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Synthesis and characterization of MTiO3 (M = Mg, Ca, Sr, Ba) sol-gel

Multiple oxide titanates were prepared via the sol-gel method by the reaction of an alcoholic solution of titanium n-butoxide, Ti(OC4H9)4, with nitrate solutions, M(NO3)2 (M = Mg, Ca, Sr, Ba) at room temperature. The amorphous gels so obtained under acidic conditions were calcined at temperatures be...

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Published in:Journal of materials chemistry 1995, Vol.5 (3), p.509-512
Main Authors: MORENO, J, DOMINGUEZ, J. M, MONTOYA, A, VICENTE, L, VIVEROS, T
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Language:English
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container_title Journal of materials chemistry
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creator MORENO, J
DOMINGUEZ, J. M
MONTOYA, A
VICENTE, L
VIVEROS, T
description Multiple oxide titanates were prepared via the sol-gel method by the reaction of an alcoholic solution of titanium n-butoxide, Ti(OC4H9)4, with nitrate solutions, M(NO3)2 (M = Mg, Ca, Sr, Ba) at room temperature. The amorphous gels so obtained under acidic conditions were calcined at temperatures between 700 and 900 C to obtain high purity crystalline MTiO3 powders. The samples were characterised by powder XRD, SEM, EDS, TG, DTA and BET surface area measurements. The stability and large surface area obtained for the Sr and Ba compounds make then suitable for use as catalyst supports. 20 refs.
doi_str_mv 10.1039/JM9950500509
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source Royal Society of Chemistry: Jisc Collections: Journals Archive 1841-2007 (2019-2023)
subjects Chemistry
Colloidal state and disperse state
Exact sciences and technology
General and physical chemistry
Powders
title Synthesis and characterization of MTiO3 (M = Mg, Ca, Sr, Ba) sol-gel
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