Weibull statistical analysis of flexure breaking performance for alumina ceramic disks sintered by solar radiation heating

• Published in: Ceramics international 2000-03, Vol.26 (2), p.203-206
• Main Authors: Cruz Fernandes, Jorge, Amaral, Pedro Miguel, Guerra Rosa, Luı́s, Shohoji, Nobumitsu
• Format: Article
• Language: English
• Subjects: Alumina ceramics; Applied sciences; Building materials. Ceramics. Glasses; Ceramic industries; Chemical industry and chemicals; Equibiaxial strength; Exact sciences and technology; Miscellaneous; Solar furnace; Technical ceramics; Weibull statistics
• ISSN: 0272-8842; 1873-3956
• DOI: 10.1016/S0272-8842(99)00041-3

Densified alumina ceramic disk specimens were prepared through sintering compacted alumina powders by concentrated solar beam in inert Ar gas atmosphere and their flexure breaking behaviour was evaluated by the ring-on-ring jig test under application of equibiaxial stress. Slope m of Weibull plot for MOR (modulus of rupture) values of these specimens was comparable to that of the reference alumina disk specimens prepared by sintering in an electric furnace under comparable conditions (1600°C for 30 min) whereas mean MOR level of the former was slightly lower than that of the latter. Thus, the failure mechanism of the specimens sintered by solar radiation heating and that of the specimens sintered in the electric furnace were concluded to be practically indistinguishable. This evidence guarantees that alumina ceramic sintered bodies, with quality comparable to those obtained through traditional sintering process, can be prepared by solar heating in spite of quite fast rate of heating and cooling realised in the solar furnace.