Cure monitoring of the liquid composite molding process using fiber optic sensors

• Published in: Polymer composites 1997-02, Vol.18 (1), p.133-150
• Main Authors: Woerdeman, Dara L., Spoerre, Julie K., Flynn, Kathleen M., Parnas, Richard S.
• Format: Article
• Language: English
• Subjects: Applied sciences; Composites; Exact sciences and technology; Forms of application and semi-finished materials; Polymer industry, paints, wood; Technology of polymers
• ISSN: 0272-8397; 1548-0569
• DOI: 10.1002/pc.10268

Fluorescence has been demonstrated to be an accurate tool for monitoring resin cure. It is measured using an evanescent wave fiber‐optic sensor. An economical optical fiber sensor has been developed with a refractive index greater than 1.6, permitting evanescent wave monitoring of epoxy resins. The fluorescence wave‐length‐shift, which has been correlated with monomer conversion, is monitored during the liquid molding process. Unidirectional glass fabrics with volume fractions from 40% to 60% were injected with epoxy resin at a variety of driving pressures and cured at several temperatures. Several composite parts were fabricated to test the effects of vacuum pressure, injection rate, cure temperature, and fiber fraction on the performance of the sensor. The sensitivity of the evanescent wave fluorescence sensor to the condition of the resin system was also examined. The sets of resin/hardener samples were subjected to rigorous chemical analysis to determine the extent of their differences.