Measurement of magnetic susceptibility and calculation of shape factor of NMR samples

A method for accurate measurement of magnetic susceptibility and determination of the shape factor in an NMR tube is shown. The combination of accurate shape factor determination with susceptibility measurement leads to improved accuracy when measuring chemical shift. This is important for comparing...

Full description

Saved in:
Bibliographic Details
Published in:Journal of magnetic resonance (1997) 2006-02, Vol.178 (2), p.237-247
Main Author: Hoffman, Roy E.
Format: Article
Language:English
Subjects:
BMS shift
Chemical shift
Shape factor
Susceptibility
Citations: Items that this one cites
Items that cite this one
Online Access:Get full text
Tags: Add Tag
No Tags, Be the first to tag this record!
cited_by cdi_FETCH-LOGICAL-c417t-c77f3d73a0810f380cfe676ebeaa85f81b8b849bfd7f4911e2e7e7569d3658353
cites cdi_FETCH-LOGICAL-c417t-c77f3d73a0810f380cfe676ebeaa85f81b8b849bfd7f4911e2e7e7569d3658353
container_end_page 247
container_issue 2
container_start_page 237
container_title Journal of magnetic resonance (1997)
container_volume 178
creator Hoffman, Roy E.
description A method for accurate measurement of magnetic susceptibility and determination of the shape factor in an NMR tube is shown. The combination of accurate shape factor determination with susceptibility measurement leads to improved accuracy when measuring chemical shift. This is important for comparing samples in different solvents or under different conditions, such as temperature, solvent, and pH.
doi_str_mv 10.1016/j.jmr.2005.09.009
format article
fullrecord <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_70704385</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><els_id>S1090780705003125</els_id><sourcerecordid>70704385</sourcerecordid><originalsourceid>FETCH-LOGICAL-c417t-c77f3d73a0810f380cfe676ebeaa85f81b8b849bfd7f4911e2e7e7569d3658353</originalsourceid><addsrcrecordid>eNp9kE1LxDAQhoMo7rr6A7xIT95aJ9uPpHiSxS_YVRD3HNJ0oin9MkmF_fe27oI3TzMDz7zMPIRcUogo0OymiqrGRkuANII8AsiPyJxCnoXA0-z4t4eQcWAzcuZcBUBpyuCUzGi2TOM0hjnZblC6wWKDrQ86HTTyo0VvVOAGp7D3pjC18btAtmWgZK2GWnrTtRPqPmWPgZbKd3aaXzZvgZNNX6M7Jyda1g4vDnVBtg_376uncP36-Ly6W4cqocyHijEdlyyWwCnomIPSmLEMC5SSp5rTghc8yQtdMp3klOISGbI0y8s4S_n4wIJc73N7230N6LxozHh2XcsWu8EJBgySmE8g3YPKds5Z1KK3ppF2JyiIyaWoxOhSTC4F5GJ0Oe5cHcKHosHyb-MgbwRu9wCOL34btMIpg63C0lhUXpSd-Sf-BzWuhSs</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>70704385</pqid></control><display><type>article</type><title>Measurement of magnetic susceptibility and calculation of shape factor of NMR samples</title><source>ScienceDirect Journals</source><creator>Hoffman, Roy E.</creator><creatorcontrib>Hoffman, Roy E.</creatorcontrib><description>A method for accurate measurement of magnetic susceptibility and determination of the shape factor in an NMR tube is shown. The combination of accurate shape factor determination with susceptibility measurement leads to improved accuracy when measuring chemical shift. This is important for comparing samples in different solvents or under different conditions, such as temperature, solvent, and pH.</description><identifier>ISSN: 1090-7807</identifier><identifier>EISSN: 1096-0856</identifier><identifier>DOI: 10.1016/j.jmr.2005.09.009</identifier><identifier>PMID: 16253530</identifier><language>eng</language><publisher>United States: Elsevier Inc</publisher><subject>BMS shift ; Chemical shift ; Shape factor ; Susceptibility</subject><ispartof>Journal of magnetic resonance (1997), 2006-02, Vol.178 (2), p.237-247</ispartof><rights>2005 Elsevier Inc.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c417t-c77f3d73a0810f380cfe676ebeaa85f81b8b849bfd7f4911e2e7e7569d3658353</citedby><cites>FETCH-LOGICAL-c417t-c77f3d73a0810f380cfe676ebeaa85f81b8b849bfd7f4911e2e7e7569d3658353</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/16253530$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Hoffman, Roy E.