Crystal structure analysis of Bis{(N,N′-dimethylformamide)-[μ-bis-N,N′-(2-oxybenzyl)-1,3-propanediaminato](μ-asetato) nickel(II)}nickel(II)

The title compound, a homotrinuclear NiII complex has been synthesized from ONNO type Schiff base reduced with the help of NaBH4. The structure of the complex, [Ni{Ni(CH3CO2) (C17H20N2O2) (C3H7NO)}2], was identified using elemental analysis, thermal analysis, IR spectroscopy and x‐ray diffraction te...

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Published in:Crystal research and technology (1979) 2002-12, Vol.37 (12), p.1352-1359
Main Authors: Tatar Yildirim, L., Atakol, O.
Format: Article
Language:English
Subjects:
Condensed matter: structure, mechanical and thermal properties
crystal structure
elemental analysis
Exact sciences and technology
Inorganic compounds
Metal complexes
NiII
Physics
Schiff base
Structure of solids and liquids
crystallography
Structure of specific crystalline solids
thermal analysis
trinuclear complex
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cited_by cdi_FETCH-LOGICAL-c3873-901d72180abef24d8b6e6dd795afb5facb05623f1cc1a6a704f8f6600f66e4903
cites cdi_FETCH-LOGICAL-c3873-901d72180abef24d8b6e6dd795afb5facb05623f1cc1a6a704f8f6600f66e4903
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container_title Crystal research and technology (1979)
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creator Tatar Yildirim, L.
Atakol, O.
description The title compound, a homotrinuclear NiII complex has been synthesized from ONNO type Schiff base reduced with the help of NaBH4. The structure of the complex, [Ni{Ni(CH3CO2) (C17H20N2O2) (C3H7NO)}2], was identified using elemental analysis, thermal analysis, IR spectroscopy and x‐ray diffraction techniques. It was established that although some bond lengths and angles changed with respect to previous complexes, the Ni…Ni distance was approximately the same.
doi_str_mv 10.1002/crat.200290013
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ispartof Crystal research and technology (1979), 2002-12, Vol.37 (12), p.1352-1359
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1521-4079
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subjects Condensed matter: structure, mechanical and thermal properties
crystal structure
elemental analysis
Exact sciences and technology
Inorganic compounds
Metal complexes
NiII
Physics
Schiff base
Structure of solids and liquids
crystallography
Structure of specific crystalline solids
thermal analysis
trinuclear complex
title Crystal structure analysis of Bis{(N,N′-dimethylformamide)-[μ-bis-N,N′-(2-oxybenzyl)-1,3-propanediaminato](μ-asetato) nickel(II)}nickel(II)
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