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Determination of ampicillin and amoxycillin by flow injection chemiluminescence method based on their enhancing effects on the luminol-periodate reaction

In this work, a new flow injection chemiluminescence method is described for the determination of ampicillin and amoxycillin. The method is based on the strong enhancing effects of these antibiotics on the luminol–periodate reaction. The present method allows the measurements of ampicillin in the ra...

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Published in:	Luminescence (Chichester, England) England), 2003-11, Vol.18 (6), p.313-317
Main Authors:	Li, Yinhuan, Tang, Yuhai, Yao, Hong, Fu, Junmei
Format:	Article
Language:	English
Subjects:	Amoxicillin - analysis amoxycillin ampicillin Ampicillin - analysis Anti-Bacterial Agents - analysis chemiluminescence flow injection Flow Injection Analysis - methods Indicators and Reagents Luminescent Measurements Luminol - chemistry Periodic Acid - chemistry
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container_title	Luminescence (Chichester, England)
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creator	Li, Yinhuan Tang, Yuhai Yao, Hong Fu, Junmei
description	In this work, a new flow injection chemiluminescence method is described for the determination of ampicillin and amoxycillin. The method is based on the strong enhancing effects of these antibiotics on the luminol–periodate reaction. The present method allows the measurements of ampicillin in the range 0.02–1.0 mg/L range and amoxycillin in the range 0.1–10.0 mg/L range with the relative standard deviations within 0.8–2.0%. The sampling frequency was calculated about 90/h. The method was successfully applied to the determination of ampicillin and amoxycillin in pharmaceutical preparations. A brief discussion on the possible chemiluminescence reaction mechanism is presented. Copyright © 2003 John Wiley & Sons, Ltd.
doi_str_mv	10.1002/bio.741
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Copyright © 2003 John Wiley & Sons, Ltd.</description><subject>Amoxicillin - analysis</subject><subject>amoxycillin</subject><subject>ampicillin</subject><subject>Ampicillin - analysis</subject><subject>Anti-Bacterial Agents - analysis</subject><subject>chemiluminescence</subject><subject>flow injection</subject><subject>Flow Injection Analysis - methods</subject><subject>Indicators and Reagents</subject><subject>Luminescent Measurements</subject><subject>Luminol - chemistry</subject><subject>Periodic Acid - chemistry</subject><issn>1522-7235</issn><issn>1522-7243</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2003</creationdate><recordtype>article</recordtype><recordid>eNp1kctu1DAUhi0EoqUg3gB5BQuU4lvi8ZK2UCpVVIhLl5bjHDMujj21M2rnUXhbzCQqK1b2kb__k45_hF5SckwJYe96n46loI_QIW0ZayQT_PHDnbcH6FkpN4SQruvUU3RARaeEoOoQ_T6DCfLoo5l8ijg5bMaNtz4EH7GJQx3T_W6Z-x12Id1hH2_A7nm7htGHbc1DsRAt4BGmdRpwbwoMuBLTGnzGENcmWh9_YnCuZsvyhPfZFJoNZJ8GMwHOYPbu5-iJM6HAi-U8Qt8_fvh2-qm5vDq_OH1_2VjeUtqsjBpWlLMWlFLQO2VEx5RUZuC9c8IBNQBMgYHeUtOBUcqyFXApqWCESX6EXs_eTU63WyiTHn3dJQQTIW2LrtxKSEkq-GYGbU6lZHB6k_1o8k5Tov-2oGsLurZQyVeLctuPMPzjlm-vwNsZuPMBdv_z6JOLq1nXzLQvE9w_0Cb_0p3kstXXn8_1j_bk6_UZbfUX_gfZXaPu</recordid><startdate>200311</startdate><enddate>200311</enddate><creator>Li, Yinhuan</creator><creator>Tang, Yuhai</creator><creator>Yao, Hong</creator><creator>Fu, Junmei</creator><general>John Wiley & Sons, Ltd</general><scope>BSCLL</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>200311</creationdate><title>Determination of ampicillin and amoxycillin by flow injection chemiluminescence method based on their enhancing effects on the luminol-periodate reaction</title><author>Li, Yinhuan ; Tang, Yuhai ; Yao, Hong ; Fu, Junmei</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3511-8a9d81325e999ebf9a462979ad3bff4fe1aee29eaebc1a6ea99c28e3771420273</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2003</creationdate><topic>Amoxicillin - analysis</topic><topic>amoxycillin</topic><topic>ampicillin</topic><topic>Ampicillin - analysis</topic><topic>Anti-Bacterial Agents - analysis</topic><topic>chemiluminescence</topic><topic>flow injection</topic><topic>Flow Injection Analysis - methods</topic><topic>Indicators and Reagents</topic><topic>Luminescent Measurements</topic><topic>Luminol - chemistry</topic><topic>Periodic Acid - chemistry</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Li, Yinhuan</creatorcontrib><creatorcontrib>Tang, Yuhai</creatorcontrib><creatorcontrib>Yao, Hong</creatorcontrib><creatorcontrib>Fu, Junmei</creatorcontrib><collection>Istex</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Luminescence (Chichester, England)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Li, Yinhuan</au><au>Tang, Yuhai</au><au>Yao, Hong</au><au>Fu, Junmei</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Determination of ampicillin and amoxycillin by flow injection chemiluminescence method based on their enhancing effects on the luminol-periodate reaction</atitle><jtitle>Luminescence (Chichester, England)</jtitle><addtitle>Luminescence</addtitle><date>2003-11</date><risdate>2003</risdate><volume>18</volume><issue>6</issue><spage>313</spage><epage>317</epage><pages>313-317</pages><issn>1522-7235</issn><eissn>1522-7243</eissn><abstract>In this work, a new flow injection chemiluminescence method is described for the determination of ampicillin and amoxycillin. 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source	Wiley-Blackwell Read & Publish Collection
subjects	Amoxicillin - analysis amoxycillin ampicillin Ampicillin - analysis Anti-Bacterial Agents - analysis chemiluminescence flow injection Flow Injection Analysis - methods Indicators and Reagents Luminescent Measurements Luminol - chemistry Periodic Acid - chemistry
title	Determination of ampicillin and amoxycillin by flow injection chemiluminescence method based on their enhancing effects on the luminol-periodate reaction
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