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Chemical recycling of polyester textile wastes using silver-doped zinc oxide nanoparticles: an economical solution for circular economy
The waste management of polyethylene terephthalate (PET)–derived polyester (PES) textile is a global issue, and material recovery through chemical recycling can restore a circular economy. In our investigation, microwave-induced catalytic aminolysis and glycolysis of PES textile wastes using Ag-dope...
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| Published in: | Environmental science and pollution research international 2023-06, Vol.30 (30), p.75401-75416 |
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| creator | Vinitha, Viswanathan Preeyanghaa, Mani Anbarasu, Murugan Neppolian, Bernaurdshaw Sivamurugan, Vajiravelu |
| description | The waste management of polyethylene terephthalate (PET)–derived polyester (PES) textile is a global issue, and material recovery through chemical recycling can restore a circular economy. In our investigation, microwave-induced catalytic aminolysis and glycolysis of PES textile wastes using Ag-doped ZnO nanoparticles have been proposed. Ag-doped ZnO is prepared by the sol-gel method and characterised by XRD, FT-IR, UV-Vis, SEM-EDX and TEM. The reaction parameters such as PET-to-catalyst ratio, microwave power and irradiation time, temperature and catalyst recycling have been optimised. The catalyst was found to be more stable and could be recycled up to six times without losing its activity. Both the aminolysis and glycolysis of PES showed 100% conversion and afforded of bis (2-hydroxy ethylene) terephthalamide (BHETA) and bis (2-hydroxy ethylene) terephthalate (BHET), respectively. The depolymerisation of PES wastes using Ag-doped ZnO afforded BHETA and BHET for about 95 and 90%, respectively. The monomers BHET and BHETA confirmed by FT-IR,
1
H NMR and mass spectroscopy. According to the findings, 2 mol% Ag-doped ZnO has higher catalytic activity.
Graphical abstract |
| doi_str_mv | 10.1007/s11356-023-27567-0 |
| format | article |
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1
H NMR and mass spectroscopy. According to the findings, 2 mol% Ag-doped ZnO has higher catalytic activity.
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1
H NMR and mass spectroscopy. According to the findings, 2 mol% Ag-doped ZnO has higher catalytic activity.
Graphical abstract</description><subject>Aquatic Pollution</subject><subject>Atmospheric Protection/Air Quality Control/Air Pollution</subject><subject>Catalysts</subject><subject>Catalytic activity</subject><subject>Chemical recycling</subject><subject>Circular economy</subject><subject>Depolymerization</subject><subject>Earth and Environmental Science</subject><subject>Ecotoxicology</subject><subject>Environment</subject><subject>Environmental Chemistry</subject><subject>Environmental Health</subject><subject>Environmental science</subject><subject>Fourier transforms</subject><subject>Glycolysis</subject><subject>Infrared spectroscopy</subject><subject>Irradiation</subject><subject>Mass spectroscopy</subject><subject>Materials recovery</subject><subject>Microwave radiation</subject><subject>Monomers</subject><subject>Nanoparticles</subject><subject>Nanoparticles - chemistry</subject><subject>NMR</subject><subject>Nuclear magnetic resonance</subject><subject>Polyesters</subject><subject>Polyethylene terephthalate</subject><subject>Polyethylene Terephthalates - 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Academic</collection><jtitle>Environmental science and pollution research international</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Vinitha, Viswanathan</au><au>Preeyanghaa, Mani</au><au>Anbarasu, Murugan</au><au>Neppolian, Bernaurdshaw</au><au>Sivamurugan, Vajiravelu</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Chemical recycling of polyester textile wastes using silver-doped zinc oxide nanoparticles: an economical solution for circular economy</atitle><jtitle>Environmental science and pollution research international</jtitle><stitle>Environ Sci Pollut Res</stitle><addtitle>Environ Sci Pollut Res Int</addtitle><date>2023-06-01</date><risdate>2023</risdate><volume>30</volume><issue>30</issue><spage>75401</spage><epage>75416</epage><pages>75401-75416</pages><issn>1614-7499</issn><issn>0944-1344</issn><eissn>1614-7499</eissn><abstract>The waste management of polyethylene terephthalate (PET)–derived polyester (PES) textile is a global issue, and material recovery through chemical recycling can restore a circular economy. In our investigation, microwave-induced catalytic aminolysis and glycolysis of PES textile wastes using Ag-doped ZnO nanoparticles have been proposed. Ag-doped ZnO is prepared by the sol-gel method and characterised by XRD, FT-IR, UV-Vis, SEM-EDX and TEM. The reaction parameters such as PET-to-catalyst ratio, microwave power and irradiation time, temperature and catalyst recycling have been optimised. The catalyst was found to be more stable and could be recycled up to six times without losing its activity. Both the aminolysis and glycolysis of PES showed 100% conversion and afforded of bis (2-hydroxy ethylene) terephthalamide (BHETA) and bis (2-hydroxy ethylene) terephthalate (BHET), respectively. The depolymerisation of PES wastes using Ag-doped ZnO afforded BHETA and BHET for about 95 and 90%, respectively. The monomers BHET and BHETA confirmed by FT-IR,
1
H NMR and mass spectroscopy. According to the findings, 2 mol% Ag-doped ZnO has higher catalytic activity.
Graphical abstract</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><pmid>37217818</pmid><doi>10.1007/s11356-023-27567-0</doi><tpages>16</tpages><orcidid>https://orcid.org/0000-0002-9295-2118</orcidid></addata></record> |
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| ispartof | Environmental science and pollution research international, 2023-06, Vol.30 (30), p.75401-75416 |
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| source | ABI/INFORM Global; Springer Nature:Jisc Collections:Springer Nature Read and Publish 2023-2025: Springer Reading List |
| subjects | Aquatic Pollution Atmospheric Protection/Air Quality Control/Air Pollution Catalysts Catalytic activity Chemical recycling Circular economy Depolymerization Earth and Environmental Science Ecotoxicology Environment Environmental Chemistry Environmental Health Environmental science Fourier transforms Glycolysis Infrared spectroscopy Irradiation Mass spectroscopy Materials recovery Microwave radiation Monomers Nanoparticles Nanoparticles - chemistry NMR Nuclear magnetic resonance Polyesters Polyethylene terephthalate Polyethylene Terephthalates - chemistry Recycling Research Article Silver Silver - chemistry Sol-gel processes Spectroscopy, Fourier Transform Infrared Textile industry wastes Textiles Waste management Waste Water Technology Wastes Water Management Water Pollution Control Zinc oxide Zinc Oxide - chemistry Zinc oxides |
| title | Chemical recycling of polyester textile wastes using silver-doped zinc oxide nanoparticles: an economical solution for circular economy |
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