Synthesis of pentafluorobenzoic anhydride: a superior derivatizing agent for lipids

Two alternative methods for preparation of pentafluorobenzoyl anhydride are described, and preliminary results on the use of this reagent for direct derivatization of the potent phospholipid autacoid, platelet-activating factor are presented.

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Bibliographic Details
Published in:Analytical chemistry (Washington) 1993-09, Vol.65 (17), p.2400-2402
Main Authors: Weintraub, Susan T, Satsangi, Rajiv K, Simmons, Anne Marie, Williams, Robert F, Pinckard, R. Neal
Format: Article
Language:English
Subjects:
Anhydrides - chemical synthesis
Benzoates - chemical synthesis
Chemistry
Chromatography, Thin Layer
Exact sciences and technology
Indicators and Reagents
Lipids
Lipids - chemistry
Noncondensed benzenic compounds
Organic chemistry
Platelet Activating Factor - analysis
Preparations and properties
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Description
Summary:Two alternative methods for preparation of pentafluorobenzoyl anhydride are described, and preliminary results on the use of this reagent for direct derivatization of the potent phospholipid autacoid, platelet-activating factor are presented.
ISSN:0003-2700
1520-6882
DOI:10.1021/ac00065a038