Effect of phosphoric acid etching and blasting with aluminum oxide on the enamel topography and adhesion of resin composite to intact or abraded enamel

• Published in: Dental materials 2024-11, Vol.40 (11), p.e102-e111
• Main Authors: Rifane, Tainah Oliveira, Hirata, Ronaldo, Araújo-Neto, Vitaliano Gomes, Ottoboni, Thiago, Feitosa, Victor Pinheiro, Giannini, Marcelo
• Format: Article
• Language: English
• Subjects: Aluminum oxide; Blasting; Enamel; Microtensile
• ISSN: 0109-5641; 1879-0097; 1879-0097
• DOI: 10.1016/j.dental.2024.08.003

To evaluate the effects of the phosphoric acid (PA) etching, self-etching technique (SE) and blasting with Al2O3 particles (BL) on the bonding of a dental adhesive to intact (INT) or abraded (ABR) enamel. Enamel surfaces were treated as follows: 1- ABR-PA: INT was abraded with SiC paper and etched with PA (20 s) before Clearfil Universal Bond Quick adhesive application; 2- ABR-SE: ABR was SiC and adhesive applied in SE mode; 3- INT-PA: INT was etched with PA and adhesive applied; 4- INT-SE: the adhesive (SE mode) was applied to INT; 5- INT-BL: INT was BL and the adhesive was applied (SE mode), and 6- INT-BA: INT was BL, etched with PA and adhesive applied (SE mode). The enamel surface treated was examined with scanning electron microscopy (SEM) (n = 3) and Al2O3 particles were characterized using SEM and EDX. The enamel bond strength was measured by microtensile test (24 h and 1 year) (n = 8) and the morphology of enamel-adhesive interfaces were analyzed by SEM (n = 3). Bond strength data were analyzed by two-way ANOVA and Tukey’s test (α = 0.05). Al2O3 particles had an irregular shape, their length varied (50–20 µm) and the perimeter mean was 38.8 µm. The enamel morphology significantly influenced the enamel bond strength. ABR-PA, INT-BL, and INT-BA provided greater and stable enamel-dentin interaction and bond strength. The enamel morphology significantly influenced the enamel bond strength. Using the adhesive in etch-and-rinse mode, enamel must be abraded before etching and must be Al2O3-blasted when used in SE mode.