A versatile method for rotation-synchronised 2D exchange spectroscopy of solids

A versatile, reliable, easy-to-use method to achieve rotor-synchronisation during the mixing time τ m in 2D magnetisation transfer experiments on rotating solids is shown. The limits of accuracy of the method are discussed and some examples of application are given. A full description of all technic...

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Bibliographic Details
Published in:Solid state nuclear magnetic resonance 1992-11, Vol.1 (4), p.231-234
Main Authors: Kümmerlen, Jörg, Sebald, Angelika, Weigel, Ralf
Format: Article
Language:English
Subjects:
2D exchange spectroscopy of solids
Carbon - chemistry
Carbon Isotopes
Electronics - instrumentation
Glycine - chemistry
high-resolution solid-state NMR
Magnetic Resonance Spectroscopy - instrumentation
Magnetic Resonance Spectroscopy - methods
Molecular Structure
rotation-synchronisation
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Summary:A versatile, reliable, easy-to-use method to achieve rotor-synchronisation during the mixing time τ m in 2D magnetisation transfer experiments on rotating solids is shown. The limits of accuracy of the method are discussed and some examples of application are given. A full description of all technical details is provided.
ISSN:0926-2040
1527-3326
DOI:10.1016/S0926-2040(10)80009-8