Impedance spectroscopy of a soda-lime glass during sintering

Impedance spectroscopy measurements were carried out during sintering of a compact of spherical soda-lime-silica glass particles (SiO 2 72.5 wt.%, MgO 3.3%, CaO 9.8%, Na 2O 13.7%, Al 2O 3 0.4%, Fe 2O 3 0.2%, K 2O 0.1%). Impedance diagrams were obtained in the 5 Hz–13 MHz frequency range at different...

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Published in:Materials science & engineering. A, Structural materials : properties, microstructure and processing Structural materials : properties, microstructure and processing, 2003-07, Vol.352 (1), p.232-239
Main Authors: Muccillo, R, Muccillo, E.N.S, França, Y.V, Fredericci, C, Prado, M.O, Zanotto, E.D
Format: Article
Language:English
Subjects:
Applied sciences
Building materials. Ceramics. Glasses
Chemical industry and chemicals
Exact sciences and technology
Glass sintering
Glasses
Impedance spectroscopy
Sintering modelling
Soda-lime glass
Structure, analysis, properties
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cited_by cdi_FETCH-LOGICAL-c368t-db930825863910512f8a9570397f6418768b739889ca806413ede34245c656fb3
cites cdi_FETCH-LOGICAL-c368t-db930825863910512f8a9570397f6418768b739889ca806413ede34245c656fb3
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container_title Materials science & engineering. A, Structural materials : properties, microstructure and processing
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creator Muccillo, R
Muccillo, E.N.S
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Fredericci, C
Prado, M.O
Zanotto, E.D
description Impedance spectroscopy measurements were carried out during sintering of a compact of spherical soda-lime-silica glass particles (SiO 2 72.5 wt.%, MgO 3.3%, CaO 9.8%, Na 2O 13.7%, Al 2O 3 0.4%, Fe 2O 3 0.2%, K 2O 0.1%). Impedance diagrams were obtained in the 5 Hz–13 MHz frequency range at different temperatures during room temperature −943 K–room temperature cycles. The glass transition temperature evaluated using the total electrical resistance of the glass specimens agrees with the value obtained by differential scanning calorimetry. The electrical conductance increases with the time that the glass is maintained at the sintering temperature suggesting that this behavior may be used to the study of sintering kinetics. A model to gather information on the sintering kinetics from conductivity data was developed and tested.
doi_str_mv 10.1016/S0921-5093(02)00893-6
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1873-4936
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source ScienceDirect Journals
subjects Applied sciences
Building materials. Ceramics. Glasses
Chemical industry and chemicals
Exact sciences and technology
Glass sintering
Glasses
Impedance spectroscopy
Sintering modelling
Soda-lime glass
Structure, analysis, properties
title Impedance spectroscopy of a soda-lime glass during sintering
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