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Channel-containing structures generated from linear coordination polymer chains containing N , N ′ -bidentate ligands and Cu–Cu dimetal units
Four new one-dimensional coordination polymers containing the dimetal cluster Cu 2(OAc) 4 have been synthesized by reacting Cu(OAc) 2 ⋅ H 2O with two different N , N ′ -bidentate ligands. Reaction of the flexible ligand, 1,2-bis(4-pyridyl)ethane ( L 1), with the copper starting material produced two...
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| Published in: | Solid state sciences 2005-09, Vol.7 (9), p.1083-1095 |
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| Main Authors: | , , , , , |
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| Language: | English |
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| creator | Goforth, Andrea M. Gerth, Kathrine Smith, Mark D. Shotwell, Sandra Bunz, Uwe H.F. zur Loye, Hans-Conrad |
| description | Four new one-dimensional coordination polymers containing the dimetal cluster Cu
2(OAc)
4 have been synthesized by reacting Cu(OAc)
2
⋅
H
2O with two different
N
,
N
′
-bidentate ligands. Reaction of the flexible ligand, 1,2-bis(4-pyridyl)ethane (
L
1), with the copper starting material produced two, co-crystallizing coordination polymers:
catena-Poly[Cu
2(OAc)
4(
L
1)]
⋅
2H
2O (
1) and
catena-Poly[Cu
2(OAc)
4(
L
1)]. In the solid state,
1 (monoclinic, C2/c,
a
=
24.9471
(
17
)
Å
,
b
=
13.3539
(
9
)
Å
,
c
=
8.8050
(
6
)
Å
,
β
=
93.6480
(
10
)
°
,
V
=
2927.4
(
3
)
Å
3
,
Z
=
4
) features linear chains which are organized into layers. These layers stack along the crystallographic
c-axis forming small hexagonal channels occupied by the solvent of crystallization. Compound
2 (triclinic, P-1,
a
=
7.6263
(
6
)
Å
,
b
=
8.5283
(
6
)
Å
,
c
=
9.8633
(
6
)
Å
,
α
=
74.1070
(
10
)
°
,
β
=
68.2160
(
10
)
°
,
γ
=
74.0090
(
10
)
°
,
V
=
561.96
(
7
)
Å
3
,
Z
=
1
) also features linear chains of the coordination polymer, but differs from
1 in that the chains are packed so as to leave no significant channels. Reaction of the rigid ligand, 1,4-bis(4-pyridyl)buta-1,3-diyne (
L
2), with the copper starting material also afforded two co-crystallizing coordination polymers:
catena-Poly[Cu
2(OAc)
4(
L
2)] (
3) and
catena-Poly[Cu
2(OAc)
4(
L
2)]
⋅
solvents (
4).
3 (monoclinic, P2
1/m,
a
=
9.8065
(
9
)
Å
,
b
=
12.3793
(
11
)
Å
,
c
=
9.9408
(
9
)
Å
,
β
=
107.6009
(
17
)
°
,
V
=
1150.29
(
18
)
Å
3
,
Z
=
2
), like
2, features linear chains and contains no significant solvent accessible void space.
