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Analysis of sulfonamides in environmental water samples based on magnetic mixed hemimicelles solid-phase extraction coupled with HPLC–UV detection
The magnetic mixed hemimicelles solid-phase extraction (MMHSPE), based on the adsorption of cation surfactant octadecyltrimethylammonium bromide (OTMABr) onto magnetite nanoparticles (Fe 3O 4 NPs) to form mixed hemimicelles, was proposed for the preconcentration of several sulfonamides (SAs) compoun...
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| Published in: | Chemosphere (Oxford) 2009-11, Vol.77 (10), p.1306-1312 |
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| creator | Sun, Lei Chen, Ligang Sun, Xin Du, Xiaobo Yue, Yanshan He, Dongqing Xu, Haoyan Zeng, Qinglei Wang, Hui Ding, Lan |
| description | The magnetic mixed hemimicelles solid-phase extraction (MMHSPE), based on the adsorption of cation surfactant octadecyltrimethylammonium bromide (OTMABr) onto magnetite nanoparticles (Fe
3O
4 NPs) to form mixed hemimicelles, was proposed for the preconcentration of several sulfonamides (SAs) compounds including sulfamethoxazole (SMX), sulfamethoxydiazine (SMD), sulfadimethoxine (SDM) and sulfaquinoxaline (SQX) from environmental water samples. This method avoided the time-consuming column-passing process of loading large volume samples in traditional SPE through the rapid isolation of OTMABr-coated Fe
3O
4 NPs with an adscititious magnet. Mixed hemimicelles formed on the surface of Fe
3O
4 NPs by OTMABr showed great adsorptive tendency towards analytes. The OTMABr-coated Fe
3O
4 NPs adsorbents were easy to be prepared, low cost and environmentally friendly. A comprehensive study on the adsorption conditions such as the amount of the surfactant, the solution pH, the desorption condition and the maximum extraction sample volume were optimized. A concentration factor of 1000 was achieved by the extraction of 500
mL of environmental water samples using MMHSPE. Detection limits obtained for SMX, SMD, SDM and SQX were 0.026, 0.024, 0.033 and 0.030
μg
L
−1, respectively. Good recoveries (70–102%) with low relative standard deviations (1–6%) were achieved in analyzing spiked water samples. Low concentration of SQX was found in hospital primary and final sewage effluent sample. |
| doi_str_mv | 10.1016/j.chemosphere.2009.09.049 |
| format | article |
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3O
4 NPs) to form mixed hemimicelles, was proposed for the preconcentration of several sulfonamides (SAs) compounds including sulfamethoxazole (SMX), sulfamethoxydiazine (SMD), sulfadimethoxine (SDM) and sulfaquinoxaline (SQX) from environmental water samples. This method avoided the time-consuming column-passing process of loading large volume samples in traditional SPE through the rapid isolation of OTMABr-coated Fe
3O
4 NPs with an adscititious magnet. Mixed hemimicelles formed on the surface of Fe
3O
4 NPs by OTMABr showed great adsorptive tendency towards analytes. The OTMABr-coated Fe
3O
4 NPs adsorbents were easy to be prepared, low cost and environmentally friendly. A comprehensive study on the adsorption conditions such as the amount of the surfactant, the solution pH, the desorption condition and the maximum extraction sample volume were optimized. A concentration factor of 1000 was achieved by the extraction of 500
mL of environmental water samples using MMHSPE. Detection limits obtained for SMX, SMD, SDM and SQX were 0.026, 0.024, 0.033 and 0.030
μg
L
