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Spectrophotometric determination of some catecholamine drugs using sodium bismuthate
A novel spectrophotometric method is described for the determination of epinephrine (EP) and norepinephrine (NE). The method is based on the development of a red colour with sodium bismuthate, as a sensitive chromogenic reagent, in aqueous medium at pH 3. Oxidation of these catecholamines produces a...
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| Published in: | Journal of pharmaceutical and biomedical analysis 1998-12, Vol.18 (4), p.877-881 |
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| Main Authors: | , , , |
| Format: | Article |
| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c455t-acf7db9911f46bdabb9301e1d8c1b1740985b9f266e79dd62dd27c72335bc07b3 |
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| cites | cdi_FETCH-LOGICAL-c455t-acf7db9911f46bdabb9301e1d8c1b1740985b9f266e79dd62dd27c72335bc07b3 |
| container_end_page | 881 |
| container_issue | 4 |
| container_start_page | 877 |
| container_title | Journal of pharmaceutical and biomedical analysis |
| container_volume | 18 |
| creator | Sorouraddin, M.H Manzoori, J.L Kargarzadeh, E Haji Shabani, A.M |
| description | A novel spectrophotometric method is described for the determination of epinephrine (EP) and norepinephrine (NE). The method is based on the development of a red colour with sodium bismuthate, as a sensitive chromogenic reagent, in aqueous medium at pH 3. Oxidation of these catecholamines produces aminochrome derivatives which can be measured spectrophotometrically at 486.0 nm. Calibration graphs are linear in the range 4.8–800 (μmol l
−1) for epinephrine bitartarate and 4.8–600 (μmol 1
−1) for norepinephrine bitartarate with detection limits of 0.26 (μmol l
−1) and 2.46 (μmol l
−1) for epinephrine and norepinephrine bitartarate salts, respectively. The method has successfully been applied to determination of these catecholamines in pharmaceutical preparations. |
| doi_str_mv | 10.1016/S0731-7085(98)00271-4 |
| format | article |
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−1) for epinephrine bitartarate and 4.8–600 (μmol 1
−1) for norepinephrine bitartarate with detection limits of 0.26 (μmol l
−1) and 2.46 (μmol l
−1) for epinephrine and norepinephrine bitartarate salts, respectively. The method has successfully been applied to determination of these catecholamines in pharmaceutical preparations.</description><identifier>ISSN: 0731-7085</identifier><identifier>EISSN: 1873-264X</identifier><identifier>DOI: 10.1016/S0731-7085(98)00271-4</identifier><identifier>PMID: 9919991</identifier><identifier>CODEN: JPBADA</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Analysis ; Antioxidants ; Biological and medical sciences ; Bismuth ; Catecholamine ; Catecholamines - analysis ; Chromogenic Compounds ; Epinephrine ; Epinephrine - analysis ; General pharmacology ; Hydrogen-Ion Concentration ; Medical sciences ; Norepinephrine ; Norepinephrine - analysis ; Pharmacology. Drug treatments ; Sodium bismuthate ; Spectrophotometry ; Spectrophotometry, Atomic - methods ; Spectrophotometry, Ultraviolet - methods ; Temperature</subject><ispartof>Journal of pharmaceutical and biomedical analysis, 1998-12, Vol.18 (4), p.877-881</ispartof><rights>1998 Elsevier Science B.V.</rights><rights>1999 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c455t-acf7db9911f46bdabb9301e1d8c1b1740985b9f266e79dd62dd27c72335bc07b3</citedby><cites>FETCH-LOGICAL-c455t-acf7db9911f46bdabb9301e1d8c1b1740985b9f266e79dd62dd27c72335bc07b3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>309,310,314,780,784,789,790,23930,23931,25140,27924,27925</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=1675063$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/9919991$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Sorouraddin, M.H</creatorcontrib><creatorcontrib>Manzoori, J.L</creatorcontrib><creatorcontrib>Kargarzadeh, E</creatorcontrib><creatorcontrib>Haji Shabani, A.M</creatorcontrib><title>Spectrophotometric determination of some catecholamine drugs using sodium bismuthate</title><title>Journal of pharmaceutical and biomedical analysis</title><addtitle>J Pharm Biomed Anal</addtitle><description>A novel spectrophotometric method is described for the determination of epinephrine (EP) and norepinephrine (NE). The method is based on the development of a red colour with sodium bismuthate, as a sensitive chromogenic reagent, in aqueous medium at pH 3. Oxidation of these catecholamines produces aminochrome derivatives which can be measured spectrophotometrically at 486.0 nm. Calibration graphs are linear in the range 4.8–800 (μmol l
−1) for epinephrine bitartarate and 4.8–600 (μmol 1
−1) for norepinephrine bitartarate with detection limits of 0.26 (μmol l
−1) and 2.46 (μmol l
