Microwave-Assisted Preparation of Aryltetrazoleboronate Esters

The addition of azido trimethylsilane to arylnitrileboronate esters is shown to proceed rapidly in dimethoxyethane to give aryltetrazoleboronate esters in moderate to good yields, with dibutyltin oxide as catalyst.

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Bibliographic Details
Published in:Organic letters 2004-09, Vol.6 (19), p.3265-3268
Main Authors: Schulz, Mark J, Coats, Steven J, Hlasta, Dennis J
Format: Article
Language:English
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Description
Summary:The addition of azido trimethylsilane to arylnitrileboronate esters is shown to proceed rapidly in dimethoxyethane to give aryltetrazoleboronate esters in moderate to good yields, with dibutyltin oxide as catalyst.
ISSN:1523-7060
1523-7052
DOI:10.1021/ol048896q