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Microwave-induced combustion for further determination of potentially toxic elements in honey by ICP-MS
Microwave-induced combustion (MIC) was proposed in this study for honey decomposition aiming for As, Cd, Hg, and Pb determination by inductively coupled plasma mass spectrometry (ICP-MS). Sample mass (up to 1.0 g), absorbing solution (0.5 to 14.4 mol L −1 HNO 3 , and H 2 O), heating program, and com...
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| Published in: | Analytical and bioanalytical chemistry 2024-05, Vol.416 (11), p.2859-2870 |
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| Main Authors: | , , , , , , |
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| container_end_page | 2870 |
| container_issue | 11 |
| container_start_page | 2859 |
| container_title | Analytical and bioanalytical chemistry |
| container_volume | 416 |
| creator | Cauduro, Vitoria H. Alves, Camila M. A. C. Nascimento, Mariele S. Druzian, Gabriel T. Balbinot, Fernanda P. Mesko, Marcia F. Flores, Erico M. M. |
| description | Microwave-induced combustion (MIC) was proposed in this study for honey decomposition aiming for As, Cd, Hg, and Pb determination by inductively coupled plasma mass spectrometry (ICP-MS). Sample mass (up to 1.0 g), absorbing solution (0.5 to 14.4 mol L
−1
HNO
3
, and H
2
O), heating program, and combustion aids were evaluated. The Eurachem guidelines were used for method validation. The proposed method enabled combustion of a high sample mass (0.8 g of honey, with 0.4 g of microcrystalline cellulose and 100 µL of 6 mol L
−1
NH
4
NO
3
) using 6 mL of an absorbing solution consisting of 1 mol L
−1
HNO
3
, which resulted in low residual carbon in solution ( |
| doi_str_mv | 10.1007/s00216-024-05235-7 |
| format | article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_3153707250</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2954775777</sourcerecordid><originalsourceid>FETCH-LOGICAL-c359t-2d7dd382d1910eee29422912cc2f73f49d6ef710a3cf88745ee4b6e330fc43fa3</originalsourceid><addsrcrecordid>eNqFkU1PHSEUholpo9b2D7gwJG66oYUDDDNLc9MPE02bVNdkLhwUMwO3MGN7_31Hr7VJF-0Kwnl4T855CDkW_J3g3LyvnINoGAfFuAapmdkjh6IRLYNG8xfPdwUH5FWtd5wL3YpmnxzIVumua8whubmMruQf_T2ymPzs0FOXx_Vcp5gTDbnQMJfpFgv1OGEZY-ofKznQTZ4wTbEfhi2d8s_oKA44Lk-VxkRvc8ItXW_p-eoru_z2mrwM_VDxzdN5RK4_frhafWYXXz6dr84umJO6mxh4471swYtOcESETgF0ApyDYGRQnW8wGMF76ULbGqUR1bpBKXlwSoZeHpG3u9xNyd9nrJMdY3U4DH3CPFcrhZaGG9D8vyh0WhmjjTELevoXepfnkpZBrOTSABgl24WCHbVstNaCwW5KHPuytYLbB2N2Z8wuxuyjMfsQffIUPa9H9M9ffitaALkD6lJKN1j-9P5H7C-_XqEL</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>3037227438</pqid></control><display><type>article</type><title>Microwave-induced combustion for further determination of potentially toxic elements in honey by ICP-MS</title><source>Springer Link</source><creator>Cauduro, Vitoria H. ; Alves, Camila M. A. C. ; Nascimento, Mariele S. ; Druzian, Gabriel T. ; Balbinot, Fernanda P. ; Mesko, Marcia F. ; Flores, Erico M. M.</creator><creatorcontrib>Cauduro, Vitoria H. ; Alves, Camila M. A. C. ; Nascimento, Mariele S. ; Druzian, Gabriel T. ; Balbinot, Fernanda P. ; Mesko, Marcia F. ; Flores, Erico M. M.</creatorcontrib><description>Microwave-induced combustion (MIC) was proposed in this study for honey decomposition aiming for As, Cd, Hg, and Pb determination by inductively coupled plasma mass spectrometry (ICP-MS). Sample mass (up to 1.0 g), absorbing solution (0.5 to 14.4 mol L
−1
HNO
3
, and H
2
O), heating program, and combustion aids were evaluated. The Eurachem guidelines were used for method validation. The proposed method enabled combustion of a high sample mass (0.8 g of honey, with 0.4 g of microcrystalline cellulose and 100 µL of 6 mol L
−1
NH
4
NO
3
) using 6 mL of an absorbing solution consisting of 1 mol L
−1
HNO
3
, which resulted in low residual carbon in solution (< 25 mg L
−1
). Honey samples from different geographical origins were analyzed. Results showed no significant difference in comparison to other two microwave decomposition methods, based on microwave-assisted wet digestion with single reaction chamber (MAWD-SRC) and microwave-assisted wet digestion (MAWD). Standard addition experiments resulted in recoveries higher than 98%. The limits of detection ranged from 1.10 (As) to 4.60 ng g
−1
(Pb). In addition to using only diluted reagents and resulting in digests virtually free of interferences, the proposed method was faster (< 30 min) than most of those presented in the literature.
