Fast synthesis of YBa2Cu3Oz superconductor at low temperatures of its orthorhombic modification existence using mechanically activated and densified two-powder precursors

The possibility of developing a fast (10-30 min) and low-temperature (500-600 C) synthesis of YBa2Cu3Oz superconductor with a Tc up to 90 K appearing immediately after preparation is discussed. Mechanically activated and densified two-powder precursors have reproducibly yielded 80-90% XRD-pure YBa2C...

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Published in:Physica. C, Superconductivity Superconductivity, 2001-01, Vol.349 (3-4), p.278-288
Main Authors: Goodilin, E.A, Pyoryshkov, D, Knot’ko, A.V, Lennikov, V.V, Oleynikov, N.N, Tretyakov, Yu.D
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description The possibility of developing a fast (10-30 min) and low-temperature (500-600 C) synthesis of YBa2Cu3Oz superconductor with a Tc up to 90 K appearing immediately after preparation is discussed. Mechanically activated and densified two-powder precursors have reproducibly yielded 80-90% XRD-pure YBa2Cu3Oz phase when using internal oxygenation of soft-chemistry produced Cu2O by YBa2O3.5 (containing BaO2) in their mixture (Y:Ba:Cu=1:2:3) mechanically activated in a planetary mill and warmly compacted at 250 C into a dense pellet. Such advantages allowed authors to obtain trial samples of Al-sheathed chemistry tapes with the YBa2Cu3Oz core. 20 refs.
doi_str_mv 10.1016/S0921-4534(00)01539-2
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title Fast synthesis of YBa2Cu3Oz superconductor at low temperatures of its orthorhombic modification existence using mechanically activated and densified two-powder precursors
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