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Characterization of partially transesterified poly(β-hydroxyalkanoate)s by matrix-assisted laser desorption/ionization time-of-flight mass spectrometry

Matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOFMS) was used for the characterization of a partially transesterified poly(beta-hydroxyalkanoate) (PHA), a polymer produced by the bacterial strain Alcaligenes eutrophus with saponified vegetable oils as the sole c...

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Bibliographic Details
Published in:Journal of AOAC International 2001-07, Vol.84 (4), p.1109-1115
Main Authors: SAEED, Kamal A, AYORINDE, Folahan O, ERIBO, Broderick E, GORDON, Michael, COLLIER, Ledelle
Format: Article
Language:English
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Summary:Matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOFMS) was used for the characterization of a partially transesterified poly(beta-hydroxyalkanoate) (PHA), a polymer produced by the bacterial strain Alcaligenes eutrophus with saponified vegetable oils as the sole carbon sources. The transesterification was carried out separately under acidic and basic conditions to obtain PHA oligomers weighing
ISSN:1060-3271
1944-7922
DOI:10.1093/jaoac/84.4.1109