−1, respectively. Good recoveries (70–102%) with low relative standard deviations (1–6%) were achieved in analyzing spiked water samples. Low concentration of SQX was found in hospital primary and final sewage effluent sample.</description><identifier>ISSN: 0045-6535</identifier><identifier>EISSN: 1879-1298</identifier><identifier>DOI: 10.1016/j.chemosphere.2009.09.049</identifier><identifier>PMID: 19836824</identifier><identifier>CODEN: CMSHAF</identifier><language>eng</language><publisher>Kidlington: Elsevier Ltd</publisher><subject>Adsorption ; Air. Soil. Water. Waste. Feeding ; Animal, plant and microbial ecology ; Applied ecology ; Applied sciences ; Biological and medical sciences ; Cations ; Chromatography, High Pressure Liquid - methods ; Ecotoxicology, biological effects of pollution ; Environment. Living conditions ; Environmental water samples ; Exact sciences and technology ; Extraction ; Fe 3O 4 nanoparticles ; Ferric Compounds - chemistry ; Fundamental and applied biological sciences. Psychology ; Hydrogen-Ion Concentration ; Magnetic mixed hemimicelles solid-phase extraction ; Magnetics ; Medical sciences ; Metal Nanoparticles - chemistry ; Micelles ; Pollution ; Public health. Hygiene ; Public health. Hygiene-occupational medicine ; SAS ; Solid Phase Extraction - methods ; Spectrophotometry, Ultraviolet - methods ; Standard deviation ; Sulfonamides ; Sulfonamides - analysis ; Sulfonamides - chemistry ; Sulfonamides - isolation & purification ; Surface chemistry ; Surface-Active Agents - chemistry ; Surfactants ; Water Pollutants, Chemical - analysis ; Water Pollutants, Chemical - chemistry ; Water Pollutants, Chemical - isolation & purification</subject><ispartof>Chemosphere (Oxford), 2009-11, Vol.77 (10), p.1306-1312</ispartof><rights>2009 Elsevier Ltd</rights><rights>2015 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c501t-803f64994bf07f0fa6f883b647d290272ccb4f96ba0fed1475f96ff8ec361b4c3</citedby><cites>FETCH-LOGICAL-c501t-803f64994bf07f0fa6f883b647d290272ccb4f96ba0fed1475f96ff8ec361b4c3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=22177314$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/19836824$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Sun, Lei</creatorcontrib><creatorcontrib>Chen, Ligang</creatorcontrib><creatorcontrib>Sun, Xin</creatorcontrib><creatorcontrib>Du, Xiaobo</creatorcontrib><creatorcontrib>Yue, Yanshan</creatorcontrib><creatorcontrib>He, Dongqing</creatorcontrib><creatorcontrib>Xu, Haoyan</creatorcontrib><creatorcontrib>Zeng, Qinglei</creatorcontrib><creatorcontrib>Wang, Hui</creatorcontrib><creatorcontrib>Ding, Lan</creatorcontrib><title>Analysis of sulfonamides in environmental water samples based on magnetic mixed hemimicelles solid-phase extraction coupled with HPLC–UV detection</title><title>Chemosphere (Oxford)</title><addtitle>Chemosphere</addtitle><description>The magnetic mixed hemimicelles solid-phase extraction (MMHSPE), based on the adsorption of cation surfactant octadecyltrimethylammonium bromide (OTMABr) onto magnetite nanoparticles (Fe
3O
4 NPs) to form mixed hemimicelles, was proposed for the preconcentration of several sulfonamides (SAs) compounds including sulfamethoxazole (SMX), sulfamethoxydiazine (SMD), sulfadimethoxine (SDM) and sulfaquinoxaline (SQX) from environmental water samples. This method avoided the time-consuming column-passing process of loading large volume samples in traditional SPE through the rapid isolation of OTMABr-coated Fe
3O
4 NPs with an adscititious magnet. Mixed hemimicelles formed on the surface of Fe
3O
4 NPs by OTMABr showed great adsorptive tendency towards analytes. The OTMABr-coated Fe
3O
4 NPs adsorbents were easy to be prepared, low cost and environmentally friendly. A comprehensive study on the adsorption conditions such as the amount of the surfactant, the solution pH, the desorption condition and the maximum extraction sample volume were optimized. A concentration factor of 1000 was achieved by the extraction of 500
mL of environmental water samples using MMHSPE. Detection limits obtained for SMX, SMD, SDM and SQX were 0.026, 0.024, 0.033 and 0.030
μg
L