Graphical Abstract</description><identifier>ISSN: 1618-2642</identifier><identifier>ISSN: 1618-2650</identifier><identifier>EISSN: 1618-2650</identifier><identifier>DOI: 10.1007/s00216-024-05235-7</identifier><identifier>PMID: 38459967</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Ammonium nitrate ; Analytical Chemistry ; atomic absorption spectrometry ; Biochemistry ; Carbon ; Cellulose ; Characterization and Evaluation of Materials ; Chemistry ; Chemistry and Materials Science ; Combustion ; Crystalline cellulose ; Decomposition ; Decomposition reactions ; Digestion ; Elemental Mass Spectrometry for Bioanalysis ; Food products ; Food Science ; Geographical distribution ; Honey ; Inductively coupled plasma mass spectrometry ; Laboratory Medicine ; Lead ; Mass spectrometry ; Mass spectroscopy ; Mercury (metal) ; Methods ; microwave treatment ; Mollusks ; Monitoring/Environmental Analysis ; Reagents ; Research Paper ; Scientific imaging ; toxicity</subject><ispartof>Analytical and bioanalytical chemistry, 2024-05, Vol.416 (11), p.2859-2870</ispartof><rights>The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2024. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><rights>2024. The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c359t-2d7dd382d1910eee29422912cc2f73f49d6ef710a3cf88745ee4b6e330fc43fa3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27901,27902</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/38459967$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Cauduro, Vitoria H.</creatorcontrib><creatorcontrib>Alves, Camila M. A. C.</creatorcontrib><creatorcontrib>Nascimento, Mariele S.</creatorcontrib><creatorcontrib>Druzian, Gabriel T.</creatorcontrib><creatorcontrib>Balbinot, Fernanda P.</creatorcontrib><creatorcontrib>Mesko, Marcia F.</creatorcontrib><creatorcontrib>Flores, Erico M. M.</creatorcontrib><title>Microwave-induced combustion for further determination of potentially toxic elements in honey by ICP-MS</title><title>Analytical and bioanalytical chemistry</title><addtitle>Anal Bioanal Chem</addtitle><addtitle>Anal Bioanal Chem</addtitle><description>Microwave-induced combustion (MIC) was proposed in this study for honey decomposition aiming for As, Cd, Hg, and Pb determination by inductively coupled plasma mass spectrometry (ICP-MS). Sample mass (up to 1.0 g), absorbing solution (0.5 to 14.4 mol L
−1
HNO
3
, and H
2
O), heating program, and combustion aids were evaluated. The Eurachem guidelines were used for method validation. The proposed method enabled combustion of a high sample mass (0.8 g of honey, with 0.4 g of microcrystalline cellulose and 100 µL of 6 mol L
−1
NH
4
NO
3
) using 6 mL of an absorbing solution consisting of 1 mol L
−1
HNO
3
, which resulted in low residual carbon in solution (< 25 mg L
−1
). Honey samples from different geographical origins were analyzed. Results showed no significant difference in comparison to other two microwave decomposition methods, based on microwave-assisted wet digestion with single reaction chamber (MAWD-SRC) and microwave-assisted wet digestion (MAWD). Standard addition experiments resulted in recoveries higher than 98%. The limits of detection ranged from 1.10 (As) to 4.60 ng g
−1
(Pb). In addition to using only diluted reagents and resulting in digests virtually free of interferences, the proposed method was faster (< 30 min) than most of those presented in the literature.
