Impact of pretreatments with ethanol and freezing on drying slice papaya: drying performance and kinetic of ultrasound‐assisted extraction of phenolics compounds

• Published in: Journal of the science of food and agriculture 2023-01, Vol.103 (1), p.125-134
• Main Authors: Santos, Newton Carlos, Almeida, Raphael Lucas Jacinto, Silva, Gabriel Monteiro, Alcântara Silva, Vírgínia Mirtes, Alcântara Ribeiro, Victor Herbert, Oliveira Brito, Ana Carla, Sousa Rodrigues, Larissa Monique, Santos, Rebeca Morais Silva, Saraiva, Maria Monique Tavares
• Format: Article
• Language: English
• Subjects: bioactives; Boundary conditions; Drying; Ethanol; Experimental data; Freezing; Heat conductivity; Heat transfer; Kinetics; Moisture content; Papayas; Phenolic compounds; Phenols; Pretreatment; Specific heat; Thermal conductivity; Thermophysical models; Thermophysical properties; Ultrasonic imaging; Ultrasound; Water content
• ISSN: 0022-5142; 1097-0010
• DOI: 10.1002/jsfa.12119

Background Pretreatments of drying can represent an alternative to minimize the negative aspect process on the dry samples. Thus, the influence of ethanol (ET) and freezing (FG) as drying pretreatments was analyzed for slices of papaya. The slices (5 mm) were submitted for drying kinetics (60 °C and 1.5 m s−1). Drying kinetics experimental data were fitted using Page's model and a diffusive model with boundary condition of types I and III. Also the thermophysical properties (thermal conductivity and specific heat) were determined and finally, the kinetics of ultrasound‐assisted (40 kHz and 132 W) extraction of total phenolic compounds (TPCs) were realized. Results The combined method (ET + FG) was more efficient in reducing the drying time of papaya slices (48%) and the model 2 simulating the boundary condition of the third type (type III) showed the best fit to the experimental data. Effective diffusivity and convective coefficient were higher for ET + FG, where the maximum reduction in water content was 91% compared to fresh slices. The pretreatments did not influence the thermal conductivity, however, they were significant in the specific heat and in the extraction of TPCs, being higher in the time of 180 min. Conclusion It was confirmed in the results presented that the combined pretreatment ET + FG is the most viable for drying papaya slices. Furthermore, it was found to be the most efficient in minimizing the loss of TPCs. Therefore, this pretreatment has great potential for application in the development of high value‐added foods. © 2022 Society of Chemical Industry.