A cell for in situ dynamic X-ray diffraction studies: application to the dehydration of zeolite SrX

A new compact cell for in situ synchrotron X‐ray diffraction studies of adsorption or catalysis reactions has been designed to enable high performance whilst minimizing difficulties in use. It includes a system for simple insertion and alignment of capillary samples and an original miniaturized furn...

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Bibliographic Details
Published in:Journal of applied crystallography 2005-04, Vol.38 (2), p.370-373
Main Authors: Palancher, H., Pichon, C., Rebours, B., Hodeau, J. L., Lynch, J., Berar, J. F., Prevot, S., Conan, G., Bouchard, C.
Format: Article
Language:English
Subjects:
adsorption
catalysis
cell
Chemistry
Condensed matter: structure, mechanical and thermal properties
dehydration
Exact sciences and technology
General and physical chemistry
in situ X-ray diffraction
Ion-exchange
Physics
Single-crystal and powder diffraction
Structure of solids and liquids
crystallography
Surface physical chemistry
X-ray diffraction and scattering
zeolite
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Description
Summary:A new compact cell for in situ synchrotron X‐ray diffraction studies of adsorption or catalysis reactions has been designed to enable high performance whilst minimizing difficulties in use. It includes a system for simple insertion and alignment of capillary samples and an original miniaturized furnace providing excellent temperature homogeneity along the sample (temperature gradient less than 1 K over a 6 mm zone at 530 K). The efficiency of this setup is illustrated by in situ characterization of a zeolite (SrX) at four hydration levels.
ISSN:1600-5767
0021-8898
1600-5767
DOI:10.1107/S0021889805000294