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Na2Fe(CN)5(NO)·2D2O at 11 and 293 K by X-ray, and at 15 K by neutron diffraction

The crystal structure of Na2Fe(CN)5(NO)·2D2O, disodium penta­cyano­nitro­syl­ferrate(III) bis­(dideuterium oxide), has been determined by X‐ray diffraction at 11 and 293 K, and by neutron diffraction at 15 K. The accurate and extensive data sets lead to more precise determinations than are available...

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Bibliographic Details
Published in:Acta crystallographica. Section C, Crystal structure communications Crystal structure communications, 2000-11, Vol.56 (11), p.1289-1291
Main Authors: Schultz, Arthur J., Figgis, Brian N., Sobolev, Alexandre N.
Format: Article
Language:English
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Summary:The crystal structure of Na2Fe(CN)5(NO)·2D2O, disodium penta­cyano­nitro­syl­ferrate(III) bis­(dideuterium oxide), has been determined by X‐ray diffraction at 11 and 293 K, and by neutron diffraction at 15 K. The accurate and extensive data sets lead to more precise determinations than are available from earlier work. The agreement in atomic positional and displacement parameters between the determinations at low temperature is very good.
ISSN:0108-2701
1600-5759
DOI:10.1107/S0108270100008763