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Synthesis and characterization of MTiO3 (M = Mg, Ca, Sr, Ba) sol-gel
Multiple oxide titanates were prepared via the sol-gel method by the reaction of an alcoholic solution of titanium n-butoxide, Ti(OC4H9)4, with nitrate solutions, M(NO3)2 (M = Mg, Ca, Sr, Ba) at room temperature. The amorphous gels so obtained under acidic conditions were calcined at temperatures be...
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Published in: | Journal of materials chemistry 1995, Vol.5 (3), p.509-512 |
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container_issue | 3 |
container_start_page | 509 |
container_title | Journal of materials chemistry |
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creator | MORENO, J DOMINGUEZ, J. M MONTOYA, A VICENTE, L VIVEROS, T |
description | Multiple oxide titanates were prepared via the sol-gel method by the reaction of an alcoholic solution of titanium n-butoxide, Ti(OC4H9)4, with nitrate solutions, M(NO3)2 (M = Mg, Ca, Sr, Ba) at room temperature. The amorphous gels so obtained under acidic conditions were calcined at temperatures between 700 and 900 C to obtain high purity crystalline MTiO3 powders. The samples were characterised by powder XRD, SEM, EDS, TG, DTA and BET surface area measurements. The stability and large surface area obtained for the Sr and Ba compounds make then suitable for use as catalyst supports. 20 refs. |
doi_str_mv | 10.1039/JM9950500509 |
format | article |
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source | Royal Society of Chemistry: Jisc Collections: Journals Archive 1841-2007 (2019-2023) |
subjects | Chemistry Colloidal state and disperse state Exact sciences and technology General and physical chemistry Powders |
title | Synthesis and characterization of MTiO3 (M = Mg, Ca, Sr, Ba) sol-gel |
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