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Synthesis and characterization of neodymium oxyhydroxide crystals
Single crystals of neodymium oxyhydroxide NdOOH were grown using an electrochemical method. Crystals having a maximum size of about 2 mm in length were grown. The structure was identified by single crystal X-ray diffraction and the refinement converged to R1 = 0.0170 and wR1 = 0.0426. NdOOH crystall...
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| Published in: | Journal of alloys and compounds 2009-01, Vol.468 (1), p.566-570 |
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| Main Authors: | , , , , , |
| Format: | Article |
| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c436t-96809af46bf862aa35036b9286f18968f21ec2a9318e14fdd0709481c24e2e693 |
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| cites | cdi_FETCH-LOGICAL-c436t-96809af46bf862aa35036b9286f18968f21ec2a9318e14fdd0709481c24e2e693 |
| container_end_page | 570 |
| container_issue | 1 |
| container_start_page | 566 |
| container_title | Journal of alloys and compounds |
| container_volume | 468 |
| creator | Samata, H. Kimura, D. Mizusaki, S. Nagata, Y. Ozawa, T.C. Sato, A. |
| description | Single crystals of neodymium oxyhydroxide NdOOH were grown using an electrochemical method. Crystals having a maximum size of about 2
mm in length were grown. The structure was identified by single crystal X-ray diffraction and the refinement converged to R1
=
0.0170 and wR1
=
0.0426. NdOOH crystallizes in a monoclinic structure of the space group
P2
1/
m with lattice parameters of
a
=
4.3896(2)
Å,
b
=
3.8319(2)
Å,
c
=
6.2424(3)
Å, and
β
=
108.131(2)°, and
Z
=
2. The resistivity shows semiconductor-like characteristics with the activation energy
E
a
=
0.93
eV. No magnetic order was found down to 5
K. |
| doi_str_mv | 10.1016/j.jallcom.2008.01.056 |
| format | article |
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mm in length were grown. The structure was identified by single crystal X-ray diffraction and the refinement converged to R1
=
0.0170 and wR1
=
0.0426. NdOOH crystallizes in a monoclinic structure of the space group
P2
1/
m with lattice parameters of
a
=
4.3896(2)
Å,
b
=
3.8319(2)
Å,
c
=
6.2424(3)
Å, and
β
=
108.131(2)°, and
Z
=
2. The resistivity shows semiconductor-like characteristics with the activation energy
E
a
=
0.93
eV. No magnetic order was found down to 5
K.</description><identifier>ISSN: 0925-8388</identifier><identifier>EISSN: 1873-4669</identifier><identifier>DOI: 10.1016/j.jallcom.2008.01.056</identifier><language>eng</language><publisher>Kidlington: Elsevier B.V</publisher><subject>Condensed matter: structure, mechanical and thermal properties ; Crystal growth ; Crystal structure ; Exact sciences and technology ; Inorganic compounds ; Magnetic measurement ; NdOOH ; Physics ; Structure of solids and liquids; crystallography ; Structure of specific crystalline solids</subject><ispartof>Journal of alloys and compounds, 2009-01, Vol.468 (1), p.566-570</ispartof><rights>2008 Elsevier B.V.</rights><rights>2009 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c436t-96809af46bf862aa35036b9286f18968f21ec2a9318e14fdd0709481c24e2e693</citedby><cites>FETCH-LOGICAL-c436t-96809af46bf862aa35036b9286f18968f21ec2a9318e14fdd0709481c24e2e693</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=21066933$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Samata, H.</creatorcontrib><creatorcontrib>Kimura, D.</creatorcontrib><creatorcontrib>Mizusaki, S.</creatorcontrib><creatorcontrib>Nagata, Y.</creatorcontrib><creatorcontrib>Ozawa, T.C.</creatorcontrib><creatorcontrib>Sato, A.</creatorcontrib><title>Synthesis and characterization of neodymium oxyhydroxide crystals</title><title>Journal of alloys and compounds</title><description>Single crystals of neodymium oxyhydroxide NdOOH were grown using an electrochemical method. Crystals having a maximum size of about 2
mm in length were grown. The structure was identified by single crystal X-ray diffraction and the refinement converged to R1
=
0.0170 and wR1
=
0.0426. NdOOH crystallizes in a monoclinic structure of the space group
P2
1/
m with lattice parameters of
a
=
4.3896(2)
Å,
b
=
3.8319(2)
Å,
c
=
6.2424(3)
Å, and
β
=
108.131(2)°, and
Z
=
2. The resistivity shows semiconductor-like characteristics with the activation energy
E
a
=
0.93
eV. No magnetic order was found down to 5
