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Synthesis and spectral characterization of novel compounds derived from 1,10-phenanthroline, lead(II) and tetrabutylammonium tetrafluoroborate
On interacting 1,10-phenanthroline (phen) with tetrabutylammonium tetrafluoroborate (Bu 4N·BF 4) two novel compounds have been obtained. These are the 1:1 adduct (phen)·(Bu 4N·BF 4) and the complex Pb(phen)(Bu 4N·BF 4) 3(NO 3) 2. The synthesized substances have been characterized by UV, IR and Raman...
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| Published in: | Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy Molecular and biomolecular spectroscopy, 2003-05, Vol.59 (7), p.1655-1662 |
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| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c361t-4de1497f298f4962ee879906bae00d0ff2fa6d14f2d49fcf47cd3603115d254a3 |
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| cites | cdi_FETCH-LOGICAL-c361t-4de1497f298f4962ee879906bae00d0ff2fa6d14f2d49fcf47cd3603115d254a3 |
| container_end_page | 1662 |
| container_issue | 7 |
| container_start_page | 1655 |
| container_title | Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy |
| container_volume | 59 |
| creator | Atanassova, Maria S Dimitrov, Georgi D |
| description | On interacting 1,10-phenanthroline (phen) with tetrabutylammonium tetrafluoroborate (Bu
4N·BF
4) two novel compounds have been obtained. These are the 1:1 adduct (phen)·(Bu
4N·BF
4) and the complex Pb(phen)(Bu
4N·BF
4)
3(NO
3)
2. The synthesized substances have been characterized by UV, IR and Raman spectroscopy as well as by
1H- and
19F-NMR spectroscopy. |
| doi_str_mv | 10.1016/S1386-1425(02)00397-9 |
| format | article |
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4N·BF
4) two novel compounds have been obtained. These are the 1:1 adduct (phen)·(Bu
4N·BF
4) and the complex Pb(phen)(Bu
4N·BF
4)
3(NO
3)
2. The synthesized substances have been characterized by UV, IR and Raman spectroscopy as well as by
1H- and
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4N·BF
4) two novel compounds have been obtained. These are the 1:1 adduct (phen)·(Bu
4N·BF
4) and the complex Pb(phen)(Bu
4N·BF
4)
3(NO
3)
2. The synthesized substances have been characterized by UV, IR and Raman spectroscopy as well as by
1H- and
19F-NMR spectroscopy.</description><subject>1,10-Phenanthroline</subject><subject>Adduct</subject><subject>Borates - chemical synthesis</subject><subject>Borates - chemistry</subject><subject>Lead - chemistry</subject><subject>Lead complexes</subject><subject>Magnetic Resonance Spectroscopy</subject><subject>Molecular Structure</subject><subject>Organometallic Compounds - chemical synthesis</subject><subject>Organometallic Compounds - chemistry</subject><subject>Phenanthrolines - chemistry</subject><subject>Quaternary Ammonium Compounds - chemical synthesis</subject><subject>Quaternary Ammonium Compounds - chemistry</subject><subject>Spectrophotometry, Infrared</subject><subject>Spectrophotometry, Ultraviolet</subject><subject>Spectrum Analysis, Raman</subject><subject>Tetrabutylammonium tetrafluoroborate</subject><issn>1386-1425</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2003</creationdate><recordtype>article</recordtype><recordid>eNqFkU2LFDEQhnNQ3HX1Jyg5yS5sayWd_shJZPFjYMHD6jlkkgoT6U7aJD0w_gh_s9mZQY-eCqre9y3qKUJeMXjLgPXvHlg79g0TvLsGfgPQyqGRT8jl3_YFeZ7zDwBgI4dn5ILxgQkYx0vy--EQyg6zz1QHS_OCpiQ9UbPTSZuCyf_SxcdAo6Mh7rFO4rzENdhMbZ3u0VKX4kzZLYNm2WHQNS_FyQe8pRNqe73Z3ByzC9bk7VoOk57nGPw6n1puWmOK25h0wRfkqdNTxpfnekW-f_r47e5Lc__18-buw31j2p6VRlhkQg6Oy9EJ2XPEcZAS-q1GAAvOcad7y4TjVkhnnBiMbXtoGess74Rur8ibU-6S4s8Vc1GzzwanSQeMa1ZDy3nPeVeF3UloUsw5oVNL8rNOB8VAPcJXR_jqkbICro7wlay-1-cF63ZG-891Jl8F708CrGfuPSaVjcdg0PpUf6Bs9P9Z8QeBFJli</recordid><startdate>20030501</startdate><enddate>20030501</enddate><creator>Atanassova, Maria