Graphical Abstract</description><subject>Ammonium nitrate</subject><subject>Analytical Chemistry</subject><subject>atomic absorption spectrometry</subject><subject>Biochemistry</subject><subject>Carbon</subject><subject>Cellulose</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Combustion</subject><subject>Crystalline cellulose</subject><subject>Decomposition</subject><subject>Decomposition reactions</subject><subject>Digestion</subject><subject>Elemental Mass Spectrometry for Bioanalysis</subject><subject>Food products</subject><subject>Food Science</subject><subject>Geographical distribution</subject><subject>Honey</subject><subject>Inductively coupled plasma mass spectrometry</subject><subject>Laboratory Medicine</subject><subject>Lead</subject><subject>Mass spectrometry</subject><subject>Mass spectroscopy</subject><subject>Mercury (metal)</subject><subject>Methods</subject><subject>microwave treatment</subject><subject>Mollusks</subject><subject>Monitoring/Environmental Analysis</subject><subject>Reagents</subject><subject>Research Paper</subject><subject>Scientific imaging</subject><subject>toxicity</subject><issn>1618-2642</issn><issn>1618-2650</issn><issn>1618-2650</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2024</creationdate><recordtype>article</recordtype><recordid>eNqFkU1PHSEUholpo9b2D7gwJG66oYUDDDNLc9MPE02bVNdkLhwUMwO3MGN7_31Hr7VJF-0Kwnl4T855CDkW_J3g3LyvnINoGAfFuAapmdkjh6IRLYNG8xfPdwUH5FWtd5wL3YpmnxzIVumua8whubmMruQf_T2ymPzs0FOXx_Vcp5gTDbnQMJfpFgv1OGEZY-ofKznQTZ4wTbEfhi2d8s_oKA44Lk-VxkRvc8ItXW_p-eoru_z2mrwM_VDxzdN5RK4_frhafWYXXz6dr84umJO6mxh4471swYtOcESETgF0ApyDYGRQnW8wGMF76ULbGqUR1bpBKXlwSoZeHpG3u9xNyd9nrJMdY3U4DH3CPFcrhZaGG9D8vyh0WhmjjTELevoXepfnkpZBrOTSABgl24WCHbVstNaCwW5KHPuytYLbB2N2Z8wuxuyjMfsQffIUPa9H9M9ffitaALkD6lJKN1j-9P5H7C-_XqEL</recordid><startdate>20240501</startdate><enddate>20240501</enddate><creator>Cauduro, Vitoria H.</creator><creator>Alves, Camila M. A. C.</creator><creator>Nascimento, Mariele S.</creator><creator>Druzian, Gabriel T.</creator><creator>Balbinot, Fernanda P.</creator><creator>Mesko, Marcia F.</creator><creator>Flores, Erico M. 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A. C.</au><au>Nascimento, Mariele S.</au><au>Druzian, Gabriel T.</au><au>Balbinot, Fernanda P.</au><au>Mesko, Marcia F.</au><au>Flores, Erico M. M.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Microwave-induced combustion for further determination of potentially toxic elements in honey by ICP-MS</atitle><jtitle>Analytical and bioanalytical chemistry</jtitle><stitle>Anal Bioanal Chem</stitle><addtitle>Anal Bioanal Chem</addtitle><date>2024-05-01</date><risdate>2024</risdate><volume>416</volume><issue>11</issue><spage>2859</spage><epage>2870</epage><pages>2859-2870</pages><issn>1618-2642</issn><issn>1618-2650</issn><eissn>1618-2650</eissn><abstract>Microwave-induced combustion (MIC) was proposed in this study for honey decomposition aiming for As, Cd, Hg, and Pb determination by inductively coupled plasma mass spectrometry (ICP-MS). Sample mass (up to 1.0 g), absorbing solution (0.5 to 14.4 mol L
−1
HNO
3
, and H
2
O), heating program, and combustion aids were evaluated. The Eurachem guidelines were used for method validation. The proposed method enabled combustion of a high sample mass (0.8 g of honey, with 0.4 g of microcrystalline cellulose and 100 µL of 6 mol L
−1
NH
4
NO
3
) using 6 mL of an absorbing solution consisting of 1 mol L
−1
HNO
3
, which resulted in low residual carbon in solution (< 25 mg L
−1
). Honey samples from different geographical origins were analyzed. Results showed no significant difference in comparison to other two microwave decomposition methods, based on microwave-assisted wet digestion with single reaction chamber (MAWD-SRC) and microwave-assisted wet digestion (MAWD). Standard addition experiments resulted in recoveries higher than 98%. The limits of detection ranged from 1.10 (As) to 4.60 ng g
−1
(Pb). In addition to using only diluted reagents and resulting in digests virtually free of interferences, the proposed method was faster (< 30 min) than most of those presented in the literature.
Graphical Abstract</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><pmid>38459967</pmid><doi>10.1007/s00216-024-05235-7</doi><tpages>12</tpages></addata></record> |
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| subjects | Ammonium nitrate Analytical Chemistry atomic absorption spectrometry Biochemistry Carbon Cellulose Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Combustion Crystalline cellulose Decomposition Decomposition reactions Digestion Elemental Mass Spectrometry for Bioanalysis Food products Food Science Geographical distribution Honey Inductively coupled plasma mass spectrometry Laboratory Medicine Lead Mass spectrometry Mass spectroscopy Mercury (metal) Methods microwave treatment Mollusks Monitoring/Environmental Analysis Reagents Research Paper Scientific imaging toxicity |
| title | Microwave-induced combustion for further determination of potentially toxic elements in honey by ICP-MS |
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