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Determination of Biogenic Amines in Squid and White Prawn by High-Performance Liquid Chromatography with Postcolumn Derivatization
A simple method was developed for the determination of biogenic amines in aquatic food products using a reverse-phase high-performance liquid chromatography with postcolumn automatic o-phthalaldehyde derivatization and fluorescence detection. The linearity, repeatability, and recovery of the method...
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Published in: | Journal of agricultural and food chemistry 2007-04, Vol.55 (8), p.3083-3088 |
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container_end_page | 3088 |
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container_start_page | 3083 |
container_title | Journal of agricultural and food chemistry |
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creator | Zhao, Qing-Xi Xu, Jie Xue, Chang-Hu Sheng, Wen-Jing Gao, Rui-Chang Xue, Yong Li, Zhao-Jie |
description | A simple method was developed for the determination of biogenic amines in aquatic food products using a reverse-phase high-performance liquid chromatography with postcolumn automatic o-phthalaldehyde derivatization and fluorescence detection. The linearity, repeatability, and recovery of the method for seven amines (tyramine, putrescine, cadaverine, histamine, agmatine, spermidine, and spermine) were evaluated. This optimized method was applied to detect biogenic amines in squid and white prawn during refrigerated storage. Sensory analysis, pH value, and total volatile base nitrogen value were combined to evaluate the freshness quality of these two raw materials. Agmatine and cadaverine in squid, cadaverine, and putrescine in white prawn were the most obviously changed amines during the storage at two different temperatures, and these biogenic amines could be the effective quality indicators for the freshness of the raw aquatic materials. Keywords: Biogenic amine; HPLC; postcolumn derivatization; squid; white prawn |
doi_str_mv | 10.1021/jf062887+ |
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The linearity, repeatability, and recovery of the method for seven amines (tyramine, putrescine, cadaverine, histamine, agmatine, spermidine, and spermine) were evaluated. This optimized method was applied to detect biogenic amines in squid and white prawn during refrigerated storage. Sensory analysis, pH value, and total volatile base nitrogen value were combined to evaluate the freshness quality of these two raw materials. Agmatine and cadaverine in squid, cadaverine, and putrescine in white prawn were the most obviously changed amines during the storage at two different temperatures, and these biogenic amines could be the effective quality indicators for the freshness of the raw aquatic materials. Keywords: Biogenic amine; HPLC; postcolumn derivatization; squid; white prawn</description><identifier>ISSN: 0021-8561</identifier><identifier>EISSN: 1520-5118</identifier><identifier>DOI: 10.1021/jf062887+</identifier><identifier>PMID: 17381105</identifier><identifier>CODEN: JAFCAU</identifier><language>eng</language><publisher>Washington, DC: American Chemical Society</publisher><subject>Animals ; biogenic amines ; Biogenic Amines - analysis ; Biological and medical sciences ; Chromatography, High Pressure Liquid - methods ; Cold Temperature ; Crustacea - chemistry ; Decapodiformes - chemistry ; Fish and seafood industries ; food composition ; Food industries ; Food Preservation ; food storage ; Fundamental and applied biological sciences. Psychology ; Illes argentinus ; Litopenaeus vannamei ; Reproducibility of Results ; reversed-phase high performance liquid chromatography ; shrimp ; squid ; storage temperature</subject><ispartof>Journal of agricultural and food chemistry, 2007-04, Vol.55 (8), p.3083-3088</ispartof><rights>Copyright © 2007 American Chemical Society</rights><rights>2007 