Spectroscopic characterization of 6-hydroxy and 1-methyl-6-hydroxybicyclo[2.2.2]octan-2-one ethylene acetals and ethylene dithioacetals

6‐endo‐ and 6‐exo‐Hydroxybicyclo[2.2.2]octan‐2‐one and 1‐methyl‐6‐endo‐ and 6‐exo‐hydroxybicyclo[2.2.2]octan‐2‐one ethylene acetals and ethylene dithioacetals 1–4 have been characterized by 1D and 2D NMR methods. Copyright © 2007 John Wiley & Sons, Ltd.

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Bibliographic Details
Published in:Magnetic resonance in chemistry 2007-05, Vol.45 (5), p.420-423
Main Authors: Leonelli, Francesca, Garofalo, Barbara, La Bella, Angela, Lasta, Ermanno, Ceccacci, Francesca, Migneco, Luisa M., Marini Bettolo, Rinaldo
Format: Article
Language:English
Subjects:
13C
6-hydroxybicyclo[2.2.2]octan-2-one
Acetals - chemistry
Bridged Bicyclo Compounds, Heterocyclic - chemistry
ethylene acetals
ethylene dithioacetals
Ethylenes - chemistry
Magnetic Resonance Spectroscopy
Molecular Structure
NMR
Stereoisomerism
Sulfur - chemistry
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Description
Summary:6‐endo‐ and 6‐exo‐Hydroxybicyclo[2.2.2]octan‐2‐one and 1‐methyl‐6‐endo‐ and 6‐exo‐hydroxybicyclo[2.2.2]octan‐2‐one ethylene acetals and ethylene dithioacetals 1–4 have been characterized by 1D and 2D NMR methods. Copyright © 2007 John Wiley & Sons, Ltd.
ISSN:0749-1581
1097-458X
DOI:10.1002/mrc.1964