Synthesis of Inorganic - Organic Polymers

In this study, 3-Glycidoxypropyl trimethoxysilane (GLYMO), Methyl triethoxy silane (MTEOS) were hydrolyzed and then polymerized with Aluminium-sec-butoxide, Al(OBus)3 that is complexed with Ethyl acetoacetate (HacacOEt). The complexation of Aluminium-sec-butoxide with Ethyl acetoacetate was investig...

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Bibliographic Details
Published in:Key engineering materials 2004-01, Vol.264-268, p.423-426
Main Authors: Arpac, E., Budakoglu, R.
Format: Article
Language:English
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Summary:In this study, 3-Glycidoxypropyl trimethoxysilane (GLYMO), Methyl triethoxy silane (MTEOS) were hydrolyzed and then polymerized with Aluminium-sec-butoxide, Al(OBus)3 that is complexed with Ethyl acetoacetate (HacacOEt). The complexation of Aluminium-sec-butoxide with Ethyl acetoacetate was investigated with Fourier Transform Infared Spectroscopy (FT-IR). The storage stability of the obtained so] was determined with viscosity measurements. Thermal behaviour of the hybrid gel was analysed with Thermogravimetric analysis (TGA). The TGA results showed that about 40% of the obtained hybrid polymer is inorganic and 60% is organic.
ISSN:1013-9826
1662-9795
1662-9795
DOI:10.4028/www.scientific.net/KEM.264-268.423