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-a433t-33a76f29fc6de97e7e095517c362a1395fcb2efb2409b73857ddaf649ba498703</citedby><cites>FETCH-LOGICAL-a433t-33a76f29fc6de97e7e095517c362a1395fcb2efb2409b73857ddaf649ba498703</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=18717623$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/17381105$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Zhao, Qing-Xi</creatorcontrib><creatorcontrib>Xu, Jie</creatorcontrib><creatorcontrib>Xue, Chang-Hu</creatorcontrib><creatorcontrib>Sheng, Wen-Jing</creatorcontrib><creatorcontrib>Gao, Rui-Chang</creatorcontrib><creatorcontrib>Xue, Yong</creatorcontrib><creatorcontrib>Li, Zhao-Jie</creatorcontrib><title>Determination of Biogenic Amines in Squid and White Prawn by High-Performance Liquid Chromatography with Postcolumn Derivatization</title><title>Journal of agricultural and food chemistry</title><addtitle>J. Agric. Food Chem</addtitle><description>A simple method was developed for the determination of biogenic amines in aquatic food products using a reverse-phase high-performance liquid chromatography with postcolumn automatic o-phthalaldehyde derivatization and fluorescence detection. The linearity, repeatability, and recovery of the method for seven amines (tyramine, putrescine, cadaverine, histamine, agmatine, spermidine, and spermine) were evaluated. This optimized method was applied to detect biogenic amines in squid and white prawn during refrigerated storage. Sensory analysis, pH value, and total volatile base nitrogen value were combined to evaluate the freshness quality of these two raw materials. Agmatine and cadaverine in squid, cadaverine, and putrescine in white prawn were the most obviously changed amines during the storage at two different temperatures, and these biogenic amines could be the effective quality indicators for the freshness of the raw aquatic materials. Keywords: Biogenic amine; HPLC; postcolumn derivatization; squid; white prawn</description><subject>Animals</subject><subject>biogenic amines</subject><subject>Biogenic Amines - analysis</subject><subject>Biological and medical sciences</subject><subject>Chromatography, High Pressure Liquid - methods</subject><subject>Cold Temperature</subject><subject>Crustacea - chemistry</subject><subject>Decapodiformes - chemistry</subject><subject>Fish and seafood industries</subject><subject>food composition</subject><subject>Food industries</subject><subject>Food Preservation</subject><subject>food storage</subject><subject>Fundamental and applied biological sciences. Psychology</subject><subject>Illes argentinus</subject><subject>Litopenaeus vannamei</subject><subject>Reproducibility of Results</subject><subject>reversed-phase high performance liquid chromatography</subject><subject>shrimp</subject><subject>squid</subject><subject>storage temperature</subject><issn>0021-8561</issn><issn>1520-5118</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2007</creationdate><recordtype>article</recordtype><recordid>eNqF0c9v0zAUB_AIgVgZHPgHwAdASChgx_GPHEcHFFGJiG4CcbEcx25dEruzE0Y58pfjLYUdOHCy5PfRe3rvm2UPEXyJYIFebQ2kBefsxa1shkgBc4IQv53NYCrmnFB0lN2LcQsh5ITBu9kRYpgjBMks-3WqBx166-RgvQPegNfWr7WzCpykXx2BdWB1MdoWSNeCzxs7aFAHeelAswcLu97ktQ7Gh146pcHSXtP5JvheDn4d5G6zB5d22IDax0H5buwdONXBfk8Df14PvZ_dMbKL-sHhPc7O3745my_y5cd37-cny1yWGA85xpJRU1RG0VZXTDMNK0IQU5gWEuGKGNUU2jRFCasm7UdY20pDy6qRZcUZxMfZs6nvLviLUcdB9DYq3XXSaT9GkQgtKa_-CwvIaEkgS_D5BFXwMQZtxC7YXoa9QFBcJSP-JJPoo0PPsel1ewMPSSTw9ABkVLIzId3TxhvHGWK0wMnlk7Nx0D_-1mX4JijDjIizeiWq5YJ--PK1Fp-Sfzx5I72Q65B6nq8KiDBMWzBOriY_mYRUUWz9GFxK4d8NfgN5rrp_</recordid><startdate>20070418</startdate><enddate>20070418</enddate><creator>Zhao, Qing-Xi</creator><creator>Xu, Jie</creator><creator>Xue, Chang-Hu</creator><creator>Sheng, Wen-Jing</creator><creator>Gao, Rui-Chang</creator><creator>Xue, Yong</creator><creator>Li, Zhao-Jie</creator><general>American Chemical Society</general><scope>FBQ</scope><scope>BSCLL</scope><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>F1W</scope><scope>H95</scope><scope>L.G</scope><scope>7X8</scope></search><sort><creationdate>20070418</creationdate><title>Determination of Biogenic Amines in Squid and White Prawn by High-Performance Liquid Chromatography with Postcolumn Derivatization</title><author>Zhao, Qing-Xi ; Xu, Jie ; Xue, Chang-Hu ; Sheng, Wen-Jing ; Gao, Rui-Chang ; Xue, Yong ; Li, Zhao-Jie</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-a433t-33a76f29fc6de97e7e095517c362a1395fcb2efb2409b73857ddaf649ba498703</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2007</creationdate><topic>Animals</topic><topic>biogenic