4 (monoclinic, C2/c,
a
=
28.9810
(
16
)
Å
,
b
=
12.9301
(
7
)
Å
,
c
=
8.6954
(
5
)
Å
,
β
=
98.8010
(
10
)
°
,
V
=
3220.0
(
3
)
Å
3
,
Z
=
4
) also consists of linear chains of the coordination polymer. However, the overall topology of
4 is identical to that of
1, with the generated hexagonal channels containing crystallographically unidentifiable solvents of crystallization. Compounds
1 and
2 and compounds
3 and
4 are pairs of polymorphic coordination polymers neglecting the solvents of crystallization in
1 and
4. The compounds, which represent four new examples of coordination polymers containing dimetal units, have been characterized by IR, elemental analysis, and thermogravimetric analysis in addition to X-ray crystallography. |
| doi_str_mv | 10.1016/j.solidstatesciences.2005.03.006 |
| format | article |
| fullrecord | <record><control><sourceid>proquest_pasca</sourceid><recordid>TN_cdi_proquest_miscellaneous_28120553</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><els_id>S1293255805001299</els_id><sourcerecordid>28120553</sourcerecordid><originalsourceid>FETCH-LOGICAL-e283t-5da4624ff935917a4609f776710e9ad572b424c2a9de6bd3676078aacdf48fc33</originalsourceid><addsrcrecordid>eNplkc9u1DAQxi0EEmXLO_gC4kCC_8RxckQRhVYVvbRny2tPtl459mI7SL31FRBvwiP1SfCqe0DiMDMe65vPI_8Q-kBJSwntP-3bHL2zuegC2TgIBnLLCBEt4S0h_Qt0RgfJG04G8bKe2cgbJsTwGr3JeU-qopfdGfo13esQwDcmhqJdcGGHc0mrKWuCjHcQINUXLJ5TXLB3AXTCJsZkXdDFxYAP0T8sUC_v63jG__h8xx9rPD3-wc3WWQjHVavFTgebcU14Wp8ef08rtm6Boj1egyv5HL2atc_w9lQ36O7iy-30rbm--Xo5fb5ugA28NMLqrmfdPI9cjFTWhoyzlL2kBEZthWTbjnWG6dFCv7W8lz2Rg9bGzt0wG8436P2z7yHFHyvkohaXDXivA8Q1KzZQRoQ4Ct-dhDob7eekg3FZHZJbdHpQVFLBRf3qDbp61kHd-qeDpE5crEtgirLRKUrUkZ7aq__pqSM9RbiqbPhfPN6ang</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>28120553</pqid></control><display><type>article</type><title>Channel-containing structures generated from linear coordination polymer chains containing N , N ′ -bidentate ligands and Cu–Cu dimetal units</title><source>ScienceDirect Journals</source><creator>Goforth, Andrea M. ; Gerth, Kathrine ; Smith, Mark D. ; Shotwell, Sandra ; Bunz, Uwe H.F. ; zur Loye, Hans-Conrad</creator><creatorcontrib>Goforth, Andrea M. ; Gerth, Kathrine ; Smith, Mark D. ; Shotwell, Sandra ; Bunz, Uwe H.F. ; zur Loye, Hans-Conrad</creatorcontrib><description>Four new one-dimensional coordination polymers containing the dimetal cluster Cu
2(OAc)
4 have been synthesized by reacting Cu(OAc)
2
⋅
H
2O with two different
N
,
N
′
-bidentate ligands. Reaction of the flexible ligand, 1,2-bis(4-pyridyl)ethane (
L
1), with the copper starting material produced two, co-crystallizing coordination polymers:
catena-Poly[Cu
2(OAc)
4(
L
1)]
⋅
2H
2O (
1) and
catena-Poly[Cu
2(OAc)
4(
L
1)]. In the solid state,
1 (monoclinic, C2/c,
a
=
24.9471
(
17
)
Å
,
b
=
13.3539
(
9
)
Å
,
c
=
8.8050
(
6
)
Å
,
β
=
93.6480
(
10
)
°
,
V
=
2927.4
(
3
)
Å
3
,
Z
=
4
) features linear chains which are organized into layers. These layers stack along the crystallographic
c-axis forming small hexagonal channels occupied by the solvent of crystallization. Compound
2 (triclinic, P-1,
a
=
7.6263
(
6
)
Å
,
b
=
8.5283
(
6
)
Å
,
c
=
9.8633
(
6
)
Å
,
α
=
74.1070
(
10
)
°
,
β
=
68.2160
(
10
)
°
,
γ
=
74.0090
(
10
)
°
,
V
=
561.96
(
7
)
Å
3
,
Z
=
1
) also features linear chains of the coordination polymer, but differs from
1 in that the chains are packed so as to leave no significant channels. Reaction of the rigid ligand, 1,4-bis(4-pyridyl)buta-1,3-diyne (
L
2), with the copper starting material also afforded two co-crystallizing coordination polymers:
catena-Poly[Cu
2(OAc)
4(
L
2)] (
3) and
catena-Poly[Cu
2(OAc)
4(
L
2)]
⋅
solvents (
4).
