13C CP-MAS solid-state n.m.r. spectra of stoving alkyd paints

A range of commercial stoving alkyd paints based on urea formaldehyde and melamine formaldehyde have been investigated using solid state n.m.r. techniques. The 1H relaxation times were measured to study the morphology of the materials, and to provide suitable values for the contact time used in the...

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Bibliographic Details
Published in:Polymer (Guilford) 1988-08, Vol.29 (8), p.1501-1506
Main Authors: Marshall, G.L., Cudby, M.E.A., Smith, K., Harris, R.K.
Format: Article
Language:English
Subjects:
Applied sciences
crosslinking
Exact sciences and technology
nuclear magnetic resonance
Organic polymers
Physicochemistry of polymers
pigmentation
Properties and characterization
solids
stoving alkyds
Structure, morphology and analysis
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Summary:A range of commercial stoving alkyd paints based on urea formaldehyde and melamine formaldehyde have been investigated using solid state n.m.r. techniques. The 1H relaxation times were measured to study the morphology of the materials, and to provide suitable values for the contact time used in the 13C cross-polarization experiments. 13C cross-polarization magic angle spinning spectra (CP-MAS) were recorded to examine the crosslinking mechanisms and to identify the repeating units present.
ISSN:0032-3861
1873-2291
DOI:10.1016/0032-3861(88)90316-3