO HMBC-H2OBC, deliver complete heteronuclear correlations and assignments on a time scale of minutes on small molecules.
ISSN:1359-7345
1364-548X
DOI:10.1039/c9cc06253j