Separation of substituted fullerenes using non-aqueous reversed-phase liquid chromatography–mass spectrometry

A simple non-aqueous reversed-phase separation HPLC–MS method has been developed to allow for the rapid screening and separation of fullerenes and substituted fullerenes. This procedure provides confirmation that the proposed substitution methodology for the fullerene is not only successful but that...

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Bibliographic Details
Published in:Journal of Chromatography A 2008-02, Vol.1181 (1), p.159-161
Main Authors: Deye, Joel R., Shiveley, Amber N., Oehrle, Stuart A., Walters, Keith A.
Format: Article
Language:English
Subjects:
Analytical chemistry
Chemistry
Chromatographic methods and physical methods associated with chromatography
Chromatography, High Pressure Liquid - methods
Diels–Alder reaction
Exact sciences and technology
Fullerenes - isolation & purification
HPLC
LC/MS
Mass Spectrometry - methods
Normal-phase
Other chromatographic methods
Substituted fullerenes
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Description
Summary:A simple non-aqueous reversed-phase separation HPLC–MS method has been developed to allow for the rapid screening and separation of fullerenes and substituted fullerenes. This procedure provides confirmation that the proposed substitution methodology for the fullerene is not only successful but that multiple substitution products are obtained. The methodology is being expanded to analyze other substituted fullerene product mixtures.
ISSN:0021-9673
DOI:10.1016/j.chroma.2007.12.052