3 (monoclinic, P2
1/m,
a
=
9.8065
(
9
)
Å
,
b
=
12.3793
(
11
)
Å
,
c
=
9.9408
(
9
)
Å
,
β
=
107.6009
(
17
)
°
,
V
=
1150.29
(
18
)
Å
3
,
Z
=
2
), like
2, features linear chains and contains no significant solvent accessible void space.
4 (monoclinic, C2/c,
a
=
28.9810
(
16
)
Å
,
b
=
12.9301
(
7
)
Å
,
c
=
8.6954
(
5
)
Å
,
β
=
98.8010
(
10
)
°
,
V
=
3220.0
(
3
)
Å
3
,
Z
=
4
) also consists of linear chains of the coordination polymer. However, the overall topology of
4 is identical to that of
1, with the generated hexagonal channels containing crystallographically unidentifiable solvents of crystallization. Compounds
1 and
2 and compounds
3 and
4 are pairs of polymorphic coordination polymers neglecting the solvents of crystallization in
1 and
4. The compounds, which represent four new examples of coordination polymers containing dimetal units, have been characterized by IR, elemental analysis, and thermogravimetric analysis in addition to X-ray crystallography.</description><identifier>ISSN: 1293-2558</identifier><identifier>EISSN: 1873-3085</identifier><identifier>DOI: 10.1016/j.solidstatesciences.2005.03.006</identifier><language>eng</language><publisher>Paris: Elsevier Masson SAS</publisher><subject>[formula omitted]-bidentate ligands ; Condensed matter: structure, mechanical and thermal properties ; Coordination polymers ; Copper dimers ; Crystalline state (including molecular motions in solids) ; Dimetal building blocks ; Exact sciences and technology ; Physics ; Polymorphic coordination polymers ; Structure of solids and liquids; crystallography ; Structure of specific crystalline solids ; Theory of crystal structure, crystal symmetry; calculations and modeling ; Twinned crystal</subject><ispartof>Solid state sciences, 2005-09, Vol.7 (9), p.1083-1095</ispartof><rights>2005 Elsevier SAS</rights><rights>2006 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,777,781,27905,27906</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=17153587$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Goforth, Andrea M.</creatorcontrib><creatorcontrib>Gerth, Kathrine</creatorcontrib><creatorcontrib>Smith, Mark D.</creatorcontrib><creatorcontrib>Shotwell, Sandra</creatorcontrib><creatorcontrib>Bunz, Uwe H.F.</creatorcontrib><creatorcontrib>zur Loye, Hans-Conrad</creatorcontrib><title>Channel-containing structures generated from linear coordination polymer chains containing N , N ′ -bidentate ligands and Cu–Cu dimetal units</title><title>Solid state sciences</title><description>Four new one-dimensional coordination polymers containing the dimetal cluster Cu
2(OAc)
4 have been synthesized by reacting Cu(OAc)
2
⋅
H
2O with two different
N
,
N
′
-bidentate ligands. Reaction of the flexible ligand, 1,2-bis(4-pyridyl)ethane (
L
1), with the copper starting material produced two, co-crystallizing coordination polymers:
catena-Poly[Cu
2(OAc)
4(
L
1)]
⋅
2H
2O (
1) and
catena-Poly[Cu
2(OAc)
4(
L
1)]. In the solid state,
1 (monoclinic, C2/c,
a
=
24.9471
(
17
)
Å
,
b
=
13.3539
(
9
)
Å
,
c
=
8.8050
(
6
)
Å
,
β
=
93.6480
(
10
)
°
,
V
=
2927.4
(
3
)
Å
3
,
Z
=
4
) features linear chains which are organized into layers. These layers stack along the crystallographic
c-axis forming small hexagonal channels occupied by the solvent of crystallization. Compound
2 (triclinic, P-1,
a
=
7.6263
(
6
)
Å
,
b
=
8.5283
(
6
)
Å
,
c
=
9.8633
(
6
)
Å
,
α
=
74.1070
(
10
)
°
,
β
=
68.2160
(
10
)
°
,
γ
=
74.0090
(
10
)
°
,
V
=
561.96
(
7
)
Å
3
,
Z
=
1
) also features linear chains of the coordination polymer, but differs from
1 in that the chains are packed so as to leave no significant channels. Reaction of the rigid ligand, 1,4-bis(4-pyridyl)buta-1,3-diyne (
L
2), with the copper starting material also afforded two co-crystallizing coordination polymers:
catena-Poly[Cu
2(OAc)
4(
L
2)] (
3) and
catena-Poly[Cu
2(OAc)
4(
L
2)]
⋅
solvents (
4).
