Microwave extraction of organochlorine pesticides from soils

The purpose of this work was to develop a rapid, reliable and sensitive method for the extraction of organochlorine pesticides from soils using microwave energy with closed vessel technology. Three oven programs were assayed with two different solvent mixtures in order to achieve adequate experiment...

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Bibliographic Details
Published in:Analytical and bioanalytical chemistry 2003-04, Vol.375 (8), p.1225-1228
Main Authors: Concha-Graña, E, Barriada-Pereira, M, Turnes-Carou, M I, Muniategui-Lorenzo, S, López-Mahía, P, Prada Rodríguez, D
Format: Article
Language:English
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Summary:The purpose of this work was to develop a rapid, reliable and sensitive method for the extraction of organochlorine pesticides from soils using microwave energy with closed vessel technology. Three oven programs were assayed with two different solvent mixtures in order to achieve adequate experimental conditions for the complete extraction of organochlorine pesticides from the matrix. The method was validated using a certified reference soil material (CRM804-050).
ISSN:1618-2642
DOI:10.1007/s00216-003-1823-3