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Synchrotron radiation FT-IR micro-spectroscopy of fluorophlogopite in the O–H stretching region
Synchrotron radiation FT-IR polarized micro-spectroscopy has been used to investigate the natural mica fluorophlogopite in order to characterize the stretching vibrations of the OH groups and their orientation relative to the mica cleavage (0 0 1) plane. A procedure to eliminate undesired interferen...
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Published in: | Vibrational spectroscopy 2006-10, Vol.42 (1), p.59-62 |
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container_start_page | 59 |
container_title | Vibrational spectroscopy |
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creator | Piccinini, M. Cibin, G. Marcelli, A. Ventura, G. Della Bellatreccia, F. Mottana, A. |
description | Synchrotron radiation FT-IR polarized micro-spectroscopy has been used to investigate the natural mica fluorophlogopite in order to characterize the stretching vibrations of the OH groups and their orientation relative to the mica cleavage (0
0
1) plane. A procedure to eliminate undesired interference fringes, typically observed when working with thin single-crystals, was set up using an ad hoc sample preparation, and tested.
The naturally high brilliance and high polarization properties of synchrotron radiation allows to study very small flakes and hence offers new analytical possibilities in comparison to conventional powder FT-IR spectroscopy. |
doi_str_mv | 10.1016/j.vibspec.2006.04.010 |
format | article |
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0
1) plane. A procedure to eliminate undesired interference fringes, typically observed when working with thin single-crystals, was set up using an ad hoc sample preparation, and tested.
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0
1) plane. A procedure to eliminate undesired interference fringes, typically observed when working with thin single-crystals, was set up using an ad hoc sample preparation, and tested.
The naturally high brilliance and high polarization properties of synchrotron radiation allows to study very small flakes and hence offers new analytical possibilities in comparison to conventional powder FT-IR spectroscopy.</description><subject>Infrared</subject><subject>Mica</subject><subject>Microscopy</subject><subject>Phyllosilicates</subject><subject>Synchrotron radiation</subject><issn>0924-2031</issn><issn>1873-3697</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2006</creationdate><recordtype>article</recordtype><recordid>eNqFkMtKAzEUhoMoWC-PIGTlbsaTy9xWIkVtQSh4WYdM5kybMp2MybTQne_gG_okptS9q3Pg_OeD_yPkhkHKgOV363Rn6zCgSTlAnoJMgcEJmbCyEInIq-KUTKDiMuEg2Dm5CGENMZgxMSH6bd-blXejdz31urF6tHF7ek_mr3RjjXfJgRzPwbhhT11L227rvBtWnVu6wY5IbU_HFdLFz9f3jIbR42hWtl9Sj8vIuiJnre4CXv_NS_Lx9Pg-nSUvi-f59OElMULCmPCCywx1XgBgyTPJqhLqRlY50zXDttZtaeosh5oXmZCyZlJoWcX-Rmet4KW4JLdH7uDd5xbDqDY2GOw63aPbBsUrmQngRQxmx2AsF4LHVg3ebrTfKwbqIFSt1Z9QdRCqQKooNP7dH_8wtthZ9CoYi73BxvpoSDXO_kP4BR6QgzQ</recordid><startdate>20061018</startdate><enddate>20061018</enddate><creator>Piccinini, M.</creator><creator>Cibin, G.</creator><creator>Marcelli, A.</creator><creator>Ventura, G. Della</creator><creator>Bellatreccia, F.</creator><creator>Mottana, A.</creator><general>Elsevier B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20061018</creationdate><title>Synchrotron radiation FT-IR micro-spectroscopy of fluorophlogopite in the O–H stretching region</title><author>Piccinini, M. ; Cibin, G. ; Marcelli, A. ; Ventura, G. Della ; Bellatreccia, F. ; Mottana, A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c340t-27245ea6700e82541980bd4961ab1efbaf8cb560b275344b143a49101ca5f3283</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2006</creationdate><topic>Infrared</topic><topic>Mica</topic><topic>Microscopy</topic><topic>Phyllosilicates</topic><topic>Synchrotron radiation</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Piccinini, M.</creatorcontrib><creatorcontrib>Cibin, G.</creatorcontrib><creatorcontrib>Marcelli, A.</creatorcontrib><creatorcontrib>Ventura, G. Della</creatorcontrib><creatorcontrib>Bellatreccia, F.</creatorcontrib><creatorcontrib>Mottana, A.</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Vibrational spectroscopy</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Piccinini, M.</au><au>Cibin, G.</au><au>Marcelli, A.</au><au>Ventura, G. Della</au><au>Bellatreccia, F.</au><au>Mottana, A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synchrotron radiation FT-IR micro-spectroscopy of fluorophlogopite in the O–H stretching region</atitle><jtitle>Vibrational spectroscopy</jtitle><date>2006-10-18</date><risdate>2006</risdate><volume>42</volume><issue>1</issue><spage>59</spage><epage>62</epage><pages>59-62</pages><issn>0924-2031</issn><eissn>1873-3697</eissn><abstract>Synchrotron radiation FT-IR polarized micro-spectroscopy has been used to investigate the natural mica fluorophlogopite in order to characterize the stretching vibrations of the OH groups and their orientation relative to the mica cleavage (0
0
1) plane. A procedure to eliminate undesired interference fringes, typically observed when working with thin single-crystals, was set up using an ad hoc sample preparation, and tested.
The naturally high brilliance and high polarization properties of synchrotron radiation allows to study very small flakes and hence offers new analytical possibilities in comparison to conventional powder FT-IR spectroscopy.</abstract><pub>Elsevier B.V</pub><doi>10.1016/j.vibspec.2006.04.010</doi><tpages>4</tpages></addata></record> |
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subjects | Infrared Mica Microscopy Phyllosilicates Synchrotron radiation |
title | Synchrotron radiation FT-IR micro-spectroscopy of fluorophlogopite in the O–H stretching region |
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