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Green synthesis, characterization, application and functionality of nitrogen-doped MgO/graphene nanocomposite
A facile, feasible, and green synthesis via an electrochemical exfoliation process was applied to synthesize nitrogen-doped MgO/graphene nanocomposite (N-MgO/G). The N-MgO/G nanocomposite was characterized by several analytical techniques including X-ray photoelectron spectroscopy, X-ray powder diff...
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| Published in: | Environmental science and pollution research international 2021-06, Vol.28 (22), p.28014-28023 |
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| container_end_page | 28023 |
| container_issue | 22 |
| container_start_page | 28014 |
| container_title | Environmental science and pollution research international |
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| creator | Husein, Dalal Z. Uddin, Mohammad Kashif Ansari, Mohammad Omaish Ahmed, Sameh S. |
| description | A facile, feasible, and green synthesis via an electrochemical exfoliation process was applied to synthesize nitrogen-doped MgO/graphene nanocomposite (N-MgO/G). The N-MgO/G nanocomposite was characterized by several analytical techniques including X-ray photoelectron spectroscopy, X-ray powder diffraction, transmission electron microscopy, field emission scanning electron microscopy, energy-dispersive X-ray spectroscopy, selected area electron diffraction, and elemental mapping analysis. N-MgO/G nanocomposite was then applied to adsorb lead metal ions (Pb
2+
) from aqueous solutions. The N-MgO/G nanocomposite demonstrated a remarkably high Langmuir maximum adsorption capacity (294.12 mg/g) for Pb
2+
ions under the optimum experimental conditions at a pH of 5.13, time of 35 min, dose of 0.025 g, the concentration of 400 mg/L, and a temperature of 36 °C. Adsorption kinetics results fitted with a pseudo-second-order model and a thermodynamic study showed that Pb
2+
adsorption is an endothermic process. The practical application of N-MgO/G was also investigated to test its applicability in real water samples collected from different sources such as deionized water, tap water, wastewater, and river water. |
| doi_str_mv | 10.1007/s11356-021-12628-z |
| format | article |
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2+
) from aqueous solutions. The N-MgO/G nanocomposite demonstrated a remarkably high Langmuir maximum adsorption capacity (294.12 mg/g) for Pb
2+
ions under the optimum experimental conditions at a pH of 5.13, time of 35 min, dose of 0.025 g, the concentration of 400 mg/L, and a temperature of 36 °C. Adsorption kinetics results fitted with a pseudo-second-order model and a thermodynamic study showed that Pb
2+
adsorption is an endothermic process. The practical application of N-MgO/G was also investigated to test its applicability in real water samples collected from different sources such as deionized water, tap water, wastewater, and river water.</description><identifier>ISSN: 0944-1344</identifier><identifier>EISSN: 1614-7499</identifier><identifier>DOI: 10.1007/s11356-021-12628-z</identifier><identifier>PMID: 33527239</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Adsorption ; Aquatic Pollution ; Aqueous solutions ; Atmospheric Protection/Air Quality Control/Air Pollution ; Deionization ; Drinking water ; Earth and Environmental Science ; Ecotoxicology ; Electrochemistry ; Electron diffraction ; Electron microscopy ; Electrons ; Endothermic reactions ; endothermy ; energy-dispersive X-ray analysis ; Environment ; Environmental Chemistry ; Environmental Health ; Environmental science ; Field emission microscopy ; Graphene ; Lead ; Magnesium oxide ; Metal ions ; Microscopy ; Nanocomposites ; Nitrogen ; Photoelectron spectroscopy ; Photoelectrons ; Research Article ; river water ; Rivers ; Scanning electron microscopy ; Spectrum analysis ; Synthesis ; tap water ; temperature ; thermodynamics ; Transmission electron microscopy ; Waste Water Technology ; Wastewater ; Water analysis ; Water Management ; Water Pollution Control ; Water sampling ; X ray powder diffraction ; X-ray diffraction ; X-ray photoelectron spectroscopy ; X-ray spectroscopy</subject><ispartof>Environmental science and pollution research international, 2021-06, Vol.28 (22), p.28014-28023</ispartof><rights>The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2021</rights><rights>The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2021.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c445t-80c44245bf1c1275aba96cdf8aba75856a2b8ea229ffc271b07ca9bf1d0927ad3</citedby><cites>FETCH-LOGICAL-c445t-80c44245bf1c1275aba96cdf8aba75856a2b8ea229ffc271b07ca9bf1d0927ad3</cites><orcidid>0000-0002-3485-7227</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.proquest.com/docview/2533987313/fulltextPDF?pq-origsite=primo$$EPDF$$P50$$Gproquest$$H</linktopdf><linktohtml>$$Uhttps://www.proquest.com/docview/2533987313?pq-origsite=primo$$EHTML$$P50$$Gproquest$$H</linktohtml><link.rule.ids>314,776,780,11669,27903,27904,36039,36040,44342,74641</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/33527239$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Husein, Dalal Z.</creatorcontrib><creatorcontrib>Uddin, Mohammad Kashif</creatorcontrib><creatorcontrib>Ansari, Mohammad Omaish</creatorcontrib><creatorcontrib>Ahmed, Sameh S.</creatorcontrib><title>Green synthesis, characterization, application and functionality of nitrogen-doped MgO/graphene nanocomposite</title><title>Environmental science and pollution research international</title><addtitle>Environ Sci Pollut Res</addtitle><addtitle>Environ Sci Pollut Res Int</addtitle><description>A facile, feasible, and green synthesis via an electrochemical exfoliation process was applied to synthesize nitrogen-doped MgO/graphene nanocomposite (N-MgO/G). The N-MgO/G nanocomposite was characterized by several analytical techniques including X-ray photoelectron spectroscopy, X-ray powder diffraction, transmission electron microscopy, field emission scanning electron microscopy, energy-dispersive X-ray spectroscopy, selected area electron diffraction, and elemental mapping analysis. N-MgO/G nanocomposite was then applied to adsorb lead metal ions (Pb
