Simultaneous Injection-Effective Mixing Analysis of Palladium

A novel concept of simultaneous injection-effective mixing analysis (SIEMA) is proposed, and a SIEMA method applied to the spectrophotometric determination of palladium using a water-soluble chromogenic reagent has been demonstrated. The flow configuration of SIEMA is a hybrid format of flow injecti...

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Bibliographic Details
Published in:Analytical Sciences 2010/02/10, Vol.26(2), pp.143-144
Main Authors: TESHIMA, Norio, NOGUCHI, Daisuke, JOICHI, Yasutaka, LENGHOR, Narong, OHNO, Noriko, SAKAI, Tadao, MOTOMIZU, Shoji
Format: Article
Language:English
Subjects:
Analytical Chemistry
Chemistry
Rapid Communications
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Summary:A novel concept of simultaneous injection-effective mixing analysis (SIEMA) is proposed, and a SIEMA method applied to the spectrophotometric determination of palladium using a water-soluble chromogenic reagent has been demonstrated. The flow configuration of SIEMA is a hybrid format of flow injection analysis (FIA), sequential injection analysis (SIA) and multicommutation in flow-based analysis. Sample and reagent solutions are aspirated into each holding coil through each solenoid valve by a syringe pump, and then the zones are simultaneously dispensed (injected) into a mixing coil by reversed flow toward a detector through a confluence point. This results in effective mixing and rapid detection with low reagent consumption.
ISSN:0910-6340
1348-2246
DOI:10.2116/analsci.26.143