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A cell for in situ dynamic X-ray diffraction studies: application to the dehydration of zeolite SrX
A new compact cell for in situ synchrotron X‐ray diffraction studies of adsorption or catalysis reactions has been designed to enable high performance whilst minimizing difficulties in use. It includes a system for simple insertion and alignment of capillary samples and an original miniaturized furn...
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| Published in: | Journal of applied crystallography 2005-04, Vol.38 (2), p.370-373 |
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| Main Authors: | , , , , , , , , |
| Format: | Article |
| Language: | English |
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| Citations: | Items that cite this one |
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| cited_by | cdi_FETCH-LOGICAL-c4202-af58ff3dd5ddd0e1a0b89f49187449281cd2de52f03010073f4f75a04e80f0ae3 |
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| container_end_page | 373 |
| container_issue | 2 |
| container_start_page | 370 |
| container_title | Journal of applied crystallography |
| container_volume | 38 |
| creator | Palancher, H. Pichon, C. Rebours, B. Hodeau, J. L. Lynch, J. Berar, J. F. Prevot, S. Conan, G. Bouchard, C. |
| description | A new compact cell for in situ synchrotron X‐ray diffraction studies of adsorption or catalysis reactions has been designed to enable high performance whilst minimizing difficulties in use. It includes a system for simple insertion and alignment of capillary samples and an original miniaturized furnace providing excellent temperature homogeneity along the sample (temperature gradient less than 1 K over a 6 mm zone at 530 K). The efficiency of this setup is illustrated by in situ characterization of a zeolite (SrX) at four hydration levels. |
| doi_str_mv | 10.1107/S0021889805000294 |
| format | article |
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The efficiency of this setup is illustrated by in situ characterization of a zeolite (SrX) at four hydration levels.</description><subject>adsorption</subject><subject>catalysis</subject><subject>cell</subject><subject>Chemistry</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>dehydration</subject><subject>Exact sciences and technology</subject><subject>General and physical chemistry</subject><subject>in situ X-ray diffraction</subject><subject>Ion-exchange</subject><subject>Physics</subject><subject>Single-crystal and powder diffraction</subject><subject>Structure of solids and liquids; crystallography</subject><subject>Surface physical chemistry</subject><subject>X-ray diffraction and scattering</subject><subject>zeolite</subject><issn>1600-5767</issn><issn>0021-8898</issn><issn>1600-5767</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2005</creationdate><recordtype>article</recordtype><recordid>eNqFkM1O3DAUhSMEEj_tA7CzkOgu9NqxY4cdGnUGCgIJaIvYWMY_wpCJp3YiGp6eDEGA6IKVr66_78g-WbaNYQ9j4N8vAAgWohLAYBgrupJt4BIgZ7zkq-_m9WwzpTsAXHJCNjJ9gLSta-RCRL5BybcdMn2j5l6jqzyqHhnvXFS69WG4bjvjbdpHarGovVbPyzag9tYiY297E8dVcOjRhtq3Fl3Eqy_ZmlN1sl9fzq3s1_TH5eQwPzmbHU0OTnJNCZBcOSacK4xhxhiwWMGNqBytsOCUVkRgbYixjDgoAAPwwlHHmQJqBThQttjKvo25ixj-dja1cu7T8neqsaFLkghRCozFAO58AO9CF5vhbZIM_VUMyBLCI6RjSClaJxfRz1XsJQa57Fz-1_ng7L4Eq6RVPfTWaJ_exLKknNFlthi5B1_b_vNg-XNyPpkxwGRQ81H1qbX_XlUV72XJC87kn9OZvKbkmF1Of8uqeAKy2580</recordid><startdate>200504</startdate><enddate>200504</enddate><creator>Palancher, H.</creator><creator>Pichon, C.</creator><creator>Rebours, B.</creator><creator>Hodeau, J. 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| fulltext | fulltext |
| identifier | ISSN: 1600-5767 |
| ispartof | Journal of applied crystallography, 2005-04, Vol.38 (2), p.370-373 |
| issn | 1600-5767 0021-8898 1600-5767 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_28868118 |
| source | Wiley-Blackwell Read & Publish Collection |
| subjects | adsorption catalysis cell Chemistry Condensed matter: structure, mechanical and thermal properties dehydration Exact sciences and technology General and physical chemistry in situ X-ray diffraction Ion-exchange Physics Single-crystal and powder diffraction Structure of solids and liquids crystallography Surface physical chemistry X-ray diffraction and scattering zeolite |
| title | A cell for in situ dynamic X-ray diffraction studies: application to the dehydration of zeolite SrX |
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