3 (monoclinic, P2
1/m,
a
=
9.8065
(
9
)
Å
,
b
=
12.3793
(
11
)
Å
,
c
=
9.9408
(
9
)
Å
,
β
=
107.6009
(
17
)
°
,
V
=
1150.29
(
18
)
Å
3
,
Z
=
2
), like
2, features linear chains and contains no significant solvent accessible void space.
4 (monoclinic, C2/c,
a
=
28.9810
(
16
)
Å
,
b
=
12.9301
(
7
)
Å
,
c
=
8.6954
(
5
)
Å
,
β
=
98.8010
(
10
)
°
,
V
=
3220.0
(
3
)
Å
3
,
Z
=
4
) also consists of linear chains of the coordination polymer. However, the overall topology of
4 is identical to that of
1, with the generated hexagonal channels containing crystallographically unidentifiable solvents of crystallization. Compounds
1 and
2 and compounds
3 and
4 are pairs of polymorphic coordination polymers neglecting the solvents of crystallization in
1 and
4. The compounds, which represent four new examples of coordination polymers containing dimetal units, have been characterized by IR, elemental analysis, and thermogravimetric analysis in addition to X-ray crystallography.</description><subject>[formula omitted]-bidentate ligands</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Coordination polymers</subject><subject>Copper dimers</subject><subject>Crystalline state (including molecular motions in solids)</subject><subject>Dimetal building blocks</subject><subject>Exact sciences and technology</subject><subject>Physics</subject><subject>Polymorphic coordination polymers</subject><subject>Structure of solids and liquids; crystallography</subject><subject>Structure of specific crystalline solids</subject><subject>Theory of crystal structure, crystal symmetry; calculations and modeling</subject><subject>Twinned crystal</subject><issn>1293-2558</issn><issn>1873-3085</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2005</creationdate><recordtype>article</recordtype><recordid>eNplkc9u1DAQxi0EEmXLO_gC4kCC_8RxckQRhVYVvbRny2tPtl459mI7SL31FRBvwiP1SfCqe0DiMDMe65vPI_8Q-kBJSwntP-3bHL2zuegC2TgIBnLLCBEt4S0h_Qt0RgfJG04G8bKe2cgbJsTwGr3JeU-qopfdGfo13esQwDcmhqJdcGGHc0mrKWuCjHcQINUXLJ5TXLB3AXTCJsZkXdDFxYAP0T8sUC_v63jG__h8xx9rPD3-wc3WWQjHVavFTgebcU14Wp8ef08rtm6Boj1egyv5HL2atc_w9lQ36O7iy-30rbm--Xo5fb5ugA28NMLqrmfdPI9cjFTWhoyzlL2kBEZthWTbjnWG6dFCv7W8lz2Rg9bGzt0wG8436P2z7yHFHyvkohaXDXivA8Q1KzZQRoQ4Ct-dhDob7eekg3FZHZJbdHpQVFLBRf3qDbp61kHd-qeDpE5crEtgirLRKUrUkZ7aq__pqSM9RbiqbPhfPN6ang</recordid><startdate>20050901</startdate><enddate>20050901</enddate><creator>Goforth, Andrea M.</creator><creator>Gerth, Kathrine</creator><creator>Smith, Mark D.</creator><creator>Shotwell, Sandra</creator><creator>Bunz, Uwe H.F.</creator><creator>zur Loye, Hans-Conrad</creator><general>Elsevier Masson SAS</general><general>Elsevier</general><scope>IQODW</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20050901</creationdate><title>Channel-containing structures generated from linear coordination polymer chains containing N , N ′ -bidentate ligands and Cu–Cu dimetal units</title><author>Goforth, Andrea M. ; Gerth, Kathrine ; Smith, Mark D. ; Shotwell, Sandra ; Bunz, Uwe H.F. ; zur Loye, Hans-Conrad</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-e283t-5da4624ff935917a4609f776710e9ad572b424c2a9de6bd3676078aacdf48fc33</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2005</creationdate><topic>[formula