−1, respectively. Good recoveries (70–102%) with low relative standard deviations (1–6%) were achieved in analyzing spiked water samples. Low concentration of SQX was found in hospital primary and final sewage effluent sample.</description><subject>Adsorption</subject><subject>Air. Soil. Water. Waste. Feeding</subject><subject>Animal, plant and microbial ecology</subject><subject>Applied ecology</subject><subject>Applied sciences</subject><subject>Biological and medical sciences</subject><subject>Cations</subject><subject>Chromatography, High Pressure Liquid - methods</subject><subject>Ecotoxicology, biological effects of pollution</subject><subject>Environment. Living conditions</subject><subject>Environmental water samples</subject><subject>Exact sciences and technology</subject><subject>Extraction</subject><subject>Fe 3O 4 nanoparticles</subject><subject>Ferric Compounds - chemistry</subject><subject>Fundamental and applied biological sciences. Psychology</subject><subject>Hydrogen-Ion Concentration</subject><subject>Magnetic mixed hemimicelles solid-phase extraction</subject><subject>Magnetics</subject><subject>Medical sciences</subject><subject>Metal Nanoparticles - chemistry</subject><subject>Micelles</subject><subject>Pollution</subject><subject>Public health. Hygiene</subject><subject>Public health. 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Soil. Water. Waste. Feeding</topic><topic>Animal, plant and microbial ecology</topic><topic>Applied ecology</topic><topic>Applied sciences</topic><topic>Biological and medical sciences</topic><topic>Cations</topic><topic>Chromatography, High Pressure Liquid - methods</topic><topic>Ecotoxicology, biological effects of pollution</topic><topic>Environment. Living conditions</topic><topic>Environmental water samples</topic><topic>Exact sciences and technology</topic><topic>Extraction</topic><topic>Fe 3O 4 nanoparticles</topic><topic>Ferric Compounds - chemistry</topic><topic>Fundamental and applied biological sciences. Psychology</topic><topic>Hydrogen-Ion Concentration</topic><topic>Magnetic mixed hemimicelles solid-phase extraction</topic><topic>Magnetics</topic><topic>Medical sciences</topic><topic>Metal Nanoparticles - chemistry</topic><topic>Micelles</topic><topic>Pollution</topic><topic>Public health. Hygiene</topic><topic>Public health. Hygiene-occupational medicine</topic><topic>SAS</topic><topic>Solid Phase Extraction - methods</topic><topic>Spectrophotometry, Ultraviolet - methods</topic><topic>Standard deviation</topic><topic>Sulfonamides</topic><topic>Sulfonamides - analysis</topic><topic>Sulfonamides - chemistry</topic><topic>Sulfonamides - isolation & purification</topic><topic>Surface chemistry</topic><topic>Surface-Active Agents - chemistry</topic><topic>Surfactants</topic><topic>Water Pollutants, Chemical - analysis</topic><topic>Water Pollutants, Chemical - chemistry</topic><topic>Water Pollutants, Chemical - isolation & purification</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Sun, Lei</creatorcontrib><creatorcontrib>Chen, Ligang</creatorcontrib><creatorcontrib>Sun, Xin</creatorcontrib><creatorcontrib>Du, Xiaobo</creatorcontrib><creatorcontrib>Yue, Yanshan</creatorcontrib><creatorcontrib>He, Dongqing</creatorcontrib><creatorcontrib>Xu, Haoyan</creatorcontrib><creatorcontrib>Zeng, Qinglei</creatorcontrib><creatorcontrib>Wang, Hui</creatorcontrib><creatorcontrib>Ding, Lan</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Environmental Engineering Abstracts</collection><collection>Technology Research Database</collection><collection>Environmental Sciences and Pollution Management</collection><collection>Engineering Research Database</collection><collection>Civil Engineering Abstracts</collection><collection>Aqualine</collection><collection>Environment Abstracts</collection><collection>Pollution Abstracts</collection><collection>Toxicology Abstracts</collection><collection>Water Resources Abstracts</collection><collection>ASFA: Aquatic Sciences and Fisheries Abstracts</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) 2: Ocean Technology, Policy & Non-Living Resources</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) 3: Aquatic Pollution & Environmental Quality</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) Professional</collection><collection>Environment