On the Use of Solomon Echoes in 27 Al NMR Studies of Complex Aluminium Hydrides

The quadrupole coupling constant C and the asymmetry parameter η have been determined for two complex aluminium hydrides from Al NMR spectra recorded for stationary samples by using the Solomon echo sequence. The thus obtained data for KAlH (C =(1.30±0.02) MHz, η=(0.64±0.02)) and NaAlH (C =(3.11±0.0...

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Published in:ChemistryOpen (Weinheim) 2024-01, Vol.13 (1), p.e202300011-e202300011
Main Authors: Zibrowius, Bodo, Fischer, Michael
Format: Article
Language:English
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Summary:The quadrupole coupling constant C and the asymmetry parameter η have been determined for two complex aluminium hydrides from Al NMR spectra recorded for stationary samples by using the Solomon echo sequence. The thus obtained data for KAlH (C =(1.30±0.02) MHz, η=(0.64±0.02)) and NaAlH (C =(3.11±0.02) MHz, η
ISSN:2191-1363
2191-1363
DOI:10.1002/open.202300011