−1) for epinephrine and norepinephrine bitartarate salts, respectively. The method has successfully been applied to determination of these catecholamines in pharmaceutical preparations.</description><subject>Analysis</subject><subject>Antioxidants</subject><subject>Biological and medical sciences</subject><subject>Bismuth</subject><subject>Catecholamine</subject><subject>Catecholamines - analysis</subject><subject>Chromogenic Compounds</subject><subject>Epinephrine</subject><subject>Epinephrine - analysis</subject><subject>General pharmacology</subject><subject>Hydrogen-Ion Concentration</subject><subject>Medical sciences</subject><subject>Norepinephrine</subject><subject>Norepinephrine - analysis</subject><subject>Pharmacology. Drug treatments</subject><subject>Sodium bismuthate</subject><subject>Spectrophotometry</subject><subject>Spectrophotometry, Atomic - methods</subject><subject>Spectrophotometry, Ultraviolet - methods</subject><subject>Temperature</subject><issn>0731-7085</issn><issn>1873-264X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1998</creationdate><recordtype>article</recordtype><recordid>eNqFkMtKxDAUhoMoOl4eQehCRBfVpG2SZiUi3kBwoYK7kMupE2mbMUkF396MM-jSxeEs_u9c-BA6JPiMYMLOnzCvSclxS09Ee4pxxUnZbKAZaXldVqx53USzX2QH7cb4jjGmRDTbaFsIInLN0PPTAkwKfjH3yQ-QgjOFhQRhcKNKzo-F74qYk8KoBGbue5UTKGyY3mIxRTe-5di6aSi0i8OU5hnbR1ud6iMcrPseerm5fr66Kx8eb--vLh9K01CaSmU6bnV-g3QN01ZpLWpMgNjWEE14g0VLtegqxoALa1llbcUNr-qaaoO5rvfQ8WrvIviPCWKSg4sG-l6N4KcomSANo4JnkK5AE3yMATq5CG5Q4UsSLJc25Y9NuVQlRSt_bMomzx2uD0x6APs7tdaX86N1rqJRfRfUaFz8W844xazO2MUKgyzj00GQ0TgYDVgXsn1pvfvnkW-k9JMw</recordid><startdate>19981201</startdate><enddate>19981201</enddate><creator>Sorouraddin, M.H</creator><creator>Manzoori, J.L</creator><creator>Kargarzadeh, E</creator><creator>Haji Shabani, A.M</creator><general>Elsevier B.V</general><general>Elsevier Science</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>19981201</creationdate><title>Spectrophotometric determination of some catecholamine drugs using sodium bismuthate</title><author>Sorouraddin, M.H ; Manzoori, J.L ; Kargarzadeh, E ; Haji Shabani, A.M</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c455t-acf7db9911f46bdabb9301e1d8c1b1740985b9f266e79dd62dd27c72335bc07b3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1998</creationdate><topic>Analysis</topic><topic>Antioxidants</topic><topic>Biological and medical sciences</topic><topic>Bismuth</topic><topic>Catecholamine</topic><topic>Catecholamines - analysis</topic><topic>Chromogenic Compounds</topic><topic>Epinephrine</topic><topic>Epinephrine - analysis</topic><topic>General pharmacology</topic><topic>Hydrogen-Ion Concentration</topic><topic>Medical sciences</topic><topic>Norepinephrine</topic><topic>Norepinephrine - analysis</topic><topic>Pharmacology. Drug treatments</topic><topic>Sodium bismuthate</topic><topic>Spectrophotometry</topic><topic>Spectrophotometry, Atomic - methods</topic><topic>Spectrophotometry, Ultraviolet - methods</topic><topic>Temperature</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Sorouraddin, M.H</creatorcontrib><creatorcontrib>Manzoori, J.L</creatorcontrib><creatorcontrib>Kargarzadeh, E</creatorcontrib><creatorcontrib>Haji Shabani, A.M</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of pharmaceutical and biomedical analysis</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Sorouraddin, M.H</au><au>Manzoori, J.L</au><au>Kargarzadeh, E</au><au>Haji Shabani, A.M</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Spectrophotometric determination of some catecholamine drugs using sodium bismuthate</atitle><jtitle>Journal of pharmaceutical and biomedical analysis</jtitle><addtitle>J Pharm Biomed Anal</addtitle><date>1998-12-01</date><risdate>1998</risdate><volume>18</volume><issue>4</issue><spage>877</spage><epage>881</epage><pages>877-881</pages><issn>0731-7085</issn><eissn>1873-264X</eissn><coden>JPBADA</coden><abstract>A novel spectrophotometric method is described for the determination of epinephrine (EP) and norepinephrine (NE). The method is based on the development of a red colour with sodium bismuthate, as a sensitive chromogenic reagent, in aqueous medium at pH 3. Oxidation of these catecholamines produces aminochrome derivatives which can be measured spectrophotometrically at 486.0 nm. Calibration graphs are linear in the range 4.8–800 (μmol l
−1) for epinephrine bitartarate and 4.8–600 (μmol 1
−1) for norepinephrine bitartarate with detection limits of 0.26 (μmol l
−1) and 2.46 (μmol l
−1) for epinephrine and norepinephrine bitartarate salts, respectively. The method has successfully been applied to determination of these catecholamines in pharmaceutical preparations.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><pmid>9919991</pmid><doi>10.1016/S0731-7085(98)00271-4</doi><tpages>5</tpages></addata></record> |
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| ispartof | Journal of pharmaceutical and biomedical analysis, 1998-12, Vol.18 (4), p.877-881 |
| issn | 0731-7085 1873-264X |
| language | eng |
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| source | ScienceDirect Freedom Collection 2022-2024 |
| subjects | Analysis Antioxidants Biological and medical sciences Bismuth Catecholamine Catecholamines - analysis Chromogenic Compounds Epinephrine Epinephrine - analysis General pharmacology Hydrogen-Ion Concentration Medical sciences Norepinephrine Norepinephrine - analysis Pharmacology. Drug treatments Sodium bismuthate Spectrophotometry Spectrophotometry, Atomic - methods Spectrophotometry, Ultraviolet - methods Temperature |
| title | Spectrophotometric determination of some catecholamine drugs using sodium bismuthate |
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