Abstracts</collection><collection>MEDLINE - Academic</collection><jtitle>Chemosphere (Oxford)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Sun, Lei</au><au>Chen, Ligang</au><au>Sun, Xin</au><au>Du, Xiaobo</au><au>Yue, Yanshan</au><au>He, Dongqing</au><au>Xu, Haoyan</au><au>Zeng, Qinglei</au><au>Wang, Hui</au><au>Ding, Lan</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Analysis of sulfonamides in environmental water samples based on magnetic mixed hemimicelles solid-phase extraction coupled with HPLC–UV detection</atitle><jtitle>Chemosphere (Oxford)</jtitle><addtitle>Chemosphere</addtitle><date>2009-11-01</date><risdate>2009</risdate><volume>77</volume><issue>10</issue><spage>1306</spage><epage>1312</epage><pages>1306-1312</pages><issn>0045-6535</issn><eissn>1879-1298</eissn><coden>CMSHAF</coden><abstract>The magnetic mixed hemimicelles solid-phase extraction (MMHSPE), based on the adsorption of cation surfactant octadecyltrimethylammonium bromide (OTMABr) onto magnetite nanoparticles (Fe
3O
4 NPs) to form mixed hemimicelles, was proposed for the preconcentration of several sulfonamides (SAs) compounds including sulfamethoxazole (SMX), sulfamethoxydiazine (SMD), sulfadimethoxine (SDM) and sulfaquinoxaline (SQX) from environmental water samples. This method avoided the time-consuming column-passing process of loading large volume samples in traditional SPE through the rapid isolation of OTMABr-coated Fe
3O
4 NPs with an adscititious magnet. Mixed hemimicelles formed on the surface of Fe
3O
4 NPs by OTMABr showed great adsorptive tendency towards analytes. The OTMABr-coated Fe
3O
4 NPs adsorbents were easy to be prepared, low cost and environmentally friendly. A comprehensive study on the adsorption conditions such as the amount of the surfactant, the solution pH, the desorption condition and the maximum extraction sample volume were optimized. A concentration factor of 1000 was achieved by the extraction of 500
mL of environmental water samples using MMHSPE. Detection limits obtained for SMX, SMD, SDM and SQX were 0.026, 0.024, 0.033 and 0.030
μg
L
−1, respectively. Good recoveries (70–102%) with low relative standard deviations (1–6%) were achieved in analyzing spiked water samples. Low concentration of SQX was found in hospital primary and final sewage effluent sample.</abstract><cop>Kidlington</cop><pub>Elsevier Ltd</pub><pmid>19836824</pmid><doi>10.1016/j.chemosphere.2009.09.049</doi><tpages>7</tpages></addata></record> |
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| ispartof | Chemosphere (Oxford), 2009-11, Vol.77 (10), p.1306-1312 |
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| subjects | Adsorption Air. Soil. Water. Waste. Feeding Animal, plant and microbial ecology Applied ecology Applied sciences Biological and medical sciences Cations Chromatography, High Pressure Liquid - methods Ecotoxicology, biological effects of pollution Environment. Living conditions Environmental water samples Exact sciences and technology Extraction Fe 3O 4 nanoparticles Ferric Compounds - chemistry Fundamental and applied biological sciences. Psychology Hydrogen-Ion Concentration Magnetic mixed hemimicelles solid-phase extraction Magnetics Medical sciences Metal Nanoparticles - chemistry Micelles Pollution Public health. Hygiene Public health. Hygiene-occupational medicine SAS Solid Phase Extraction - methods Spectrophotometry, Ultraviolet - methods Standard deviation Sulfonamides Sulfonamides - analysis Sulfonamides - chemistry Sulfonamides - isolation & purification Surface chemistry Surface-Active Agents - chemistry Surfactants Water Pollutants, Chemical - analysis Water Pollutants, Chemical - chemistry Water Pollutants, Chemical - isolation & purification |
| title | Analysis of sulfonamides in environmental water samples based on magnetic mixed hemimicelles solid-phase extraction coupled with HPLC–UV detection |
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