omitted]-bidentate ligands</topic><topic>Condensed matter: structure, mechanical and thermal properties</topic><topic>Coordination polymers</topic><topic>Copper dimers</topic><topic>Crystalline state (including molecular motions in solids)</topic><topic>Dimetal building blocks</topic><topic>Exact sciences and technology</topic><topic>Physics</topic><topic>Polymorphic coordination polymers</topic><topic>Structure of solids and liquids; crystallography</topic><topic>Structure of specific crystalline solids</topic><topic>Theory of crystal structure, crystal symmetry; calculations and modeling</topic><topic>Twinned crystal</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Goforth, Andrea M.</creatorcontrib><creatorcontrib>Gerth, Kathrine</creatorcontrib><creatorcontrib>Smith, Mark D.</creatorcontrib><creatorcontrib>Shotwell, Sandra</creatorcontrib><creatorcontrib>Bunz, Uwe H.F.</creatorcontrib><creatorcontrib>zur Loye, Hans-Conrad</creatorcontrib><collection>Pascal-Francis</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Solid state sciences</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Goforth, Andrea M.</au><au>Gerth, Kathrine</au><au>Smith, Mark D.</au><au>Shotwell, Sandra</au><au>Bunz, Uwe H.F.</au><au>zur Loye, Hans-Conrad</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Channel-containing structures generated from linear coordination polymer chains containing N , N ′ -bidentate ligands and Cu–Cu dimetal units</atitle><jtitle>Solid state sciences</jtitle><date>2005-09-01</date><risdate>2005</risdate><volume>7</volume><issue>9</issue><spage>1083</spage><epage>1095</epage><pages>1083-1095</pages><issn>1293-2558</issn><eissn>1873-3085</eissn><abstract>Four new one-dimensional coordination polymers containing the dimetal cluster Cu
2(OAc)
4 have been synthesized by reacting Cu(OAc)
2
⋅
H
2O with two different
N
,
N
′
-bidentate ligands. Reaction of the flexible ligand, 1,2-bis(4-pyridyl)ethane (
L
1), with the copper starting material produced two, co-crystallizing coordination polymers:
catena-Poly[Cu
2(OAc)
4(
L
1)]
⋅
2H
2O (
1) and
catena-Poly[Cu
2(OAc)
4(
L
1)]. In the solid state,
1 (monoclinic, C2/c,
a
=
24.9471
(
17
)
Å
,
b
=
13.3539
(
9
)
Å
,
c
=
8.8050
(
6
)
Å
,
β
=
93.6480
(
10
)
°
,
V
=
2927.4
(
3
)
Å
3
,
Z
=
4
) features linear chains which are organized into layers. These layers stack along the crystallographic
c-axis forming small hexagonal channels occupied by the solvent of crystallization. Compound
2 (triclinic, P-1,
a
=
7.6263
(
6
)
Å
,
b
=
8.5283
(
6
)
Å
,
c
=
9.8633
(
6
)
Å
,
α
=
74.1070
(
10
)
°
,
β
=
68.2160
(
10
)
°
,
γ
=
74.0090
(
10
)
°
,
V
=
561.96
(
7
)
Å
3
,
Z
=
1
) also features linear chains of the coordination polymer, but differs from
1 in that the chains are packed so as to leave no significant channels. Reaction of the rigid ligand, 1,4-bis(4-pyridyl)buta-1,3-diyne (
L
2), with the copper starting material also afforded two co-crystallizing coordination polymers:
catena-Poly[Cu
2(OAc)
4(
L
2)] (
3) and
catena-Poly[Cu
2(OAc)
4(
L
2)]
⋅
solvents (
4).