S</creator><creator>Dimitrov, Georgi D</creator><general>Elsevier B.V</general><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20030501</creationdate><title>Synthesis and spectral characterization of novel compounds derived from 1,10-phenanthroline, lead(II) and tetrabutylammonium tetrafluoroborate</title><author>Atanassova, Maria S ; Dimitrov, Georgi D</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c361t-4de1497f298f4962ee879906bae00d0ff2fa6d14f2d49fcf47cd3603115d254a3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2003</creationdate><topic>1,10-Phenanthroline</topic><topic>Adduct</topic><topic>Borates - chemical synthesis</topic><topic>Borates - chemistry</topic><topic>Lead - chemistry</topic><topic>Lead complexes</topic><topic>Magnetic Resonance Spectroscopy</topic><topic>Molecular Structure</topic><topic>Organometallic Compounds - chemical synthesis</topic><topic>Organometallic Compounds - chemistry</topic><topic>Phenanthrolines - chemistry</topic><topic>Quaternary Ammonium Compounds - chemical synthesis</topic><topic>Quaternary Ammonium Compounds - chemistry</topic><topic>Spectrophotometry, Infrared</topic><topic>Spectrophotometry, Ultraviolet</topic><topic>Spectrum Analysis, Raman</topic><topic>Tetrabutylammonium tetrafluoroborate</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Atanassova, Maria S</creatorcontrib><creatorcontrib>Dimitrov, Georgi D</creatorcontrib><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Atanassova, Maria S</au><au>Dimitrov, Georgi D</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and spectral characterization of novel compounds derived from 1,10-phenanthroline, lead(II) and tetrabutylammonium tetrafluoroborate</atitle><jtitle>Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy</jtitle><addtitle>Spectrochim Acta A Mol Biomol Spectrosc</addtitle><date>2003-05-01</date><risdate>2003</risdate><volume>59</volume><issue>7</issue><spage>1655</spage><epage>1662</epage><pages>1655-1662</pages><issn>1386-1425</issn><abstract>On interacting 1,10-phenanthroline (phen) with tetrabutylammonium tetrafluoroborate (Bu
4N·BF
4) two novel compounds have been obtained. These are the 1:1 adduct (phen)·(Bu
4N·BF
4) and the complex Pb(phen)(Bu
4N·BF
4)
3(NO
3)
2. The synthesized substances have been characterized by UV, IR and Raman spectroscopy as well as by
1H- and
19F-NMR spectroscopy.</abstract><cop>England</cop><pub>Elsevier B.V</pub><pmid>12714088</pmid><doi>10.1016/S1386-1425(02)00397-9</doi><tpages>8</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1386-1425 |
| ispartof | Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy, 2003-05, Vol.59 (7), p.1655-1662 |
| issn | 1386-1425 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_73226225 |
| source | ScienceDirect Journals |
| subjects | 1,10-Phenanthroline Adduct Borates - chemical synthesis Borates - chemistry Lead - chemistry Lead complexes Magnetic Resonance Spectroscopy Molecular Structure Organometallic Compounds - chemical synthesis Organometallic Compounds - chemistry Phenanthrolines - chemistry Quaternary Ammonium Compounds - chemical synthesis Quaternary Ammonium Compounds - chemistry Spectrophotometry, Infrared Spectrophotometry, Ultraviolet Spectrum Analysis, Raman Tetrabutylammonium tetrafluoroborate |
| title | Synthesis and spectral characterization of novel compounds derived from 1,10-phenanthroline, lead(II) and tetrabutylammonium tetrafluoroborate |
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