Changes in surface stress at the liquid/solid interface measured with a microcantilever

The bending of microfabricated silicon nitride cantilevers was used to determine surface stress changes at solid–liquid interfaces. The radius of curvature of the bent cantilever is directly proportional to changes in the differential surface stress between its opposite sides. To demonstrate the pos...

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Published in:Electrochimica acta 2000-11, Vol.46 (2), p.157-163
Main Authors: Raiteri, R., Butt, H.-J., Grattarola, M.
Format: Article
Language:English
Subjects:
Atomic force microscopy
Biosensors
Cantilevers
Chemistry
Exact sciences and technology
General and physical chemistry
Solid-liquid interface
Surface energy of solids
Surface physical chemistry
Surface stress
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description The bending of microfabricated silicon nitride cantilevers was used to determine surface stress changes at solid–liquid interfaces. The radius of curvature of the bent cantilever is directly proportional to changes in the differential surface stress between its opposite sides. To demonstrate the possibilities and limitations of the technique, cantilevers coated on both sides with gold and densely packed monolayers of different thiols were put in a constant flow of aqueous electrolyte solution and the deflection was measured using a optical lever technique. Changes in the surface stress for the different thiol monolayers due to specific proton adsorption are presented. Possible applications and improvements of this technique are discussed.
doi_str_mv 10.1016/S0013-4686(00)00569-7
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subjects Atomic force microscopy
Biosensors
Cantilevers
Chemistry
Exact sciences and technology
General and physical chemistry
Solid-liquid interface
Surface energy of solids
Surface physical chemistry
Surface stress
title Changes in surface stress at the liquid/solid interface measured with a microcantilever
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