</creatorcontrib><title>Measurement of magnetic susceptibility and calculation of shape factor of NMR samples</title><title>Journal of magnetic resonance (1997)</title><addtitle>J Magn Reson</addtitle><description>A method for accurate measurement of magnetic susceptibility and determination of the shape factor in an NMR tube is shown. The combination of accurate shape factor determination with susceptibility measurement leads to improved accuracy when measuring chemical shift. This is important for comparing samples in different solvents or under different conditions, such as temperature, solvent, and pH.</description><subject>BMS shift</subject><subject>Chemical shift</subject><subject>Shape factor</subject><subject>Susceptibility</subject><issn>1090-7807</issn><issn>1096-0856</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2006</creationdate><recordtype>article</recordtype><recordid>eNp9kE1LxDAQhoMo7rr6A7xIT95aJ9uPpHiSxS_YVRD3HNJ0oin9MkmF_fe27oI3TzMDz7zMPIRcUogo0OymiqrGRkuANII8AsiPyJxCnoXA0-z4t4eQcWAzcuZcBUBpyuCUzGi2TOM0hjnZblC6wWKDrQ86HTTyo0VvVOAGp7D3pjC18btAtmWgZK2GWnrTtRPqPmWPgZbKd3aaXzZvgZNNX6M7Jyda1g4vDnVBtg_376uncP36-Ly6W4cqocyHijEdlyyWwCnomIPSmLEMC5SSp5rTghc8yQtdMp3klOISGbI0y8s4S_n4wIJc73N7230N6LxozHh2XcsWu8EJBgySmE8g3YPKds5Z1KK3ppF2JyiIyaWoxOhSTC4F5GJ0Oe5cHcKHosHyb-MgbwRu9wCOL34btMIpg63C0lhUXpSd-Sf-BzWuhSs</recordid><startdate>20060201</startdate><enddate>20060201</enddate><creator>Hoffman, Roy E.</creator><general>Elsevier Inc</general><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20060201</creationdate><title>Measurement of magnetic susceptibility and calculation of shape factor of NMR samples</title><author>Hoffman, Roy E.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c417t-c77f3d73a0810f380cfe676ebeaa85f81b8b849bfd7f4911e2e7e7569d3658353</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2006</creationdate><topic>BMS shift</topic><topic>Chemical shift</topic><topic>Shape factor</topic><topic>Susceptibility</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Hoffman, Roy E.</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of magnetic resonance (1997)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Hoffman, Roy E.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Measurement of magnetic susceptibility and calculation of shape factor of NMR samples</atitle><jtitle>Journal of magnetic resonance (1997)</jtitle><addtitle>J Magn Reson</addtitle><date>2006-02-01</date><risdate>2006</risdate><volume>178</volume><issue>2</issue><spage>237</spage><epage>247</epage><pages>237-247</pages><issn>1090-7807</issn><eissn>1096-0856</eissn><abstract>A method for accurate measurement of magnetic susceptibility and determination of the shape factor in an NMR tube is shown. The combination of accurate shape factor determination with susceptibility measurement leads to improved accuracy when measuring chemical shift. This is important for comparing samples in different solvents or under different conditions, such as temperature, solvent, and pH.</abstract><cop>United States</cop><pub>Elsevier Inc</pub><pmid>16253530</pmid><doi>10.1016/j.jmr.2005.09.009</doi><tpages>11</tpages></addata></record>
fulltext fulltext
identifier ISSN: 1090-7807
ispartof Journal of magnetic resonance (1997), 2006-02, Vol.178 (2), p.237-247
issn 1090-7807
1096-0856
language eng
recordid cdi_proquest_miscellaneous_70704385
source ScienceDirect Journals
subjects BMS shift
Chemical shift
Shape factor
Susceptibility
title Measurement of magnetic susceptibility and calculation of shape factor of NMR samples
url http://sfxeu10.hosted.exlibrisgroup.com/loughborough?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-04T19%3A07%3A07IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Measurement%20of%20magnetic%20susceptibility%20and%20calculation%20of%20shape%20factor%20of%20NMR%20samples&rft.jtitle=Journal%20of%20magnetic%20resonance%20(1997)&rft.au=Hoffman,%20Roy%20E.&rft.date=2006-02-01&rft.volume=178&rft.issue=2&rft.spage=237&rft.epage=247&rft.pages=237-247&rft.issn=1090-7807&rft.eissn=1096-0856&rft_id=info:doi/10.1016/j.jmr.2005.09.009&rft_dat=%3Cproquest_cross%3E70704385%3C/proquest_cross%3E%3Cgrp_id%3Ecdi_FETCH-LOGICAL-c417t-c77f3d73a0810f380cfe676ebeaa85f81b8b849bfd7f4911e2e7e7569d3658353%3C/grp_id%3E%3Coa%3E%3C/oa%3E%3Curl%3E%3C/url%3E&rft_id=info:oai/&rft_pqid=70704385&rft_id=info:pmid/16253530&rfr_iscdi=true