amines</topic><topic>Biogenic Amines - analysis</topic><topic>Biological and medical sciences</topic><topic>Chromatography, High Pressure Liquid - methods</topic><topic>Cold Temperature</topic><topic>Crustacea - chemistry</topic><topic>Decapodiformes - chemistry</topic><topic>Fish and seafood industries</topic><topic>food composition</topic><topic>Food industries</topic><topic>Food Preservation</topic><topic>food storage</topic><topic>Fundamental and applied biological sciences. Psychology</topic><topic>Illes argentinus</topic><topic>Litopenaeus vannamei</topic><topic>Reproducibility of Results</topic><topic>reversed-phase high performance liquid chromatography</topic><topic>shrimp</topic><topic>squid</topic><topic>storage temperature</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Zhao, Qing-Xi</creatorcontrib><creatorcontrib>Xu, Jie</creatorcontrib><creatorcontrib>Xue, Chang-Hu</creatorcontrib><creatorcontrib>Sheng, Wen-Jing</creatorcontrib><creatorcontrib>Gao, Rui-Chang</creatorcontrib><creatorcontrib>Xue, Yong</creatorcontrib><creatorcontrib>Li, Zhao-Jie</creatorcontrib><collection>AGRIS</collection><collection>Istex</collection><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>ASFA: Aquatic Sciences and Fisheries Abstracts</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) 1: Biological Sciences & Living Resources</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) Professional</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of agricultural and food chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Zhao, Qing-Xi</au><au>Xu, Jie</au><au>Xue, Chang-Hu</au><au>Sheng, Wen-Jing</au><au>Gao, Rui-Chang</au><au>Xue, Yong</au><au>Li, Zhao-Jie</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Determination of Biogenic Amines in Squid and White Prawn by High-Performance Liquid Chromatography with Postcolumn Derivatization</atitle><jtitle>Journal of agricultural and food chemistry</jtitle><addtitle>J. Agric. Food Chem</addtitle><date>2007-04-18</date><risdate>2007</risdate><volume>55</volume><issue>8</issue><spage>3083</spage><epage>3088</epage><pages>3083-3088</pages><issn>0021-8561</issn><eissn>1520-5118</eissn><coden>JAFCAU</coden><abstract>A simple method was developed for the determination of biogenic amines in aquatic food products using a reverse-phase high-performance liquid chromatography with postcolumn automatic o-phthalaldehyde derivatization and fluorescence detection. The linearity, repeatability, and recovery of the method for seven amines (tyramine, putrescine, cadaverine, histamine, agmatine, spermidine, and spermine) were evaluated. This optimized method was applied to detect biogenic amines in squid and white prawn during refrigerated storage. Sensory analysis, pH value, and total volatile base nitrogen value were combined to evaluate the freshness quality of these two raw materials. Agmatine and cadaverine in squid, cadaverine, and putrescine in white prawn were the most obviously changed amines during the storage at two different temperatures, and these biogenic amines could be the effective quality indicators for the freshness of the raw aquatic materials. Keywords: Biogenic amine; HPLC; postcolumn derivatization; squid; white prawn</abstract><cop>Washington, DC</cop><pub>American Chemical Society</pub><pmid>17381105</pmid><doi>10.1021/jf062887+</doi><tpages>6</tpages></addata></record> |
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subjects | Animals biogenic amines Biogenic Amines - analysis Biological and medical sciences Chromatography, High Pressure Liquid - methods Cold Temperature Crustacea - chemistry Decapodiformes - chemistry Fish and seafood industries food composition Food industries Food Preservation food storage Fundamental and applied biological sciences. Psychology Illes argentinus Litopenaeus vannamei Reproducibility of Results reversed-phase high performance liquid chromatography shrimp squid storage temperature |
title | Determination of Biogenic Amines in Squid and White Prawn by High-Performance Liquid Chromatography with Postcolumn Derivatization |
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