3 (monoclinic, P2
1/m,
a
=
9.8065
(
9
)
Å
,
b
=
12.3793
(
11
)
Å
,
c
=
9.9408
(
9
)
Å
,
β
=
107.6009
(
17
)
°
,
V
=
1150.29
(
18
)
Å
3
,
Z
=
2
), like
2, features linear chains and contains no significant solvent accessible void space.
4 (monoclinic, C2/c,
a
=
28.9810
(
16
)
Å
,
b
=
12.9301
(
7
)
Å
,
c
=
8.6954
(
5
)
Å
,
β
=
98.8010
(
10
)
°
,
V
=
3220.0
(
3
)
Å
3
,
Z
=
4
) also consists of linear chains of the coordination polymer. However, the overall topology of
4 is identical to that of
1, with the generated hexagonal channels containing crystallographically unidentifiable solvents of crystallization. Compounds
1 and
2 and compounds
3 and
4 are pairs of polymorphic coordination polymers neglecting the solvents of crystallization in
1 and
4. The compounds, which represent four new examples of coordination polymers containing dimetal units, have been characterized by IR, elemental analysis, and thermogravimetric analysis in addition to X-ray crystallography.</abstract><cop>Paris</cop><pub>Elsevier Masson SAS</pub><doi>10.1016/j.solidstatesciences.2005.03.006</doi><tpages>13</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1293-2558 |
| ispartof | Solid state sciences, 2005-09, Vol.7 (9), p.1083-1095 |
| issn | 1293-2558 1873-3085 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_28120553 |
| source | ScienceDirect Journals |
| subjects | [formula omitted]-bidentate ligands Condensed matter: structure, mechanical and thermal properties Coordination polymers Copper dimers Crystalline state (including molecular motions in solids) Dimetal building blocks Exact sciences and technology Physics Polymorphic coordination polymers Structure of solids and liquids crystallography Structure of specific crystalline solids Theory of crystal structure, crystal symmetry calculations and modeling Twinned crystal |
| title | Channel-containing structures generated from linear coordination polymer chains containing N , N ′ -bidentate ligands and Cu–Cu dimetal units |
| url | http://sfxeu10.hosted.exlibrisgroup.com/loughborough?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-19T19%3A50%3A39IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_pasca&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Channel-containing%20structures%20generated%20from%20linear%20coordination%20polymer%20chains%20containing%20N%20,%20N%20%E2%80%B2%20-bidentate%20ligands%20and%20Cu%E2%80%93Cu%20dimetal%20units&rft.jtitle=Solid%20state%20sciences&rft.au=Goforth,%20Andrea%20M.&rft.date=2005-09-01&rft.volume=7&rft.issue=9&rft.spage=1083&rft.epage=1095&rft.pages=1083-1095&rft.issn=1293-2558&rft.eissn=1873-3085&rft_id=info:doi/10.1016/j.solidstatesciences.2005.03.006&rft_dat=%3Cproquest_pasca%3E28120553%3C/proquest_pasca%3E%3Cgrp_id%3Ecdi_FETCH-LOGICAL-e283t-5da4624ff935917a4609f776710e9ad572b424c2a9de6bd3676078aacdf48fc33%3C/grp_id%3E%3Coa%3E%3C/oa%3E%3Curl%3E%3C/url%3E&rft_id=info:oai/&rft_pqid=28120553&rft_id=info:pmid/&rfr_iscdi=true |