Study on the Tribological Properties of DIN 16MnCr5 Steel after Duplex Gas-Nitriding and Pack Boriding

• Published in: Materials 2024-06, Vol.17 (13), p.3057
• Main Authors: Carrera Espinoza, Rafael, Alvarez Vera, Melvyn, Wettlaufer, Marc, Kerl, Manuel, Barth, Stefan, Moreno Garibaldi, Pablo, Díaz Guillen, Juan Carlos, Hernández García, Héctor Manuel, Muñoz Arroyo, Rita, Ortega, Javier A
• Format: Article
• Language: English
• Subjects: Ammonia; Bolted joints; Boriding; Chromium manganese steels; Coefficient of friction; Elastic properties; Evaluation; Friction resistance; Gases; Mechanical engineering; Mechanical properties; Microhardness; Microstructure; Modulus of elasticity; Nanoindentation; Nitriding; Optical microscopy; Optical properties; Quenching and tempering; Salt; Steel; Surface treatment; Tribology; Wear resistance
• ISSN: 1996-1944; 1996-1944
• DOI: 10.3390/ma17133057

DIN 16MnCr5 is commonly used in mechanical engineering contact applications such as gears, joint parts, shafts, gear wheels, camshafts, bolts, pins, and cardan joints, among others. This study examined the microstructural and mechanical properties and tribological behavior of different surface treatments applied to DIN 16MnCr5 steel. The samples were hardened at 870 °C for 15 min and then quenched in water. The surface conditions evaluated were as follows: quenched and tempered DIN 16MnCr5 steel samples without surface treatments (control group), quenched and tempered DIN 16MnCr5 steel samples with gas-nitriding at 560 °C for 6 h, quenched and tempered DIN 16MnCr5 steel samples with pack boriding at 950 °C for 4 h, and quenched and tempered DIN 16MnCr5 steel samples with duplex gas-nitriding and pack boriding. Microstructure characterization was carried out using metallographic techniques, optical microscopy, scanning electron microscopy with energy-dispersive spectroscopy, and X-ray diffraction. The mechanical properties were assessed through microhardness and elastic modulus tests using nanoindentation. The tribological behavior was evaluated using pin-on-disc tests following the ASTM G99-17 standard procedure under dry sliding conditions. The results indicated that the surface treated with duplex gas-nitriding and pack boriding exhibited the highest wear resistance and a reduced coefficient of friction due to improved mechanical properties, leading to increased hardness and elastic modulus.