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Subsurface detection of fossil fuel pollutants by photoionization and gas chromatography/mass spectrometry
This paper describes analysis of environmental pollutants at depth without bringing sample to the surface. It is based on an improved 3-stage Peltier freeze trap, which efficiently pre-concentrates volatile coal tar and petroleum hydrocarbons, and an integrated system for detecting pollutants on-lin...
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| Published in: | Chemosphere (Oxford) 2010-09, Vol.80 (11), p.1370-1376 |
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| Main Authors: | , , |
| Format: | Article |
| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c471t-2dff06aaacfebef966d074e8491a6f7f4e2f20ded40b43cffa5aad9f2a8075be3 |
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| cites | cdi_FETCH-LOGICAL-c471t-2dff06aaacfebef966d074e8491a6f7f4e2f20ded40b43cffa5aad9f2a8075be3 |
| container_end_page | 1376 |
| container_issue | 11 |
| container_start_page | 1370 |
| container_title | Chemosphere (Oxford) |
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| creator | Robbat, Albert Considine, Thomas Antle, Patrick M. |
| description | This paper describes analysis of environmental pollutants at depth without bringing sample to the surface. It is based on an improved 3-stage Peltier freeze trap, which efficiently pre-concentrates volatile coal tar and petroleum hydrocarbons, and an integrated system for detecting pollutants on-line, in real-time by photoionization detection and quantitation by gas chromatography/mass spectrometry (GC/MS) as the probe is advanced into the subsurface. Findings indicate measurement precision and accuracy for volatiles meet EPA criteria for hazardous waste site investigations. When a Teflon membrane inlet is used to detect contaminants in groundwater, its 140
°C temperature limit restricts analyte collection in soil to
C
2-phenanthrenes. Two case studies demonstrate the probe is well-suited to tracking petroleum and coal tar plumes from source to groundwater. |
| doi_str_mv | 10.1016/j.chemosphere.2010.06.005 |
| format | article |
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°C temperature limit restricts analyte collection in soil to
C
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°C temperature limit restricts analyte collection in soil to
C
2-phenanthrenes. 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°C temperature limit restricts analyte collection in soil to
C
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| ispartof | Chemosphere (Oxford), 2010-09, Vol.80 (11), p.1370-1376 |
| issn | 0045-6535 1879-1298 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_759313945 |
| source | ScienceDirect Freedom Collection |
| subjects | Applied sciences Coal tar Coal Tar - analysis Crude oil Dense non aqueous phase liquids Environmental Monitoring - methods Exact sciences and technology Fossil Fuels - analysis Gas chromatography Gas Chromatography-Mass Spectrometry GC/MS Groundwater Hazardous waste site characterization Hazardous wastes Hydrocarbons - analysis In situ sampling probe Kinetics Mass spectrometry Photochemical Processes Photoionization Photoionization detector Pollutants Pollution Polytetrafluoroethylenes Soil Pollutants - analysis Subsurface Water Pollutants - analysis |
| title | Subsurface detection of fossil fuel pollutants by photoionization and gas chromatography/mass spectrometry |
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