Growth and characterization of 4-(2-hydroxyphenylamino)-pent-3-en-2-one single crystals

4‐(2‐hydroxyphenylamino)‐pent‐3‐en‐2‐one (HPAP) was synthesized and single crystals were grown by the solution growth technique using methanol as a solvent. The crystals having orthorhombic symmetry were characterized by single crystal XRD, FTIR spectroscopy, NMR spectroscopy, TGA, DSC and dielectri...

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Bibliographic Details
Published in:Crystal research and technology (1979) 2007-04, Vol.42 (4), p.407-415
Main Authors: Parekh, B. B., Purohit, D. H., Sagayaraj, P., Joshi, H. S., Joshi, M. J.
Format: Article
Language:English
Subjects:
growth from solution
organic compounds
single crystal growth
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Summary:4‐(2‐hydroxyphenylamino)‐pent‐3‐en‐2‐one (HPAP) was synthesized and single crystals were grown by the solution growth technique using methanol as a solvent. The crystals having orthorhombic symmetry were characterized by single crystal XRD, FTIR spectroscopy, NMR spectroscopy, TGA, DSC and dielectric studies. Very less variation in the value of dielectric constant is found for different frequencies of applied field. The crystals were exhibiting positive photoconductivity and poor NLO responses. (© 2007 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)
ISSN:0232-1300
1521-4079
DOI:10.1002/crat.200610836