2+
) from aqueous solutions. The N-MgO/G nanocomposite demonstrated a remarkably high Langmuir maximum adsorption capacity (294.12 mg/g) for Pb
2+
ions under the optimum experimental conditions at a pH of 5.13, time of 35 min, dose of 0.025 g, the concentration of 400 mg/L, and a temperature of 36 °C. Adsorption kinetics results fitted with a pseudo-second-order model and a thermodynamic study showed that Pb
2+
adsorption is an endothermic process. The practical application of N-MgO/G was also investigated to test its applicability in real water samples collected from different sources such as deionized water, tap water, wastewater, and river water.</description><subject>Adsorption</subject><subject>Aquatic Pollution</subject><subject>Aqueous solutions</subject><subject>Atmospheric Protection/Air Quality Control/Air Pollution</subject><subject>Deionization</subject><subject>Drinking water</subject><subject>Earth and Environmental Science</subject><subject>Ecotoxicology</subject><subject>Electrochemistry</subject><subject>Electron diffraction</subject><subject>Electron microscopy</subject><subject>Electrons</subject><subject>Endothermic reactions</subject><subject>endothermy</subject><subject>energy-dispersive X-ray analysis</subject><subject>Environment</subject><subject>Environmental Chemistry</subject><subject>Environmental Health</subject><subject>Environmental science</subject><subject>Field emission microscopy</subject><subject>Graphene</subject><subject>Lead</subject><subject>Magnesium oxide</subject><subject>Metal ions</subject><subject>Microscopy</subject><subject>Nanocomposites</subject><subject>Nitrogen</subject><subject>Photoelectron spectroscopy</subject><subject>Photoelectrons</subject><subject>Research Article</subject><subject>river water</subject><subject>Rivers</subject><subject>Scanning electron microscopy</subject><subject>Spectrum analysis</subject><subject>Synthesis</subject><subject>tap water</subject><subject>temperature</subject><subject>thermodynamics</subject><subject>Transmission electron microscopy</subject><subject>Waste Water Technology</subject><subject>Wastewater</subject><subject>Water analysis</subject><subject>Water Management</subject><subject>Water Pollution Control</subject><subject>Water sampling</subject><subject>X ray powder diffraction</subject><subject>X-ray diffraction</subject><subject>X-ray photoelectron spectroscopy</subject><subject>X-ray 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Z.</au><au>Uddin, Mohammad Kashif</au><au>Ansari, Mohammad Omaish</au><au>Ahmed, Sameh S.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Green synthesis, characterization, application and functionality of nitrogen-doped MgO/graphene nanocomposite</atitle><jtitle>Environmental science and pollution research international</jtitle><stitle>Environ Sci Pollut Res</stitle><addtitle>Environ Sci Pollut Res Int</addtitle><date>2021-06-01</date><risdate>2021</risdate><volume>28</volume><issue>22</issue><spage>28014</spage><epage>28023</epage><pages>28014-28023</pages><issn>0944-1344</issn><eissn>1614-7499</eissn><abstract>A facile, feasible, and green synthesis via an electrochemical exfoliation process was applied to synthesize nitrogen-doped MgO/graphene nanocomposite (N-MgO/G). The N-MgO/G nanocomposite was characterized by several analytical techniques including X-ray photoelectron spectroscopy, X-ray powder diffraction, transmission electron microscopy, field emission scanning electron microscopy, energy-dispersive X-ray spectroscopy, selected area electron diffraction, and elemental mapping analysis. N-MgO/G nanocomposite was then applied to adsorb lead metal ions (Pb
2+
) from aqueous solutions. The N-MgO/G nanocomposite demonstrated a remarkably high Langmuir maximum adsorption capacity (294.12 mg/g) for Pb
2+
ions under the optimum experimental conditions at a pH of 5.13, time of 35 min, dose of 0.025 g, the concentration of 400 mg/L, and a temperature of 36 °C. Adsorption kinetics results fitted with a pseudo-second-order model and a thermodynamic study showed that Pb
2+
adsorption is an endothermic process. The practical application of N-MgO/G was also investigated to test its applicability in real water samples collected from different sources such as deionized water, tap water, wastewater, and river water.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><pmid>33527239</pmid><doi>10.1007/s11356-021-12628-z</doi><tpages>10</tpages><orcidid>https://orcid.org/0000-0002-3485-7227</orcidid></addata></record> |
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| subjects | Adsorption Aquatic Pollution Aqueous solutions Atmospheric Protection/Air Quality Control/Air Pollution Deionization Drinking water Earth and Environmental Science Ecotoxicology Electrochemistry Electron diffraction Electron microscopy Electrons Endothermic reactions endothermy energy-dispersive X-ray analysis Environment Environmental Chemistry Environmental Health Environmental science Field emission microscopy Graphene Lead Magnesium oxide Metal ions Microscopy Nanocomposites Nitrogen Photoelectron spectroscopy Photoelectrons Research Article river water Rivers Scanning electron microscopy Spectrum analysis Synthesis tap water temperature thermodynamics Transmission electron microscopy Waste Water Technology Wastewater Water analysis Water Management Water Pollution Control Water sampling X ray powder diffraction X-ray diffraction X-ray photoelectron spectroscopy X-ray spectroscopy |
| title | Green synthesis, characterization, application and functionality of nitrogen-doped MgO/graphene nanocomposite |
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