K.</description><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Crystal growth</subject><subject>Crystal structure</subject><subject>Exact sciences and technology</subject><subject>Inorganic compounds</subject><subject>Magnetic measurement</subject><subject>NdOOH</subject><subject>Physics</subject><subject>Structure of solids and liquids; crystallography</subject><subject>Structure of specific crystalline solids</subject><issn>0925-8388</issn><issn>1873-4669</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2009</creationdate><recordtype>article</recordtype><recordid>eNqFkEtPwzAQhC0EEuXxE5BygVvC2k5c-4QqxEtC4gCcLeOsVVdJXOwUEX49rlpx5TSHndnZ_Qi5oFBRoOJ6Va1M19nQVwxAVkAraMQBmVE552UthDokM1CsKSWX8picpLQCAKo4nZHF6zSMS0w-FWZoC7s00dgRo_8xow9DEVwxYGin3m_6InxPy6mN4du3WNg4pdF06YwcuSx4vtdT8n5_93b7WD6_PDzdLp5LW3MxlkpIUMbV4sNJwYzhDXDxoZgUjso8dIyiZSYfJZHWrm1hDqqW1LIaGQrFT8nVbu86hs8NplH3PlnsOpMP3CTNmZrLhtJsbHZGG0NKEZ1eR9-bOGkKegtMr_QemN4C00B1BpZzl_sCk6zpXDSD9ekvzChklJxn383Oh_nbL49RJ-txsNj6iHbUbfD_NP0CviuEGw</recordid><startdate>20090122</startdate><enddate>20090122</enddate><creator>Samata, H.</creator><creator>Kimura, D.</creator><creator>Mizusaki, S.</creator><creator>Nagata, Y.</creator><creator>Ozawa, T.C.</creator><creator>Sato, A.</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20090122</creationdate><title>Synthesis and characterization of neodymium oxyhydroxide crystals</title><author>Samata, H. ; Kimura, D. ; Mizusaki, S. ; Nagata, Y. ; Ozawa, T.C. ; Sato, A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c436t-96809af46bf862aa35036b9286f18968f21ec2a9318e14fdd0709481c24e2e693</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2009</creationdate><topic>Condensed matter: structure, mechanical and thermal properties</topic><topic>Crystal growth</topic><topic>Crystal structure</topic><topic>Exact sciences and technology</topic><topic>Inorganic compounds</topic><topic>Magnetic measurement</topic><topic>NdOOH</topic><topic>Physics</topic><topic>Structure of solids and liquids; crystallography</topic><topic>Structure of specific crystalline solids</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Samata, H.</creatorcontrib><creatorcontrib>Kimura, D.</creatorcontrib><creatorcontrib>Mizusaki, S.</creatorcontrib><creatorcontrib>Nagata, Y.</creatorcontrib><creatorcontrib>Ozawa, T.C.</creatorcontrib><creatorcontrib>Sato, A.</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of alloys and compounds</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Samata, H.</au><au>Kimura, D.</au><au>Mizusaki, S.</au><au>Nagata, Y.</au><au>Ozawa, T.C.</au><au>Sato, A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and characterization of neodymium oxyhydroxide crystals</atitle><jtitle>Journal of alloys and compounds</jtitle><date>2009-01-22</date><risdate>2009</risdate><volume>468</volume><issue>1</issue><spage>566</spage><epage>570</epage><pages>566-570</pages><issn>0925-8388</issn><eissn>1873-4669</eissn><abstract>Single crystals of neodymium oxyhydroxide NdOOH were grown using an electrochemical method. Crystals having a maximum size of about 2
mm in length were grown. The structure was identified by single crystal X-ray diffraction and the refinement converged to R1
=
0.0170 and wR1
=
0.0426. NdOOH crystallizes in a monoclinic structure of the space group
P2
1/
m with lattice parameters of
a
=
4.3896(2)
Å,
b
=
3.8319(2)
Å,
c
=
6.2424(3)
Å, and
β
=
108.131(2)°, and
Z
=
2. The resistivity shows semiconductor-like characteristics with the activation energy
E
a
=
0.93
eV. No magnetic order was found down to 5
K.</abstract><cop>Kidlington</cop><pub>Elsevier B.V</pub><doi>10.1016/j.jallcom.2008.01.056</doi><tpages>5</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0925-8388 |
| ispartof | Journal of alloys and compounds, 2009-01, Vol.468 (1), p.566-570 |
| issn | 0925-8388 1873-4669 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_32978511 |
| source | ScienceDirect Freedom Collection 2022-2024 |
| subjects | Condensed matter: structure, mechanical and thermal properties Crystal growth Crystal structure Exact sciences and technology Inorganic compounds Magnetic measurement NdOOH Physics Structure of solids and liquids crystallography Structure of specific crystalline solids |
| title | Synthesis and characterization of neodymium oxyhydroxide crystals |
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